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47results about How to "Analytical data is reliable" patented technology

Classified display and quantitative detection method for martensite and residual austenite in M-A island

ActiveCN104111230AEffective separate quantitative analysis of contentEfficient separate quantification of distributionsPreparing sample for investigationColor/spectral properties measurementsAlcoholRoom temperature
The invention relates to microstructure classified display and quantitative detection technology in iron and steel material, belongs to the field of iron and steel material, and particularly relates to a classified display and quantitative detection method for martensite and residual austenite in low-alloy granular bainite steel martensite/austenite island (M-A island). The method comprises steps: (1) a grinding and mechanical polishing method is used for preparing a low-alloy granular bainite steel metallographic sample; (2) an electrolytic polishing method is used for removing the stress layer on the surface of the metallographic sample, a nitric acid alcohol solution of 2wt% to 6wt% is then used for carrying out pre-corrosion for 5 to 15s, and absolute alcohol is finally used for ultrasonic cleaning for 10 to 20m; (3) the metallographic sample after ultrasonic cleaning is placed in a furnace free of atmosphere protection at the temperature of 150 to 300 DEG C for heat preservation for 2 to 6 hours, and when getting out of the furnace, the metallographic sample is placed in a dryer for air cooling till the room temperature; (4) the microscopic structure is observed in a metallographic microscope, wherein polygonal ferrite and bainitic ferrite are bluish violet, the martensite is brown and the residual austenite is off-white; and (5) distribution of each phase of the structure and quantitative analysis are carried out.
Owner:SHANGHAI SHENJIANG FORGING

Method of catalytic resonance scattering spectral determination of mercury by using aptamer modified nanogold

The invention discloses a method of catalytic resonance scattering spectral determination of mercury by using aptamer modified nanogold, which comprises the following steps: Hg2+ aptamer ssDNA and nanogold are combined to form nanogold AussDNA modified by DNA, stable Hg2+aptamer-Hg2+compound is generated by T-T mismatching when Hg2+ and AussDNA coexist, nanogold is gathered under the action of high-concentration NaCl, redundant AussDNA in filtrate after membrane filtration is taken as a nano catalytic seed crystal to catalyze the reaction of Cu2+ and furfural so as to reduce Cu2+ into Cu+, Cu+ reacts with OH- in solution to generate CuOH, and finally generate Cu2O particles. From the above preparation method, a determined system and a reagent blank system of mercury concentration can be known, resonance scattering strength of the two systems are measured at the 605nm part, drawn into a standard curve, and then prepared into a sample detection system, a deltaI sample is solved, the mercury content in the sample is calculated on the standard curve. The invention has the advantages of high sensitivity, strong specificity, wide determination range, simple equipment, and convenient operation, is suitable for determining various samples containing mercury, and provides reliable analysis data for environment monitoring, foods, cosmetics and other fields.From the above method, a determined system and a reagent blank system of which the mercury concentration is known can be prepared, resonance scattering strength of the two systems are measured at the 605nm part and drawn into a standard curve, and then a sample detection system is prepared, delta I sample is calculated, the mercury content in the sample is calculated by the standard curve.The invention has the advantages of high sensitivity, strong specificity, wide determination range, simple equipment, and convenient operation, and is suitable for determining various samples containing mercury.
Owner:GUANGXI NORMAL UNIV

Sample preparation method by fusing medium-carbon ferrochrome and high-carbon ferrochrome

