The invention relates to a
titanate precursor
sol spinning solution, a Ti < 3 + > self-doped
titanate fiber photocatalyst and a preparation method and application of the Ti < 3 + > self-doped
titanate fiber photocatalyst. According to the preparation method, PAT or PET is taken as a
titanium source,
metal acetate is taken as a
metal source, low-carbon
alcohol and organic
carboxylic acid are taken as solvents, and the titanate
fiber photocatalyst or the Ti < 3 + > self-doped titanate fiber photocatalyst is successfully prepared through a
sol-gel combined electrostatic
spinning technology. The organic
carboxylic acid is introduced to be used as one of solvents to dissolve acetate, and is also used as a ligand to coordinate with
metal ions, so that the organic
carboxylic acid has certain spinnability, meanwhile, a
titanium precursor is protected from being hydrolyzed, and the spinnability and the stability of the obtained
spinning solution are both excellent. The method disclosed by the invention is simple in process, is
safer, more environment-friendly and more reliable compared with a method for preparing the Ti < 3 + > self-doped titanate fiber photocatalyst by using strong
reducing substances such as H2 and NaBH4, and shows good catalytic performance.