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39results about How to "Wide range of process parameters" patented technology

Method for continuously preparing regenerated cellulose fibre

The invention discloses a method for continuously preparing regenerated cellulose fibers through the solvent method, comprising the following steps that: a cellulose raw material is dissolved into an ion liquid to prepare a spinning liquid; gel type regenerated cellulose fibers are obtained through spinning; and the regenerated cellulose fibers are obtained through cleaning, rear draft and drying, wherein, the ion liquid is selected from one or a plurality among the following ion liquids: a). an ion liquid with 1, 3-dialkyl imidazole as a cation and formiate radical, radical vinegar or propionate radical as an anion; and b). an ion liquid with 1-R1-3-R2- dialkyl imidazole as the cation and chlorine, bromine, iodine, formiate radical, radical vinegar, sulfate radical, nitrate radical, tetrafluoroborate radical, thiocyanate radical, hexafluorophosphate radical, p-toluenesulfonate radical or trifluoromethanesulfonic acid radical as the anion. The method has the advantages of wide technological range, mild temperature condition, adequate pressure, quick spinning speed and so on, can prepare the regenerated cellulose fibers with superior performance and complete specifications, and has low production cost, high production efficiency and wide application prospect.
Owner:INST OF CHEM CHINESE ACAD OF SCI +1

Method for deep penetration laser welding of plate under assistance of ultrasound

The invention relates to a method for deep penetration laser welding of a plate under the assistance of ultrasound. The method is characterized by comprising the following steps that firstly, first base metal (10) and second base metal (11) are machined to form butt joint end faces, and a series of inclined semicircular grooves are machined; secondly, the first base metal (10) and the second base metal (11) are in butt joint and are clamped, and a series of inclined blind holes are formed in a weld bead; thirdly, a first ultrasonic amplitude-changing rod (3) is pressed to the upper surface of a workpiece to be welded; fourthly, a second ultrasonic amplitude-changing rod (4) is fixed to one side of a laser welding head; fifthly, an ultrasonic generation device is started, the ultrasonic frequency is adjusted; sixthly, a laser beam (5) perpendicularly irradiates the upper surface of the workpiece, and the welding process is completed under continuous ultrasonic vibration; and seventhly, after welding is completed, ultrasonic vibration is maintained for 1-2 minutes. In the method, due to the pre-formed inclined blind holes and ultrasonic vibration, weld joint root leakage caused by molten pool downward flowing driven by local evaporation back flushing pressure of the front edge walls of the small holes is avoided.
Owner:CHANGSHA UNIVERSITY OF SCIENCE AND TECHNOLOGY

Welding method for obtaining amorphous connector for FeSiB amorphous strip

The invention relates to the technical field of amorphous materials and welding, in particular to a welding method for obtaining an amorphous connector for a FeSiB amorphous strip and belongs to the technology of amorphous material connection. The method is used for solving the problems that the size of a Fe-based amorphous alloy strip is limited, materials are crisp and extremely thin, and weldability is poor. The completely amorphous connector is obtained successfully through a micropulse laser technology. The welding method includes the steps that the surface of a FeSiB amorphous alloy strip sample is ground, cleaned and blown to be dried; a self-designed special clamp is clamped at one end, the other end of the special clamp is used for fixing base metal in a flattening manner, and gas Ar is laterally blown to protect a weld pool; and the micropulse laser technology is used for conducting lap joint welding, technological parameters such as the pulse power P, the pulse width T, the pulse frequency F and the like are optimized, and the completely amorphous connector is obtained. The welding method has the advantages that a welding tool is simple, welding efficiency is high, cost is low, connector quality is good, and the connector has the completely amorphous characteristic.
Owner:NANCHANG HANGKONG UNIVERSITY

Current-assisted laser brazing method or laser fusion brazing method

The invention relates to a current-assisted laser brazing method or laser fusion brazing method, and belongs to the field of welding. The invention aims to solve the problems of poor moistening and spreading capabilities of brazing materials, and space nonuniformity and low energy utilization efficiency of interface reaction in the traditional laser brazing and laser fusion brazing. In the welding process, two mother metals are connected to one output end of an auxiliary current power supply, the other output end of the auxiliary power supply is connected with a welding wire or a non-fusion electrode through a welding controller, a laser beam is vertically incident to a welding seam, and the welding wire or the non-fusion electrode is added along the front or back side of the welding direction of the laser beam. The method comprises the following steps of: 1. pretreating two mother metals to be welded; 2. fixing the two mother metals to be welded on a worktable, connecting the auxiliary current power supply to the two mother metals; 3. putting the welding wire or the non-fusion electrode at the front or rear side of the welding direction of the laser beam; 4. and starting the laser welding, switching on the auxiliary current power supply, and coordinating and controlling the matching relation between the laser beam and the auxiliary current so as to implement welding.
Owner:HARBIN INST OF TECH

