236results about How to "Thin diameter" patented technology

The invention discloses an air jet assisting multi-needle electrostatic spinning device which comprises a spinneret plate with the air jet assisting function. Multiple metal needles are arranged on the spinneret plate. The head ends of all the metal needles are connected in series through a wire. The wire is connected with the positive electrode of a direct-current high-pressure generator. The tail end of each metal needle is connected with an injector through a liquid guide pipe. The injector is driven through a micro-injection pump. A receiving device is arranged below the spinneret plate and connected with the negative electrode of the direct-current high-pressure generator. By the adoption of the air jet assisting multi-needle electrostatic spinning device, the spinneret plate with the multiple needles serves as a spinning module, on the basis, the air jet assisting function is added to increase the volatilizing speed of a spinning solvent, accelerate jet flow solidification and increase the operation speed, so that the yield of unit time of nanofibers is increased, the fibers are stretched to a certain degree through jet air flow, and the nanofibers with the smaller diameter can be acquired.

The invention discloses a preparation method of a one-way wet conduction nano-fiber multilayer composite membrane with the wettability gradient. The method comprises the following steps that hydrophilic nano materials are dispersed in solvent, the nano materials are dispersed uniformly through ultrasound, a hydrophilic polymer is dissolved in the dispersing agent, a spinning solution A1 is obtained, and a hydrophilic nano-fiber membrane is deposited on a receiving base material through an electrostatic spinning method; hydrophilic nano materials are dispersed in solvent, the nano materials are dispersed uniformly through the ultrasound, a hydrophilic polymer is dissolved in the dispersing agent, and a spinning solution A2 is obtained; a hydrophobic polymer is dissolved in solvent, and a spinning solution B1 is obtained; the two spinning solutions are deposited on the hydrophilic nano-fiber membrane to form at least one diversion layer through the electrostatic spinning method; a hydrophobic polymer is dissolved in solvent, a spinning solution B2 is obtained, a hydrophobic nano-fiber membrane is deposited on the diversion layers through the electrostatic spinning method, and the one-way wet conduction nano-fiber multilayer composite membrane with the wettability gradient is obtained.

The invention relates to a device and a method for manufacturing an airflow melting electrostatic spinning nano-fiber non-woven fabric. The device for manufacturing the airflow melting electrostatic spinning nano-fiber non-woven fabric comprises a stock hoper, a screw extruder, a filter, a metering pump, a material path, a melt-blown die head, a hot-air pipeline, an air compressor, a heating device, a high voltage electrostatic generator and a receiving device. The material path is made of high thermal conductivity insulating ceramics. The method for manufacturing the nano-fiber non-woven fabric adopts the device disclosed by the invention and comprises the following processing steps: (1) preparing a polymer melt; (2) jetting nano-fibers by using airflow static electricity; and (3) moulding the non-woven fabric. The method for manufacturing the nano-fiber non-woven fabric of the invention adopts airflow-melting electrostatic spinning technology, avoids a problem of pollution of electrostatic spinning solvent, and is novel environment-friendly non-woven fabric manufacturing technology. In the manufacturing method, high voltage electrostatic is directly acted on the melt-blown die head; the melt has high and uniform charge; and simultaneously by utilizing drafting of the airflow, the prepared nano-fiber has the advantages of thin diameter and narrow distribution. The device can meet production requirements by improving the conventional melt-blown manufacturing device, and has low implementation cost and easy industrialization promotion.

A curing device comprises a first elliptic cylindrical reflector and a second elliptic cylindrical reflector, the first elliptic cylindrical reflector and the second elliptic cylindrical reflector arranged to have a co-located focus, and a light source located at a second focus of the first elliptic cylindrical reflector, wherein light emitted from the light source is reflected to the co-located focus from the first elliptic cylindrical reflector and retro-reflected to the co-located focus from the second elliptic cylindrical reflector.

The invention discloses dispersion strengthening platinum/rhodium10-platinum thermocouple wires, comprising a cathode and an anode; the thermocouple wires are characterized in that the anode contains ingredients according to the following weight percentage: 9.9-10% of rhodium; 0-0.5% of zirconium; 0-0.5% of yttrium; 0-0.5% of calcium; 0-0.5% of lanthanum; 0-0.5% of titanium; the excess is platinum; the cathode contains ingredients according to the following weight percentage: 0-0.5% of zirconium; 0-0.5% of yttrium; 0-0.5% of calcium; 0-0.5% of lanthanum; 0-0.5% of titanium; the excess is platinum. The production method of dispersion strengthening platinum/rhodium10-platinum thermocouple wires comprises mixing ingredients, vacuum melting, placing and rolling, oxidizing, combined machining and drawing forming. The dispersion strengthening platinum/rhodium10-platinum thermocouple wires of the invention enjoy long service life, high adaptive temperature, strong contamination resistance and low use cost.

