1610results about "Tin oxides" patented technology

A process for the production of ultrafine powders that includes subjecting a mixture of precursor metal compound and a non-reactant diluent phase to mechanical milling whereby the process of mechanical activation reduces the microstructure of the mixture to the form of nano-sized grains of the metal compound uniformly dispersed in the diluent phase. The process also includes heat treating the mixture of nano-sized grains of the metal compound uniformly dispersed in the diluent phase to convert the nano-sized grains of the metal compound into a metal oxide phase. The process further includes removing the diluent phase such that the nano-sized grains of the metal oxide phase are left behind in the form of an ultrafine powder.

A nanocomposite structure comprising a nanostructured filler or carrier intimately mixed with a matrix, and methods of making such a structure. The nanostructured filler has a domain size sufficiently small to alter an electrical, magnetic, optical, electrochemical, chemical, thermal, biomedical, or tribological property of either filler or composite by at least 20%.

Non-hydroxyalkylated cyclodextrins are disclosed wherein at least one primary alcohol function (CH2OH) is substituted, the -OH portion being replaced by a substituent with formula -O-CO-R or -NR1R2, where:R, R1 and R2 independently represent a linear or cyclic, saturated or unsaturated, hydroxylated or non-hydroxylated alkyl group containing 1 to 30 carbon atoms, preferably 1 to 22 carbon atoms, more preferably a fatty chain containing 2 to 22 carbon atoms. These cyclodextrins are used as vectors for at least one active ingredient, in particular to encourage tissue penetration, in a cosmetic application, or for the production of pharmaceutical compositions, in particular dermopharmaceuticals.

Doped, pyrogenically prepared oxides of metals and / or non-metals which are doped with one or more doping components in an amount of 0.00001 to 20 wt. %. The doping component may be a metal and / or non-metal or an oxide and / or a salt of a metal and / or a non-metal. The BET surface area of the doped oxide may be between 5 and 600 m2 / g. The doped pyrogenically prepared oxides of metals and / or non-metals are prepared by adding an aerosol which contains an aqueous solution of a metal and / or non-metal to the gas mixture during the flame hydrolysis of vaporizable compounds of metals and / or non-metals.

Provided is a simple, fast, scalable, and environmentally benign method of producing graphene-embraced or encapsulated particles of a battery electrode active material directly from a graphitic material, the method comprising: a) mixing graphitic material particles and multiple particles of a solid electrode active material to form a mixture in an impacting chamber of an energy impacting apparatus, wherein the graphitic material has never been intercalated, oxidized, or exfoliated and the chamber contains therein no previously produced graphene sheets and no ball-milling media; b) operating the energy impacting apparatus with a frequency and an intensity for a length of time sufficient for transferring graphene sheets from the graphitic material to surfaces of electrode active material particles to produce graphene-embraced electrode active material particles; and c) recovering the particles from the impacting chamber. Also provided is a mass of the graphene-embraced particles, electrode containing such particles, and battery containing this electrode.

Provided here is a method of producing a monolithic body from a porous matrix, comprising: (i) providing a porous matrix having interstitial spaces and comprising at least a first reactant; (ii) contacting the porous matrix with an infiltrating medium that carries at least a second reactant; (iii) allowing the infiltrating medium to infiltrate at least a portion of the interstitial spaces of the porous matrix under conditions that promote a reaction between the at least first reactant and the at least second reactant to provide at least a first product; and (iv) allowing the at least first product to form and fill at least a portion of the interstitial spaces of the porous matrix, thereby producing a monolithic body, wherein the monolithic body does not comprise barium titanate.

The present invention relates to nano structures of metal oxides having a nanostructured shell (or wall), and an internal space or void. Nanostructures may be nanoparticles, nanorod / belts / arrays, nanotubes, nanodisks, nanoboxes, hollow nanospheres, and mesoporous structures, among other nanostructures. The nanostructures are composed of polycrystalline metal oxides such as SnO2. The nanostructures may have concentric walls which surround the internal space of cavity. There may be two or more concentric shells or walls. The internal space may contain a core such ferric oxides or other materials which have functional properties. The invention also provides for a novel, inexpensive, high-yield method for mass production of hollow metal oxide nanostructures. The method may be template free or contain a template such as silica. The nanostructures prepared by the methods of the invention provide for improved cycling performance when tested using rechargeable lithium-ion batteries.