Double-pulse cyanide-free alkali silver electroplating method

The invention discloses components of double-pulse cyanide-free alkali silver electroplating solution and a process. Silver nitrate is used as a main salt, sodium thiosulfate and ammonium thiosulfate are used as complexing agents, sodium metabisulfite is used as an auxiliary complexing agent, sodium sulfate is used as a conductive salt, boric acid is used as a pH value adjustor, and gelatin is added into the plating solution. The operation conditions comprise that the pH value of the plating solution is 4.0 to 4.5, the temperature of the plating solution is 20 to 30 DEG C, and the mechanical stirring speed is 100 to 150rpm. A silver plating layer with fine and compact crystallization can be obtained by adopting double-pulse electroplating, controlling the duty ratio, average current density and working time of the positive and negative pulses and electroplating on pure copper or copper alloy without silver immersion plating pretreatment. The plating solution of the invention has the advantages of simple formulation, easy control, strong even plating and covering capabilities, and high batch production stability. The plating layer has fine and compact crystallization and good appearance luster, and has no peeling, shedding and stripping; and the technology can replace a cyanide silver electroplating process, and can be used as a surface electroplating process for jewelries, artware and parts of electronic products.
Owner:KUNMING UNIV OF SCI & TECH

Injection mold capable of realizing local delayed ejection

PendingCN111152424ASolve the problem of top block printingSolve the long-term problem of top block printing in injection molding productionEngineeringMechanical engineering
The invention provides an injection mold capable of realizing local delayed ejection, and is used for solving the problem that in the prior art, ejection block marks are generated when the mold is used for forming. The injection mold capable of realizing the local delayed ejection comprises a movable mold, a fixed mold, a first straight ejector rod and a first straight ejector block, wherein a forming inner cavity is formed between the movable mold and the fixed mold, the movable mold comprises a driving plate, the first straight ejector rod is arranged in the movable mold, the driving plate can push the first straight ejector rod in the mold closing direction, the first straight ejector block is installed at the end, close to the forming inner cavity, of the first straight ejector rod, afirst elastic piece is arranged at the end, away from the forming inner cavity, of the first straight ejector rod, the first elastic piece is installed at the end, away from the forming inner cavity,of the first straight ejector rod, the first elastic piece is used for tensioning the first straight ejector rod in the movable mold side direction, and in an initial state of the driving plate, a first initial interval is formed between the first straight ejector rod and the driving plate. The injection mold capable of realizing the local delayed ejection can avoid generation of the ejection block marks.
Owner:CHONGQING PINGWEI AUTO PARTS CO LTD

Method for extracting crude salamander oil from giant salamander tail fat by using papain

The invention provides a method for extracting crude salamander oil from giant salamander tail fat by using papain. The method comprises the following steps: separating tail subcutaneous fat from the skin of a giant salamander to obtain the giant salamander tail fat, then stirring the giant salamander tail fat into paste, blending the giant salamander tail fat and water at the ratio of 1:0.5-1:2.0, regulating the pH value of a material liquid to 6.0-7.0, adding the papain of which the weight is 0.1-0.5% of that of the giant salamander tail fat, shaking well, heating to 40-60 DEG C, stirring and shocking for reaction for 0.5-2.0h, centrifuging the obtained enzymatic hydrolysate for 5-15min by a centrifugal machine at 4000-5000r / min, acquiring three layers of the mixture after centrifuging, and absorbing the upper layer to obtain the crude salamander oil. According to the method provided by the invention, the constraint of protein on the fat is removed, meanwhile, the protein formed by combining emulsion and the fat in the process of enzymolysis is also degraded, and the reaction condition is mild, so that effective ingredients in the salamander oil are enabled to be stable. The reaction operation is simple, the extraction ratio of the crude salamander oil and the additional valve of the product are increased, the cost is low, and the method is environment-friendly and can be widely applied to industrial production.
Owner:张家界金鲵生物产品开发有限公司