An ultrasonic endoscope comprises an insertion portion comprising a distal hard portion which has: an endoscopic observation unit; and an ultrasonic observation unit having ultrasonic transducers arranged circumferentially on an outer circumferential section of the distal hard portion, wherein the ultrasonic observation unit comprises an ultrasonic-wave transmission/reception unit having an tunnel-shaped path which has an inner circumferential surface formed as a backing layer; a distal block is arranged on a distal side in an axial direction of the distal hard portion with respect to a location where the ultrasonic-wave transmission/reception unit is arranged, and distal ends of respective members constituting the endoscopic observation unit are fixed to the distal block; and part of the members which constitute the endoscopic observation unit are fitted so as to be partially protruded from an inside diameter of the tunnel-shaped path toward an outer circumferential side thereof.

The invention discloses a method for manufacturing a vacuum insulation panel core material with high performance and low cost. The method comprises the following steps of: pulping glass fiber cotton which is produced by a centrifuge method; diluting; screening; performing dehydration molding; performing pressure roller sizing; performing vacuum negative pressure dehydration; drying; cooling; and cutting. In the manufacturing method, the glass fiber cotton which is completely produced by the centrifuge method is used as a raw material of the vacuum insulation panel core material with high performance and low cost, the coefficient of thermal conductivity of the produced vacuum insulation panel core is between 0.003 and 0.008 W/m.k, and the coefficient of heat insulation is greatly improved;the thickness of the panel core material is between 0.5 and 30 mm, and the thickness is thinner; and the glass fiber cotton with the diameter of 3.5 to 5 mu m and the length of 5 to 20 mm has low cost and low overall manufacturing cost, and the overall cost of the vacuum insulation panel is lowered.

The invention discloses a manufacturing method for a fibrous membrane of an extremely hydrophobic organic macromolecule chemical compound with an oil-water separation function in the technical field of fibrous membrane manufacturing. The manufacturing method comprises the following steps: synthetizing a copolymer with excellent electrostatic spinnability by regulating the compounding ratio of a monomer and controlling the condition of a suspension polymerization technology and by adjusting and controlling the compositions of a solution, processing parameters and the temperature and humidity conditions of environment, and spinning a copolymer solution into the fibrous membrane with the advantages of uniform and small bore diameters, high porosity, large flux and extremely hydrophobic and oleophylic properties by using an electrostatic spinning technique. The obtained fibrous membrane has the advantages that the specific surface area is large, the patterns are large, the stacking structure is proper, and the fibrous membrane is in a three-dimensional bore channel structure. Compared with an existing polymer-based oil-water separation member, the fibrous membrane has the advantages that the bore channel structure is more reasonable, the separation capacity is stronger, the separation efficiency is higher, the anti-pollution capacity is stronger, the membrane bores are not easy to block, the oil-water selectivity is stronger, the mechanical strength is higher, the flexibility and the temperature resistance are better, the preparation process is shorter, the consumed energy is little, the filtering rate is higher, and the cost is lower, so that the fibrous membrane can better satisfy the requirements of industrial practicality.

The invention relates to a method for preparing an oil absorption material, in particular to a method for preparing a carbon nanofiber aerogel oil absorption material from bacterial cellulose. According to the method, bacterial cellulose aerogel is modified to obtain the carbon nanofiber aerogel oil absorption material. The method comprises the following steps: culturing the bacterial cellulose; preparing the bacterial cellulose aerogel; and preparing the carbon nanofiber aerogel oil absorption material. The method for preparing the carbon nanofiber aerogel from the bacterial cellulose is simple, novel in design, high in environment-friendly biocompatibility and high in absorption efficiency, and the oil absorption material can be recycled for many times. The hydrophobic carbon nanofiber aerogel prepared by the process can widely absorb multiple organic solvents and oil products, and is high in recyclability and selectivity; the absorption rate is up to 50-300 times the self-weight of the hydrophobic carbon nanofiber aerogel.

