The invention discloses a
graphite sagger preparation method based on a secondary isostatic pressing process. According to the method, natural crystalline
flake graphite and artificial
graphite powder are selected as raw materials,
coal pitch is selected as a binder, and
boron carbide micro
powder is selected as a filler. The preparation method comprises the following steps: dry-mixing a
graphite raw material, preparing crushed and molten
coal pitch and
boron carbide into a suspension, and mixing and kneading the
coal pitch and the
boron carbide into paste; the paste is pre-pressed into a biscuit through a hydraulic
machine, the biscuit is sealed in a rubber sheath and then subjected to primary cold isostatic pressing, then primary
roasting is carried out, the blank is subjected to vacuum impregnation in a suspension liquid after primary
roasting, secondary cold isostatic pressing and secondary
roasting treatment are carried out after impregnation is completed, graphitization treatment and
cutting shaping are sequentially carried out after roasting, and the finished graphite
saggar is obtained. The degree of dependence on equipment is effectively reduced through a secondary isostatic pressing process, so that the prepared graphite
saggar has good performance, and the density, bending strength,
porosity,
thermal shock performance and other indexes of the graphite
saggar all meet the specialized operation requirements in the fields of
photovoltaics,
new energy and the like.