The invention discloses a sample preparation method by fusing medium-carbon ferrochrome and high-carbon ferrochrome, which comprises the following steps of: (1) suspending wall: fusing lithium tetraborate in a platinum crucible, and rotating the platinum crucible, so that the fused lithium tetraborate is evenly suspended at the side wall and the bottom of the surface in the crucible, and a fusion agent crucible is formed; (2) previously oxidizing: mixing oxidizing agent with a standard sample or a sample to be tested of the medium-carbon ferrochrome or the high-carbon ferrochrome, and oxidizing in the fusion agent crucible which is cooled to be room temperature; (3) fusing: fusing the previously-oxidized standard sample or the sample to be tested; and (4) preparing a sample glass piece: cooling the fused standard sample or the sample to be tested to be room temperature, and forming the glass piece of the standard sample or the sample to be tested by the fused sample. Therefore, the influence of line spectrum peak shift or spectrum peak shape change and the like to an analysis result caused by the inconsistent absorption and enhancement effect, the mineral effect, the surface effect, the granularity and the analysis element chemical valence among ferrochrome alloy elements can be effectively eliminated.
Owner:HBIS COMPANY LIMITED HANDAN BRANCH COMPANY

Nonlinear ultrasonic detection method for evaluating thermo-oxidative ageing of organic material

A nonlinear ultrasonic detection method for evaluating the thermo-oxidative ageing of an organic material comprises the following steps: building an organic material thermo-oxidative ageing damage nonlinear ultrasonic detection system based on a nonlinear acoustic detection system; respectively setting corresponding parameters of an excitation signal and a reception signal, and finely adjusting the corresponding parameters of the excitation signal and the reception signal by a time domain waveform signal observed and received by an oscilloscope; selecting the optimum work frequency range of a probe according to the frequency characteristic of the ultrasonic probe, and determining the initial frequency and the ending frequency of the swept frequency range; adjusting integrator gate parameters, carrying out frequency sweeping to obtain the change rule of an supersonic wave fundamental wave amplitude and a secondary harmonic amplitude with the frequency, and storing the change rule in a computer; calculating corresponding nonlinear coefficients of all frequency points in the swept frequency range, and calculating the accumulated nonlinear effect in the swept frequency range; and determining a corresponding relationship between the accumulated nonlinear effect and the thermo-oxidative ageing time of the organic material, and assessing the existence or not and the degree of the thermo-oxidative ageing damage of the organic material.
Owner:BEIJING UNIV OF TECH

Self-propelled hollow slip casting anchor rod with stress-measuring function and operating method

The invention relates to the technical field of tunnel and underground construction anchoring equipment, in particular to a self-propelled hollow slip casting anchor rod with a stress-measuring function and an operating method. The self-propelled hollow slip casting anchor rod with the stress-measuring function includes a rod body with a hollow structure, a self-propelled drill is connected at thefront end of the rod body, and the back end of the rod body is provided with a slip casting opening which communicates with an inner cavity of the rod body; and the rod body is further provided witha stress-measuring device and an anchoring structure which is close to the self-propelled drill. According to the self-propelled hollow slip casting anchor rod with the stress-measuring function, thestress-measuring device is arranged to combine the processes of drilling, anchoring and slip casting into the same construction process, and the anchoring can be achieved in short time; and stress conditions of all sections of the anchoring rod in the supporting process can be monitored, so that the supporting mechanism of action and the stress conditions of the anchoring rod under the various kinds of surrounding rock conditions can be known, and critical evidences and references are supplied to the research of design parameters for the anchoring rod, improvement of the construction techniqueand the surrounding rock failure mechanism.
Owner:SOUTHWEST PETROLEUM UNIV

Method for measuring content of aluminum, silicon and zinc in coating of aluminum-plated zinc plate

The invention provides a method for measuring the content of aluminum, silicon and zinc in the coating of an aluminum-plated zinc plate, comprising the following steps: dissolving a sample to be measured by hydrochloric acid and sodium hydroxide, introducing dissolved solution into an inductively coupled plasma atomic emission spectrometer, and automatically calculating and displaying the concentration of aluminum, silicon and zinc in the coating sample according to the spectral line intensity which is stored in the inductively coupled plasma atomic emission spectrometer of the standard aluminum, silicon and zinc solution with measured concentration. The method adopting chemical and physical analysis has greatly simplified processes, high analysis speed and high accuracy and is easy to master and operate. The linear correlation coefficient of the measured sample and the standard work curve is more than 0.999, the content of aluminum, silicon and zinc can be measured at the same time by dissolving the sample for one time, and reliable analysis data can be provided rapidly for the manufacturing plant. In addition, a few kinds of chemical agents is adopted, a small amount of the chemical agents is used, and the pollution of the medicament to the environment is reduced.
Owner:ANGANG STEEL CO LTD