The present invention provides a topical composition for application to the perianal and / or labial areas of the skin which helps prevent viscoelastic fluids, such as menses and feces, from attaching to the skin and aids in the reducing the viscoelastic properties of the fluid so that the fluid can flow into absorbent articles. The composition contains at least one viscoelastant material and at least one an anti-adherent material. the composition may be applied with a wipe, including mitts and gloves, a solid stick composition, an aerosol dispenser, a pump spray, a trigger spray, a squeeze bottle, as a foam, as a cream, as an ointment, as a salve, as a gel, as a wash or as a lotion. In addition, absorbent articles, such as pads or pants, diapers and the like may also be used as a means to transfer the composition to the skin.

Mesoscopically ordered, hydrothermally stable metal oxide-block copolymer composite or mesoporous materials are described herein that are formed by using amphiphilic block polymers which act as structure directing agents for the metal oxide in a self-assembling system.

A process of treating metal oxide nanoparticles that includes mixing metal oxide nanoparticles, a solvent, and a surface treatment agent that is preferably a silane or siloxane is described. The treated metal oxide nanoparticles are rendered hydrophobic by the surface treatment agent being surface attached thereto, and are preferably dispersed in a hydrophobic aromatic polymer binder of a charge transport layer of a photoreceptor, whereby π—π interactions can be formed between the organic moieties on the surface of the nanoparticles and the aromatic components of the binder polymer to achieve a stable dispersion of the nanoparticles in the polymer that is substantially free of large sized agglomerations.

The invention discloses nano / micron binary structured powders for superhydrophobic, self-cleaning applications. The powders are featured by micron-scale diameter and nano-scale surface roughness. In one embodiment, the average diameter is about 1-25 μm, and the average roughness Ra is about 3-100 nm. The nano / micron binary structured powders may be made of silica, metal oxide, or combinations thereof.

A general, reproducible, and simple synthetic method that employs readily available chemicals permits control of the size, shape, and size distribution of metal oxide nanocrystals. The synthesis entails reacting a metal fatty acid salt, the corresponding fatty acid, and a hydrocarbon solvent, with the reaction product being pyrolyzed to the metal oxide. Nearly monodisperse oxide nanocrystals of Fe3O4, Cr2O3, MnO, Co3O4, NiO, ZnO, SnO2, and In2O3, in a large size range (3-50 nm), are described. Size and shape control of the nanocrystals is achieved by varying the reactivity and concentration of the precursors.

An electrode material for an anode of a rechargeable lithium battery, containing a particulate comprising an amorphous Sn.A.X alloy with a substantially non-stoichiometric ratio composition. For said formula Sn.A.X, A indicates at least one kind of an element selected from a group consisting of transition metal elements, X indicates at least one kind of an element selected from a group consisting of O, F, N, Mg, Ba, Sr, Ca, La, Ce, Si, Ge, C, P, B, Pb, Bi, Sb, Al, Ga, In, Tl, Zn, Be, Pr, Nd, Sm, Eu, Gd, Tb, Dy, Ho, Er, Tm, Yb, Lu, As, Se, Te, Li and S, where the element X is not always necessary to be contained. The content of the constituent element Sn of the amorphous Sn.A.X alloy is Sn / (Sn+A+X)=20 to 80 atomic %. An electrode structural body for a rechargeable lithium battery, comprising said electrode material for an anode and a collector comprising a material incapable of being alloyed with lithium in electrochemical reaction, and a rechargeable lithium battery having an anode comprising said electrode structural body.

Polycrystalline materials of macroscopic size exhibiting Single-Crystal-Like properties are formed from a plurality of Single-Crystal Particles, having Self-Aligning morphologies and optionally ling morphology, bonded together and aligned along at least one, and up to three, crystallographic directions.