Discontinuous point type blank holder for fine blanking die and design method of technological parameters of discontinuous point type blank holder

The invention discloses a discontinuous point type blank holder for a fine blanking die and a design method of technological parameters of the discontinuous point type blank holder. The blank holder comprises a point type blank holder body, wherein a group of raised points are uniformly distributed on the lower surface of the point type blank holder body along the shape contour of a part required to be formed through fine blanking; rounded corners are arranged on the raised points; when the thickness of the part required to be formed through fine blanking is smaller than 5 mm, the point type blank holder is single-sided, and the technological parameters are determined; and when the thickness of the part required to be formed through fine blanking is larger than or equal to 5 mm, a group of raised points which have the same parameters with the raised points on the point type blank holder body are arranged on the upper surface of the fine blanking die, and the technological parameters are determined. According to the design method, aimed at fine blanking parts with different thicknesses, the technological parameters of the discontinuous point type blank holder can be effectively determined, the discontinuous point type blank holder can be widely applied to fine blanking, the cost of the fine blanking die is reduced, and the perfectness ratio of the surfaces of the parts is increased.
Owner:WUHAN UNIV OF TECH

Semi-bright lead-free chemical tinning liquid and using method thereof

InactiveCN101717929BEnables continuous autocatalytic depositionFast depositionLiquid/solution decomposition chemical coatingThioureaBenzaldehyde
The invention discloses new semi-bright lead-free chemical tinning liquid and a using method thereof. A semi-bright silver tin-copper alloy chemical plating layer is obtained on copper and copper alloy matrix. In the chemical plating liquid, tin sulfate is used as a main salt, thiourea is used as a main complexing agent, citric acid is used as an auxiliary complexing agent, sodium hypophosphite is used as a reducing agent, ethylene diamine tetraacetic acid is used as an antioxidant, sulfuric acid is used as a stabilizing agent, gelatin is used as a leveling agent, and benzaldehyde is used as an auxiliary brightening agent. The pH value of the plating liquid is 0.8 to 2.0, the temperature of the plating liquid is between 80 and 90 DEG C, the carrying capacity of the plating liquid is 0.8 to 1.5dm2 / L, and the mechanical stirring speed is 50 to 100 rpm. The continuous self-catalytic deposition of tin is implemented on the copper and copper alloy matrix, plating layers of different thicknesses can be obtained by controlling the chemical plating time, and the deposition speed is high; crystalline grains are obviously refined, the surface flatness of the plating layer is improved, and the plating surface area is large; the plating layer and the matrix are combined firmly; and after passivating treatment, the change resistance of the plating layer is high. The technology has broad application prospect in products such as deep hole pieces, blind hole pieces, small-sized electronic parts and components which are difficult to process, printed circuit boards (PCB) and the like.
Owner:KUNMING UNIV OF SCI & TECH

Slantwise type self-tidying integrated equipment with functions of handle cutting, handle releasing and cutting off

The invention provides slantwise type self-tidying integrated equipment with functions of handle cutting, handle releasing and cutting off, comprising an accessory material charging part and a handle-cutting, handle-releasing and cutting-off part, wherein the accessory material charging part comprises an accessory material charging belt which is slantwise arranged and a base support belt which is perpendicular to the accessory material charging belt, vertical plates which are perpendicular to the accessory material charging belt are evenly arranged on the accessory material charging belt, the handle-cutting, handle-releasing and cutting-off part comprises a handle-cutting and handle-releasing machine, a cutting-off machine and supports of the handle-cutting and handle-releasing machine and the cutting-off machine, the sliding pair connection is formed between the lower part of the handle-cutting and handle-releasing machine and the support through a slide groove and a slide rail, the sliding pair connection is formed between the lower part of the cutting-off machine and the support through the slide groove and the slide rail, support belts of the handle-cutting and handle-releasing machine and the cutting-off machine and the accessory material charging belt are arranged on the same slantwise plane, and driving mechanisms matched with the sliding pairs are arranged between the lower parts of the handle-cutting and handle-releasing machine and the cutting-off machine and the supports. The accessory material charging part of the equipment is slantwise arranged, so that the self-tidying can be realized, the manual investment can be reduced, and the work efficiency and quality can be improved.
Owner:BAOFENG REDRYING FACTORY OF TIANCHANG INT TOBACCO CO LTD +1

