The invention relates to the technical field of
electrode materials, in particular to a three-dimensional
nanostructure NiCo2S4
electrode material and a preparation method and application thereof. The preparation method of the
electrode material comprises the following steps: S1, dissolving a
cobalt source and a
nickel source in deionized water to obtain a
metal salt solution; s2, adding
ammonium hydroxide, a surfactant CTAB (cetyltrimethyl
ammonium bromide) and an organic
sulfur source into the
metal salt solution, and uniformly mixing; and S3, carrying out a
hydrothermal reaction, and carrying out
solid-liquid separation, washing and
drying to obtain the NiCo2S4
electrode material with the three-dimensional
nanostructure. According to the preparation method disclosed by the invention, the three-dimensional
nanostructure NiCo2S4 material which is formed by ultrathin nanosheets and has a high specific surface area is synthesized through a one-step hydrothermal method by utilizing a synergistic effect of
ammonium hydroxide, an organic
sulfur source and a surfactant CTAB (Cetyltrimethyl
Ammonium Bromide); when the material is used as an
electrode material, the electrochemical performance of a battery or a
supercapacitor can be remarkably improved; and the preparation process is simple and efficient.