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83results about How to "Reduce hydrolysis rate" patented technology

Method for preparing hydrogen fluoride and coproducing white carbon black with silicon tetrafluoride

The invention discloses a method for preparing hydrogen fluoride and coproducing white carbon black with silicon tetrafluoride, comprising the following steps: letting crude silicon tetrafluoride as byproduct from a phosphate fertilizer be subject to dedusting and dehumidification, then reacting with steam with the reacting dose for hydrolysis at the temperature of 200-800 DEG C, carrying out gas-solid separation on the obtained products to respectively obtain hydrogen fluoride and white carbon black. According to the invention, the low grade silicon tetrafluoride as byproduct of fluorine resources is used for preparing high purity absolute hydrogen fluoride and coproducing gas phase white carbon black, thus a novel method for producing gas phase white carbon black is developed, a novel technology of preparing gas phase white carbon black at low temperature is realized, the energy consumption in the preparation is reduced, the raw material is easily available, the price is low, the utilization rate of the raw material is low, and a cost advantage is achieved compared with traditional production method of absolute hydrogen fluoride. The invention can create good economical benefits, and bring huge environmental benefits and social benefits, belonging to a clean production process.
Owner:DUOFUDUO KUNMING TECH DEV CO LTD

Method for synthesizing polyepoxysuecinic acid salt

The invention discloses a method for synthesizing a polyepoxysuecinic acid salt, which is characterized by comprising the following steps of: dissolving maleic anhydride in deionized water; adding a solution of sodium hydroxide at 30 to 60 DEG C with stirring; adding sodium tungstate and hydrogen peroxide when the temperature is controlled to be between 60 to 100 DEG C; adjusting the pH value to 5 to 7 for reaction for 2 to 100 hours; cooling the reaction solution to below 20 DEG C; adding a precipitator, mixing and stirring the precipitator and the solution; performing suction filtration, adding water into filtrate obtained after suction filtration; keeping the pH value between 6 and 7; heating the filtrate added with water to 70 to 100 DEG C to obtain an epoxysuecinic acid salt; preparing a 0.2 to 4.0 mol/L aqueous solution of the epoxysuecinic acid salt; adding calcium hydroxide and a polymerization promoter into the aqueous solution for performing polymerization reaction till liquid turns yellowish and pasty; and cooling the yellowish and pasty liquid to room temperature to obtain the polyepoxysuccinic acid salt. The method has the advantages of good product quality, low raw material cost and product scale inhibition performance advantageous over that of the prior art.
Owner:北京合创同盛科技有限公司

Preparation method of antibacterial veterinary drug sulfamonomethoxine sodium

InactiveCN106565616AEliminate large-scale water removal operationsImprove reaction efficiencyOrganic chemistrySulfonyl chlorideSulfamonomethoxine
The invention relates to preparation of a veterinary drug, namely, sulfamonomethoxine sodium used for treating animal diseases caused by sensitive bacteria. An anhydrous lewis acid catalyst, namely, anhydrous calcium chloride is introduced into a condensation reaction step, and 4-methoxy group-2-aminopyrimidine serves as a reaction raw material; in organic alkaline solvent, the 4-methoxy group-2-aminopyrimidine and the catalyst are added in the first place, and then p-acetamidobenzene sulfonyl chloride is added in batches; the effect that moisture in a reaction system is controlled to be always in a low level can be achieved, and meanwhile a reaction substrate can also be effectively activated, so that an intermediate product with the purity being more than 98% can be obtained in short time at a high temperature through a condensation reaction, and the yield can reach more than 95%; and then after hydrolysis, decoloration and crystallization operation in specific mixed crystallization solvent, a target product, namely, the sulfamonomethoxine sodium with the purity reaching more than 99% can be obtained, and the situation of requirements for animal antibacterial veterinary drugs in the prior art is relieved.
Owner:杭州洪晟生物技术股份有限公司

A kind of self-emulsifying water-based alkyd resin and self-emulsifying water-based alkyd paint and preparation method

The invention discloses self-emulsifying waterborne alkyd resin as well as self-emulsifying waterborne alkyd paint and a preparation method of the self-emulsifying waterborne alkyd paint. The self-emulsifying waterborne alkyd resin has a solid content of 80 plus or minus 1%, and is the self-emulsifying waterborne alkyd resin with a transparent appearance; the self-emulsifying waterborne alkyd paint is prepared by taking the self-emulsifying waterborne alkyd resin as a matrix, and mixing and stirring the self-emulsifying waterborne alkyd resin with a pigment, a drier, a neutralizer, deionized water, a defoaming agent, a substrate wetting agent, a dispersing agent and a thickener; the non-volatile matter content of the self-emulsifying waterborne alkyd paint is 45-55, the hardness is 0.3-0.5, and the VOC content is below 100g / L; the preparation method mainly comprises the following steps: a) preparation of pigment slurry, b) a mixing stage; the self-emulsifying waterborne alkyd paint iscapable of achieving or approaching the performance of solvent-based paint, and mainly used in building enamels, primers of wooden products, anti-corrosive primers, agricultural machinery, construction machinery, trains, trolleybuses, buses and steel strength beam coating systems.
Owner:浙江大桥油漆有限公司
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