The application discloses a kind of
carbonate geological sample
carbonate combined state
chlorine extraction test methods, using deionized water to wash
carbonate geological sample to no
chlorine ion, after sample
drying, add
acetic acid solution to dissolve, obtain dissolving solution;Dissolving solution is added in cation exchange resin, and the solution after exchange is collected;10ppm In
internal standard is added in the solution collected after resin exchange, the
chlorine ion content in solution is detected using
inductively coupled plasma mass spectrometry;Dilute dissolving solution using dilute
nitric acid solution, use
inductively coupled plasma optical emission spectrometry to detect the
calcium magnesium content in
dilution solution liquid, calculate carbonate combined state chlorine value, i.e. Cl / Ca value or Cl / (Ca+Mg) value.The application is washed by deionized
water Sample,
acetic acid dissolves sample, ICP-MS, ICP-OES detects solution element content, not only can effectively extract, test carbonate combined state chlorine in carbonate geological sample, avoid the
pollution of non-carbonate mineral chlorine, also have the characteristics that experimental
reagent is easy to obtain, simple operation, detection precision is high.