Multi-temporal high-resolution remote sensing image building extraction method based on multi-feature LSTM network

The invention discloses a multi-temporal high-resolution remote sensing image building extraction method based on a multi-feature LSTM network, and belongs to the technical field of satellite remote sensing image processing and application. The method aims to solve the problems of low accuracy, high error rate, fuzzy boundary and the like of a building extraction result of an existing method. According to the invention, a plurality of multi-temporal high-resolution No.2 remote sensing images are used as data sources; building spectral characteristics are extracted by using a method based on HSI color transformation; based on a method of combining graph segmentation and conditional random field post-processing, shape features of a building are extracted, based on a Gabor wavelet transform method, texture information features of the building are extracted, and based on a DSBI index method, index features of the building are extracted. A building characteristic set with 60 characteristicwave bands is formed by the extracted spectrum, shape, texture and index characteristics of the multi-temporal building, a manufactured building sample and a label are sent into an LSTM network to obtain a building coarse extraction result, and a final result is obtained after morphological processing.
Owner:JILIN UNIV

A method and apparatus for establishing a computable road network

The invention discloses a method and an apparatus for establishing a computable road network, wherein, the method comprises the following steps: collecting static and dynamic data of the road network;the road nodes being calibrated according to the static data of the road network, and the nodes being connected into roads according to the connection relations among the nodes, and the basic road network being constructed; constructing a connectivity road network according to the connectivity information between roads; according to the static and dynamic data of the road network, the traffic facilities in the road network being precisely calibrated by the calibration function and the computable road network being constructed. A basic road network is established according to the calibration node, then the connectivity road network is constructed and all kinds of traffic facilities are demarcated, and the computable road network is constructed, which can be calculated for different nodes and roads to obtain more accurate information of the road network, and the topological relationship of the road is used in the construction process, which is suitable for the calculation of complex road network and provides reliable analysis data for traffic operation, management and so on. As a method and a device for establishing a computable road network, the invention can be widely applied in the field of electronic map.
Owner:GUANGDONG FUNDWAY TECH

Anti-seismic testing device for karst pile foundation based on minitype vibration platform model

The invention discloses an anti-seismic testing device for a karst pile foundation based on a minitype vibration platform model, and belongs to the technical field of anti-seismic tests for pile foundations. A pile foundation model of the anti-seismic testing device is embedded in a prefabricated top plate, the prefabricated top plate is arranged on the tops of two supports, gaps between the supports and a visual simulation box are filled with a simulated similar material, and several strain devices are uniformly arranged on the upper surface and lower surface of the prefabricated top plate; adisplacement changing marking pen is arranged in the simulated similar material, movable striped coordinate paper used for recording a displacement changing track is arranged on a front-side panel ofthe visual simulation box, and a rolling device used for driving the striped coordinated paper to move is arranged on the outer side of the visual simulation box. The anti-seismic testing device canreally simulate the prefabricated top plate, the bearing principle of the karst pile foundation and sedimentation conditions of the whole structure of the karst pile foundation under the small earthquake condition in a laboratory to obtain the reasonable and reliable thickness of the top plate of a karst cave and the pile diameter, and the stability of the karst pile foundation in a practical project is ensured.
Owner:YELLOW RIVER CONSERVANCY TECHN INST