The present invention includes a method of producing a crystalline metal oxide nanostructure. The method comprises providing a metal salt solution and providing a basic solution; placing a porous membrane between the metal salt solution and the basic solution, wherein metal cations of the metal salt solution and hydroxide ions of the basic solution react, thereby producing a crystalline metal oxide nanostructure.

The invention relates to a method for preparing nano-doped tin oxide sol, belonging to the technical field of semiconductor nano film preparation process. The method provided by the invention mainly uses a sol-gel method to prepare nano-doped SnO2 sol on compatible reaction condition via hydrothermal processing. In the method, tin salt is taken as main raw material, villaumite and antimony salt or two parts of antimony or two parts of villaumite in appropriate content are added as doping agent to obtain doped SnO2 sol. High temperature calcination is unnecessary in the synthesized process, and nano-doped SnO2 sol can be obtained with even grains and fine dispersivity. Spray finishing, spin coating, and dipping and drawing method can be carried out on the obtained sol to prepare nano-doped SnO2 film. The film can be applied into various fields, such as low emissivity glass, display equipment, gas sensor, transparency electrode of solar battery and the like.

Methods are described that have the capability of producing submicron / nanoscale particles, in some embodiments dispersible, at high production rates. In some embodiments, the methods result in the production of particles with an average diameter less than about 75 nanometers that are produced at a rate of at least about 35 grams per hour. In other embodiments, the particles are highly uniform. These methods can be used to form particle collections and / or powder coatings. Powder coatings and corresponding methods are described based on the deposition of highly uniform submicron / nanoscale particles.

The invention relates to platinum-metal oxide composite particles and their use as electrocatalysts in oxygen-reducing cathodes and fuel cells. The invention particularly relates to methods for preventing the oxidation of the platinum electrocatalyst in the cathodes of fuel cells by use of these platinum-metal oxide composite particles. The invention additionally relates to methods for producing electrical energy by supplying such a fuel cell with an oxidant, such as oxygen, and a fuel source, such as hydrogen. The invention also relates to methods of making the metal-metal oxide composites.

A method for producing fine particles of metal oxide characterized in that metal halide is hydrolyzed in the presence of organic solvent. According to this invention, under hydrolysis of titanium tetrachrolide, anatase type titanium oxide can be obtained by selecting hydrophilic organic solvent, and rutile type titanium oxide can be obtained by selecting hydrophobic organic solvent.

Nanoparticles comprising titanium, such as nanoscale doped titanium metal compounds, inorganic titanium compounds, and organic titanium compounds, their methods of manufacture, and methods of preparation of products from nanoparticles comprising titanium are provided.

A general, reproducible, and simple synthetic method that employs readily available chemicals permits control of the size, shape, and size distribution of metal oxide nanocrystals. The synthesis entails reacting a metal fatty acid salt, the corresponding fatty acid, and a hydrocarbon solvent, with the reaction product being pyrolyzed to the metal oxide. Nearly monodisperse oxide nanocrystals of Fe3O4, Cr2O3, MnO, Co3O4, NiO, ZnO, SnO2, and In2O3, in a large size range (3-50 nm), are described. Size and shape control of the nanocrystals is achieved by varying the reactivity and concentration of the precursors.

Nanoparticles comprising titanium, such as nanoscale doped titanium metal compounds, inorganic titanium compounds, and organic titanium compounds, their methods of manufacture, and methods of preparation of products from nanoparticles comprising titanium are provided.

A low-temperature hydrothermal reaction is provided to generate crystalline perovskite nanotubes such as barium titanate (BaTiO3) and strontium titanate (SrTiO3) that have an outer diameter from about 1 nm to about 500 nm and a length from about 10 nm to about 10 micron. The low-temperature hydrothermal reaction includes the use of a metal oxide nanotube structural template, i.e., precursor. These titanate nanotubes have been characterized by means of X-ray diffraction and transmission electron microscopy, coupled with energy dispersive X-ray analysis and selected area electron diffraction (SAED).