A method for ultrasonic-assisted laser deep penetration welding of plates

The invention relates to a method for deep penetration laser welding of a plate under the assistance of ultrasound. The method is characterized by comprising the following steps that firstly, first base metal (10) and second base metal (11) are machined to form butt joint end faces, and a series of inclined semicircular grooves are machined; secondly, the first base metal (10) and the second base metal (11) are in butt joint and are clamped, and a series of inclined blind holes are formed in a weld bead; thirdly, a first ultrasonic amplitude-changing rod (3) is pressed to the upper surface of a workpiece to be welded; fourthly, a second ultrasonic amplitude-changing rod (4) is fixed to one side of a laser welding head; fifthly, an ultrasonic generation device is started, the ultrasonic frequency is adjusted; sixthly, a laser beam (5) perpendicularly irradiates the upper surface of the workpiece, and the welding process is completed under continuous ultrasonic vibration; and seventhly, after welding is completed, ultrasonic vibration is maintained for 1-2 minutes. In the method, due to the pre-formed inclined blind holes and ultrasonic vibration, weld joint root leakage caused by molten pool downward flowing driven by local evaporation back flushing pressure of the front edge walls of the small holes is avoided.
Owner:CHANGSHA UNIVERSITY OF SCIENCE AND TECHNOLOGY

Continuously self-catalyzed deposition chemical plating solution of tin and using method thereof

InactiveCN101724834BEnables continuous autocatalytic depositionFast depositionLiquid/solution decomposition chemical coatingAntioxidantBenzaldehyde
The invention discloses continuously self-catalyzed deposition chemical plating solution of tin and a using method thereof. Half-bright and silvery-white tin-copper alloy deposition layers are obtained on pure copper and a copper alloy substrate. In the chemical plating solution, stannous chloride serves as a main salt, thiourea serves as a main complexing agent, trisodium citrate serves as an auxiliary complexing agent, sodium hypophosphite serves as a reducing agent, disodium ethylene diamine tetraacetate serves as an antioxidant, a hydrochloric acid serves as a stabilizing agent, gelatin serves as a leveling agent and benzaldehyde serves as an auxiliary brightening agent. The using method comprises the following operating conditions that: the pH value of the plating solution is 0.8 to 2.0; the temperature is 80 to 90 DEG C; the loading capacity is 0.8 to 1.5 dm2 / L; and the mechanical stirring speed is 50 to 100 rpm. The continuously self-catalyzed deposition chemical plating solution of the tin and the using method thereof have the advantages of capability of obtaining half-bright and silvery-while tin-copper alloy clad layers with different thicknesses by controlling chemical plating time, high deposition rate, remarkable grain refinement, improvement on surface evenness of the clad layer and batch production stability, secure interface combination, strong change resistance of the clad layer after being passivated, and broad application prospect in the products of deep hole elements, blind hole elements, difficult-to-handle miniature electronic components and parts, printed circuit boards PCBs and the like.
Owner:KUNMING UNIV OF SCI & TECH

A non-continuous point blank holder for a fine blanking die and its process parameter design method

The invention discloses a discontinuous point type blank holder for a fine blanking die and a design method of technological parameters of the discontinuous point type blank holder. The blank holder comprises a point type blank holder body, wherein a group of raised points are uniformly distributed on the lower surface of the point type blank holder body along the shape contour of a part required to be formed through fine blanking; rounded corners are arranged on the raised points; when the thickness of the part required to be formed through fine blanking is smaller than 5 mm, the point type blank holder is single-sided, and the technological parameters are determined; and when the thickness of the part required to be formed through fine blanking is larger than or equal to 5 mm, a group of raised points which have the same parameters with the raised points on the point type blank holder body are arranged on the upper surface of the fine blanking die, and the technological parameters are determined. According to the design method, aimed at fine blanking parts with different thicknesses, the technological parameters of the discontinuous point type blank holder can be effectively determined, the discontinuous point type blank holder can be widely applied to fine blanking, the cost of the fine blanking die is reduced, and the perfectness ratio of the surfaces of the parts is increased.
Owner:WUHAN UNIV OF TECH
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