Determination method of iron content in coating of alloying hot galvanized plate

The invention discloses a determination method of the iron content in a coating of an alloying hot galvanized plate and belongs to the technical field of detection of alloying galvanized plates. The determination method comprises the steps of: leading a volumetric flask of a standard stock solution into inductively coupled plasma emission spectrum equipment, and drawing a standard solution working curve for forming Fe; placing an alloying hot galvanized plate coating sample into a stripping device, and pouring 50ml of stripping liquid into the stripping device to dissolve the coating until bubbles disappear completely; pouring the reacted stripping liquid into the volumetric flask, and adding ultrapure water for constant volume being 100ml to obtain a sample to be tested; leading the sample to be tested into the inductively coupled plasma emission spectrum equipment for determination, so as to obtain the iron content in the coating of the alloying hot galvanized plate through the calculation of the inductively coupled plasma emission spectrum equipment. The determination method is high in analysis speed and accuracy, the linear correlation coefficient of the tested sample and the standard working curve is greater than 0.999, and reliable analysis data can be provided quickly.
Owner:SHOUGANG CORPORATION

Grouting sealing hole stop grout visual experimental device and experimental method thereof

The utility model provides a grouting sealing hole stop grout visual experimental device which comprises a pressure supply system, a grout supply system and a sealing hole stop grout visual system which are mutually connected. The pressure provided by the pressure supply system allows the grout in the grout supply system to be injected into the transparent sealing hole stop grout visual system. The device also comprises a pair of monitoring systems which carry out whole-process monitoring on the grout injection process. An experimental method comprises the steps of debugging and starting the monitoring system to carry out recording, closing the pressure adjusting value of the pressure supply system and pressing air into the system, starting the grout supply system such that the grout enters into the sealing hole stop grout visual system under the effect of high pressure air under a set start and stop time alternative change parameter and pulsing grouting is effectively simulated, and collecting and processing various parameters in a grouting experimental process through a monitoring system and analyzing the parameters to complete the experiment. The experimental device has the advantage of simple structure, convenient assembly and low cost, and the pressure change and sealing hole stop grout parameters can be effectively simulated.
Owner:CHANGSHA UNIVERSITY OF SCIENCE AND TECHNOLOGY +1

Test sample treatment method for simultaneously measuring content of silicon and phosphor in silicon-manganese alloy by ICP

The invention discloses a test sample treatment method for simultaneously measuring content of silicon and phosphor in a silicon-manganese alloy by ICP. The test sample treatment method comprises the following steps: weighing 0.1000g of a silicon-manganese alloy test sample with particle size of 160-200mesh, putting the silicon-manganese alloy test sample into filter paper which is pre-filled with 2.0-2.5g of a mixed solvent of anhydrous sodium carbonate and boric acid in a ratio of 2 to 1, uniformly mixing, packaging and putting into an iron crucible with a graphite layer bottom for fusing for 12-18 minutes at 800-900 DEG C, cooling for 2-3 minutes to obtain a sample, putting the sample into a container which is pre-filled with 90-110ml of a diluted hydrochloric acid solution consisting of hydrochloric acid and water in a ratio of 1 to 3, dissolving clinkers, filtering the obtained sample through rapid quantitative filter paper into a 250ml volumetric flask, cleaning the sample containing container and the filter paper with deionized water, and adding deionized water to the scale after cooling the filtrate and washing liquor. According to the test sample treatment method, the silicon-manganese alloy test sample is fused and decomposed through an alkaline fusion method, thereby avoiding volatilization loss of silicon when hydrofluoric acid is added to dissolve the test sample through an acid dissolving method; the test sample is completely decomposed without interference or dissipation, so that the analyzed results are accurate and stable; moreover, an ICP spectrograph is used for simultaneously measuring the content of silicon and phosphor in the silicon-manganese alloy.
Owner:WUKUN STEEL

Classified display and quantitative detection method for martensite and retained austenite in m‑a islands