The invention discloses dispersion strengthening platinum/rhodium13-platinum thermocouple wires, comprising a cathode and an anode; the thermocouple wires are characterized in that the anode contain ingredients according to the following weight percentage: 12.87-13% of rhodium; 0-0.5% of zirconium; 0-0.5% of yttrium; 0-0.5% of calcium; 0-0.5% of lanthanum; 0-0.5% of titanium; the excess is platinum; the cathode contains ingredients according to the following weight percentage: 0-0.5% of zirconium; 0-0.5% of yttrium; 0-0.5% of calcium; 0-0.5% of lanthanum; 0-0.5% of titanium; the allowance platinum. The production method of dispersion strengthening platinum/rhodium13-platinum thermocouple wires comprise mixing ingredients, vacuum melting, placing and rolling, oxidizing, combined machining and drawing forming. The dispersion strengthening platinum/rhodium13-platinum thermocouple wires of the invention enjoy long service life, high adaptive temperature, strong contamination resistance and low use cost.

The invention belongs to the field of preparation of composite materials, and relates to a preparation method of ultrafine fibrous membrane-toughened prepreg of thermoplastic resin with a toughening function. The method comprises the following steps: electrostatically spinning a toughening agent of thermoplastic resin to obtain ultrafine fibers of the thermoplastic resin with diameter of 100-5000nm, and directly spraying the fibers on the surface of a reinforced fiber fabric so as to form a toughening layer consisting of thermoplastic resin fibers which are distributed irregularly and are uniform in surface density on the surface of the fiber fabric; attaching the toughening layer with the fiber fabric to form a whole through a hot rolling process; and then, compounding the fiber fabric product with the toughening function and a prepreg resin base body to prepare the ultrafine fibrous membrane-toughened prepreg product of thermoplastic resin. The preparation method provided by the invention is simple in technical process and easy to implement, and can realize continuous production of high toughness prepreg, thereby greatly improving the production efficiency.

The invention discloses a method for preparing an acetylation-modified bacterial cellulose aerogel oil-absorbent material and relates to a method for preparing an oil-absorbent material. The invention aims to provide a method for preparing an acetylation-modified bacterial cellulose aerogel oil-absorbent material and the novel oil absorbent material is prepared by carrying out acetylation surface modification on the bacterial cellulose aerogel. The preparation method comprises the following steps of firstly culturing the bacterial cellulose; secondly, acetylating the bacterial cellulose microfibrils; and thirdly, preparing the hydrophobic acetylated bacterial cellulose aerogel. The acetylation-modified bacterial cellulose aerogel oil-absorbent material provided by the invention has the advantages of simple preparation method, novel design, environment friendliness, good biocompatibility and reusability and high absorption efficiency. The oil-absorbent material has very high affinity to oil, no absorption capability to water, good phase selectivity, can absorb leaked and spilled oil and organic solvents in water and can be used as an oil-water separation material. The oil-absorbent material is easily biodegradable and causes almost no pollution to the water body.

The invention relates to a preparation method of carbon nanofibers and particularly relates to a preparation method of polyacrylonitrile-based carbon nanofibers. The preparation method comprises the following steps: dissolving polyacrylonitrile into a solvent to form a spinning solution, supplying the spinning solution to a spinning die head with a series of spinning holes, and extruding from the spinning holes to form fine spinning solution flow; blowing and extruding the fine spinning solution flow by utilizing one high-speed jet air flow at an included angle being 0-30 degrees, thus refining the fine solution flow and promoting the evaporation of the solvent to form polyacrylonitrile nanofibers, wherein the temperature of the high-speed jet air flow is 20-80 DEG C, and the speed of the high-speed jet air flow is higher than the extruding speed of the fine solution flow by 500-3000 times; and arranging the polyacrylonitrile nanofibers in air atmosphere being 160-300 DEG C to conduct pre-oxidization treatment and conduct carbonization treatment in the nitrogen atmosphere being 900-1800 DEG C to obtain the carbon nanofibers. The preparation method has the advantages of high production efficiency, simple process, uniform diameter distribution of fibers and the like, and is suitable for large-scale production.

The invention discloses a method for preparing a carbon fiber reinforced thermoplastic composite material, which comprises the following steps: 1)alternatively paving carbon fiber and thermoplastic resin in a die, wherein a bottom layer and a top layer of the die are thermoplastic resin, closing the die and applying pressure; 2)accessing power supply to a carbon fiber layer, rapidly heating under current effect, when the temperature is higher than the melting point of thermoplastic resin, fusing thermoplastic resin, dipping carbon fiber under pressure; and 3)breaking power, cooling the die, and then opening the die to obtain the carbon fiber reinforced thermoplastic composite material. The method takes carbon fiber as a heat-generating body, the electrothermal conversion efficiency can reach as high as more than 90%, and the energy saving effect is obvious; simultaneously, carbon fiber is capable of melting thermoplastic resin and completing dipping, and has the advantages of short moulding time and good dipping effect, formation of good cross section of thermoplastic resin and fiber can be realized, composite material performance is increased, and processing of product with large thickness can be realized in short time.