The invention discloses a preparation method of a nitrogen doped graphene / metal oxide nanometer composite material. The preparation method comprises the following steps of: weighing graphene and metal salt the cation of which is trivalent or quadrivalent to be added in a dispersant, and then carrying out ultrasonic dispersion to obtain mixed liquor; (2), reacting the mixed liquor obtained in the step (1) with alkaline air on a gas-liquid interface for 3-12hours at the temperature of 60-200 DEG C, cooling, centrifuging, washing a precipitate and drying to obtain powder; and (3) introducing the alkaline air or a mixed gas of the alkaline air and inert gas, maintaining the powder to be at the constant temperature of 600-900 DEG C for 2-6 hours, and cooling to room temperature to obtain the nitrogen doped graphene / metal oxide nanometer composite material. According to the invention, the conductibility and interface action of the composite material obtained by the method provided by the invention are improved due to the doping of nitrogen; and the method provided by the invention has the advantages of simple process, cheap cost, high productive rate, short cycle and the like, and is environment-friendly, and can be suitable for industrialization large-scale production.

The invention discloses a preparation method of a super nanostructure material formed by quantum dots self-assembly. That the alcohols are used as solvent to prepare nano-metal oxides and sulphides or metal oxides and sulphides are reduced to get nano-metal is a widely used method. The super nanostructure material formed by the quantum dots self-assembly draws much attention because of the superior comprehensive properties. The application prospect is wide enough. The invention adopts a method of using the alcohols as the solvent that a super nanostructure with different appearances and is formed by the quantum dots self-assembly which is obtained by changing the condition under the existence condition of surfactant. According to the invention, precursor, namely organic metal compound is dissolved in the alcohol solvent by ultrasonic, stirring and being laid down quietly. Under the effect of the surfactant, the precursor has a nucleation and grows into a plurality of quantum dots, the size of which is similar to nano. Then the dots form a super nanostructure which has a certain shape or space structure along the defined growing direction of the surfactant.

The present invention is directed to producing nano-structured particles that have high specific surface-areas and high thermal stability. By aging nanoparticle precursors, and processing them under appropriate conditions, one is able to generate nano-structured particles that may be used in catalysts. By adding a stabilizing agent one is able to further improve the high thermal stability. These nano-structured particle products are particularly advantageous in applications as catalysts or catalyst supports that operate at high temperatures.

Disclosed are a method for fabricating nanopowders, nano ink containing the nanopowders and micro rods, and nanopowders containing nanoparticles, nano clusters or mixture thereof, milled from nano fiber composed of at least one kind of nanoparticles selected from a group consisting of metal, nonmetal, metal oxide, metal compound, nonmetal compound and composite metal oxide, nano ink containing the nanopowders and microrods, the method comprising spinning a spinning solution containing at least one kind of precursor capable of composing at least one kind selected from a group consisting of metal, nonmetal, metal oxide, metal compound, nonmetal compound and composite metal oxide, crystallizing or amorphizing the spun precursor to produce nano fiber containing at least one kind of nanoparticles selected from a group consisting of metal, nonmetal, metal oxide, metal compound, nonmetal compound and composite metal oxide, and milling the nano fiber to fabricate nanopowders containing nanoparticles, nano clusters or mixture thereof.

A method of preparing metal chalcogenides from elemental metal or metal compounds has the following steps: providing at least one elemental metal or metal compound; providing at least one element from periodic table groups 13-15; providing at least one chalcogen; and combining and heating the chalcogen, the group 13-15 element and the metal at sufficient time and temperature to form a metal chalcogenide. A method of functionalizing the surface of semiconducting nanoparticles has the following steps: providing at least one metad compound; providing one chalcogenide having a cation selected from the group 13-15 (B, Al, Ga, In, Si, Ge, Sn, Pb, P, As, Sb and Bi); dissolving the chalcogenide in a first solution; dissolving the metal compound in a second solution; providing and dissolving a functional capping agent in at least one of the solutions of the metal compounds and chalcogenide; combining all solutions; and maintaining the combined solution at a proper temperature for an appropriate time.