The invention relates to microstructure classified display and quantitative detection technology in iron and steel material, belongs to the field of iron and steel material, and particularly relates to a classified display and quantitative detection method for martensite and residual austenite in low-alloy granular bainite steel martensite / austenite island (M-A island). The method comprises steps: (1) a grinding and mechanical polishing method is used for preparing a low-alloy granular bainite steel metallographic sample; (2) an electrolytic polishing method is used for removing the stress layer on the surface of the metallographic sample, a nitric acid alcohol solution of 2wt% to 6wt% is then used for carrying out pre-corrosion for 5 to 15s, and absolute alcohol is finally used for ultrasonic cleaning for 10 to 20m; (3) the metallographic sample after ultrasonic cleaning is placed in a furnace free of atmosphere protection at the temperature of 150 to 300 DEG C for heat preservation for 2 to 6 hours, and when getting out of the furnace, the metallographic sample is placed in a dryer for air cooling till the room temperature; (4) the microscopic structure is observed in a metallographic microscope, wherein polygonal ferrite and bainitic ferrite are bluish violet, the martensite is brown and the residual austenite is off-white; and (5) distribution of each phase of the structure and quantitative analysis are carried out.
Owner:SHANGHAI SHENJIANG FORGING

Sampling control system for online detection of VOCs in environmental chambers

The invention relates to the technical field of environmental protection, and particularly relates to a sampling control system for online detection of VOCs in environmental chambers. The sampling control system comprises a multi-way electromagnetic switching valve, an online gas chromatograph, a sampling pump and a PLC (programmable logic controller), wherein a gas outlet path contact of the multi-way electromagnetic switching valve is respectively switched and conducted with each gas inlet path contact, and the gas outlet path contact is connected to a sample inlet of the online gas chromatograph through the sampling pump; a plurality of gas inlet path contacts of the multi-way electromagnetic switching valve are respectively connected to sampling ports of a plurality of environment chambers in a one-to-one correspondence manner; and an I / O signal output contact of the online gas chromatograph is connected to an I / O signal input contact of the PLC, and an I / O signal output contact ofthe PLC is connected to a circuit control device of the multi-way electromagnetic switching valve. According to the sampling control system, one set of detection equipment can detect VOCs in a plurality of environment chambers, intermediate links are omitted, analysis data is reliable, the use cost is reduced for a user, and the occupied space is saved.
Owner:SHANGHAI FUXUAN ENVIRONMENTAL PROTECTION TECH CO LTD +1

A method for measuring nutrients in soil

ActiveCN107894405AAccurate measurementAvoid the problem of difficult guarantee of measurement reliabilityPreparing sample for investigationColor/spectral properties measurementsCentrifugationPeak value
A method for measuring nutrients in soil is disclosed. The method includes a sampling step, namely a step of sampling the soil, with the sampling depth being 0.5-1.5 m; a solution preparing step, namely a step of weighing 10 parts by mass of the sieved soil, adding 80-100 parts by mass of deionized water into the soil, adding 2-3 parts by mass of an extracting agent into the mixture, stirring themixture at a high speed of 2000-3000 r/min for 10-20 min, and then stirring the mixture at a rotating speed of 40-60 r/min to achieve hydration; a step of allowing the mixture to stand, namely a stepof allowing the liquid mixture obtained in the step A2 to stand at 30-40 DEG C for 2-3 h; a step of separation, namely a step of inserting two electrode plates into the liquid mixture, and inputting steep pulse current to the two electrode plates, with the peak value of steep pluses being 150-180 V, the pulse width being 0.5-0.8 ms, the repetition frequency being 200-300 kHz, and the pulse steepness being 50-100 ns; a step of centrifugation, namely a step of adding a separated liquid obtained in the step A4 into a centrifuge, and performing centrifugation at a rotating speed of 10000-15000 r/min; and a step of measurement, namely a step of drawing a liquid supernatant after centrifugation, and measuring nutrients in the liquid supernatant by utilizing an ultraviolet-visible light spectrophotometer. When the method is used for measuring nutrient ions in soil, measured data are more accurate and the measurement efficiency is higher.
Owner:XIAN BOTANICAL GARDEN SHAANXI PROV