The invention discloses a test method for bonding strength of chopped ultrafine organic fiber and a cement-based composite interface. The method comprises steps as follows: fiber is bonded on a sample loading cuboid, and a part of the lower end of the fiber is exposed; a mold is prepared, uniformly stirred cement-based materials are poured into the mold and compacted, the surface is flattened, and a cement matrix is obtained; the exposed end of the fiber is perpendicularly inserted into the cement matrix; after the cement matrix is cured to a test age, the sample loading cuboid is removed, and a free end of the fiber is exposed; an instant adhesive is bonded to the free end of the fiber and is congealed to form small balls; the fiber is tested on a monofilament stretching machine, the stretching speed is controlled, the fiber is pulled out of the cement matrix, and a load displacement curve is obtained; the bonding strength of the fiber and the cement-based composite interface is calculated. The exposed length of the fiber is controlled in advance, and the embedded length of the fiber in the cement matrix can be controlled precisely; requirements for the length and the diameter of the fiber are low, and the test method can be used for testing longer and thinner fiber; a tested sample is not required to be cut, and the testing result is more accurate.

A preparation method of an organic-inorganic hybrid super hydrophobic modified bacterial cellulose aerogel oil absorption material relates to a preparation method of an oil absorption material. The invention aims to provide the preparation method of the organic-inorganic hybrid super hydrophobic modified bacterial cellulose aerogel oil absorption material. The bacterial cellulose aerogel is subjected to organic-inorganic hybrid super hydrophobic modification to obtain the super hydrophobic aerogel oil absorption material. The method comprises the steps as follows: 1, bacterial cellulose cultivation; 2, bacterial cellulose aerogel preparation; and 3, preparation of the organic-inorganic hybrid super hydrophobic modified bacterial cellulose aerogel. The oil absorption material prepared by the invention has good selective oil absorption performance, can be conveniently used for oil-water separation or absorption of the oil spill in the water, has no pollution to the water body, and is a novel oil absorption material with great application potential.

The invention provides a sampler for sediment pore water sampling in rivers or lakes. The lower end of a sampling tube is fixedly connected with a conical head, an internal thread port is arranged at the upper end of the sampling tube, and a screen mesh area is arranged at the lower part of the sampling tube. The sampling tube inner the screen mesh area is provided with line cutting seams. The sampling tube outer wall in the screen mesh area is covered with stainless steel screen meshes, and the lower end of a T- shaped handle is plugged in the upper end of the sampling tube. The pore water sampler has a maximum sampling depth of 3.5 m relative to the maximum sampling depth of the common interstitial water sampler of about 80-100 cm, so that comprehensiveness of pore water sampling investigation work of the bottom sediments in the rivers or lakes can be improved. Through use of the sampler, disturbance on the pore water is smaller, undisturbedness of the pore water of the bottom sediments in different depth of the rivers or lakes can be greatly maintained, and the accuracy of the sample analysis of the pore water of the sediments can be improved. The sampler has the advantages of small and exquisite volume, simple operation and adjustable sampling depth.

The invention discloses a preparation method of chalcogenide glass tapered fibers. Chalcogenide glass fibers are tapered by the aid of accurate temperature control of a specific electric-heating coil and traction of a precision stepping motor, important parameters such as taper zone lengths, taper zone outer diameters and the like of the tapered fibers are controlled through control on the heating temperature and the tapering traction speed, and the chalcogenide glass tapered fibers with different taper zone lengths and taper zone outer diameters are drawn accurately. The method is simple in technology, high in operability, good in repeatability and high in accuracy and can effectively solve problems that the chalcogenide glass fibers are broken easily during tapering, fiber core diameters and taper zone lengths are difficult to control accurately and the like, the fiber core diameters of the prepared chalcogenide glass tapered fibers with nanoscale or submicron diameters range from 700 mu m to 1,000 mu m, the taper zone lengths range from 3 cm to 7 cm, the production cycle is short, the success rate is high, the chalcogenide glass tapered fibers can be applied to new technical fields of coupling of micro-waveguides, generation of super-continuum spectrum and the like, and research and application fields of the chalcogenide glass tapered fibers are greatly extended.