Constant temperature control module and microwave scintiloscope

PendingCN109164508ASimple circuit and control structure designImprove heat transfer efficiencyInstrumentsData transmissionCollections data
The invention discloses a microwave scintiloscope, comprising an antenna reflection metal cover, a constant temperature heating module and a heat conduction connecting piece, wherein a constant temperature control module is composed of a controller, a PWM duty ratio pulse generator, a heating circuit and a heating resistor, which are connected with each other in sequence, a temperature sensing probe is installed in the antenna reflection metal cover to transmit temperature collection data to the controller, the controller uses the PID technology to calculate the data returned by the temperature sensing and converts the data into an output signal of the controller, the PWM duty ratio pulse generator converts the output signal into a PWM waveform of a corresponding duty ratio for output, theheating resistor is heated by the heating circuit, and the heat is transferred to the antenna reflection metal cover by the heat conduction connecting piece. The circuit and control structure designof the microwave scintiloscope disclosed by the invention is simple, the heat conduction efficiency is high, and the microwave scintiloscope capable of providing reliable analytical data for the scientific research while working in a stable temperature environment is provided while achieving the purpose of saving resources and reducing the cost.
Owner:北京雨根科技有限公司

Vibration isolation support for mounting static leveling instrument and design method of vibration isolation support

The invention discloses a vibration isolation support for mounting a static force level gauge and a design method of the vibration isolation support, which can effectively reduce the interference of liquid level oscillation on the measurement of the static force level gauge. The vibration isolation support for installing the static force level gauge is an adjustable passive vibration isolation support, the static force level gauge is placed on the vibration isolation support, the liquid level oscillation phenomenon caused by environment pulsation and vehicle excitation can be effectively eliminated, the accuracy of bridge safety monitoring is enhanced, and the safety of a bridge is improved. High-reliability analysis data is provided for subsequent bridge operation state evaluation, the health condition of the bridge is truly reflected, unnecessary maintenance cost is reduced, and the maintenance cost of the whole life cycle of the bridge can be effectively reduced. The bridge deflection monitoring device solves the problem that the monitoring accuracy is affected by liquid level oscillation in a communicating pipe of a static force level gauge when the bridge deflection is monitored by the static force level gauge in the prior art.
Owner:CHINA CONSTR EIGHT ENG DIV CORP LTD

A seismic test device for karst pile foundation based on a small shaking table model

The invention discloses a karst pile foundation anti-seismic testing test device based on a small-scale shaking table model, and belongs to the technical field of pile foundation anti-seismic testing. The pile foundation model of the seismic test device is embedded in the prefabricated roof, and the prefabricated roof is set on the top of the two supports, and similar materials are filled in the gap between the supports and the visual simulation box, and several strain gauges are evenly arranged On the upper surface and the lower surface of the prefabricated top plate; a displacement change marking pen is set in the simulation similar material, and a movable strip coordinate paper for recording the displacement change track is set on the front side panel of the visual simulation box, and the visual simulation The outer side of the box is provided with a winding device for driving the strip graph paper to move. The seismic test device of the present invention can truly simulate the bearing mechanism of prefabricated roof and karst pile foundation in the laboratory and the settlement of the overall structure in small earthquakes, obtain reasonable and reliable thickness of karst cave roof and pile diameter, and ensure karst pile foundation in actual engineering of stability.
Owner:YELLOW RIVER CONSERVANCY TECHN INST

Building extraction method of multi-temporal high-resolution remote sensing images based on multi-feature lstm network

The invention discloses a multi-temporal high-resolution remote sensing image building extraction method based on a multi-feature LSTM network, which belongs to the technical field of satellite remote sensing image processing and application. The purpose is to solve the problems of low accuracy rate, high misclassification rate and blurred boundary of building extraction results in existing methods. The present invention uses multiple multi-temporal Gaofen No. 2 remote sensing images as the data source, uses the method based on HSI color transformation to extract the spectral features of the building, and extracts the shape features of the building based on the method of combining image segmentation and conditional random field post-processing. The method based on Gabor wavelet transform to extract the texture information features of the building and the method based on the DSBI index to extract the index features of the building, and the extracted spectrum, shape, texture and index features of the multi-temporal buildings are composed of 60 feature bands The building feature set, and the produced building samples and labels are sent to the LSTM network to obtain the rough extraction results of the buildings, and the final results are obtained after morphological processing.
Owner:JILIN UNIV
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