407 results about "Oil water" patented technology

This utility model discloses an ultra-clean circulating cooling device for an electric furnace transformer, comprising an ultra-clean circulating water tank (2) that cooperates with a transformer oil-water cooler (1). A pair of outlet pipes (3) are connected to the ultra-clean circulating water tank (2), and the outlet pipes (3) are respectively connected to two transformer oil-water coolers (1). The transformer oil-water coolers (1) are then connected to a pair of plate heat exchangers (4) via pipes. The outlets of the plate heat exchangers (4) are connected to the ultra-clean circulating water tank (2) via return pipes (5). The advantage of this utility model is that it can eliminate water blockage in the oil-water cooler, ensure the heat exchange efficiency of the transformer oil-water cooler, thereby maintaining the normal operation of the cooler and preventing excessively high transformer oil and winding temperatures.

Disclosed are an integrated device for multiphase extraction and tail gas and wastewater treatment and a control method therefor. The integrated device comprises at least one set of small multiphase extraction units connected to an extraction well, a reagent tank storing a solubilizing agent and an oxidizing agent, a resin adsorption tower, an oil-water separator, a photocatalytic reactor, an oil storage tank, a heating system for heating the reagent tank and the oil-water separator and providing high-temperature steam for the resin adsorption tower, and a controller, wherein the reagent tank is separately connected to the extraction well and the photocatalytic reactor. Each multiphase extraction unit comprises a gas-liquid separator, a water ring vacuum pump, and a jet pump, wherein an extracted gas-liquid mixture undergoes gas-liquid separation by means of the gas-liquid separator, a waste gas is conveyed to the resin adsorption tower by means of the water ring vacuum pump, waste liquid and an extracted oil-water mixture are respectively conveyed to the oil-water separator by means of the jet pump, wastewater is conveyed to the photocatalytic reactor, and waste oil is conveyed to the oil storage tank. The present invention effectively ensures the stability and high efficiency of removal while realizing miniaturization.

The application discloses a Pickering emulsion based on ring-shaped colloidal particles, a preparation method thereof and application thereof in biphasic interface catalysis. The Pickering emulsion is an oil-in-water emulsion, which comprises a water phase, an oil phase and ring-shaped colloidal particles. The oil phase is dispersed in the water phase in the form of small droplets. The ring-shaped colloidal particles are located at an oil-water interface or at the oil-water interface and the water phase, and the ring-shaped colloidal particles are assembled to form a monolayer structure on the oil-water interface. The Pickering emulsion is not only beneficial to the contact between reactants or between the reactants and a catalyst, but also can enhance the interface mass transfer rate, promote the product to rapidly diffuse from one phase to another phase, has advantages of high conversion rate, high catalytic efficiency, simple product separation and the like, and has an important application prospect in the field of interface catalysis.

This application discloses a desalination system and method for kitchen waste. The system includes a filter press chamber, a feeding chamber, a washing chamber, an oil-water buffer tank, and a solid material silo connected in sequence. The filter press chamber is equipped with a cross-shaped rotating filter plate and a filter press pusher cylinder to achieve preliminary desalination of kitchen waste through filter pressing. The feeding chamber transports the solid material after filter pressing to the washing chamber through a feeding mechanism. The spray pipes and circulating pump in the washing chamber form a hot water circulating spray system. The oil-water mixture at the bottom of the washing chamber enters the oil-water buffer tank through an overflow hole, and the oil and water are automatically separated by a capacitive oil level sensor and an electrically controlled valve. The receiving screen sends the desalinated solid material into the solid material silo. By adopting the above solution, this invention can solve the technical problems of low salt removal efficiency and waste of resources, difficulty in separating oil and water layers that easily leads to secondary pollution, low degree of process automation resulting in cumbersome and unstable operation, low equipment integration and poor compatibility with existing production lines of livestock and poultry manure treatment enterprises in the current pretreatment of kitchen waste.

This utility model discloses an integrated oil-water separation device. The oil-water separation device includes a processing tank. A cover plate is movably mounted on the top of the processing tank via a rotating assembly, and an inlet is reserved on the top of the cover plate. An outlet is installed at the bottom of the processing tank. This utility model utilizes a motor to drive a rod, which in turn rotates a movable sleeve rod, causing a gear to rotate. A toothed block meshing with the gear is fixedly connected to the inner wall of a pre-reserved annular groove in the cover plate, causing the cover plate to rotate. Simultaneously, the arc-shaped plate rotates, allowing for vertical movement. This facilitates the lifting of the oil-water filter plate during cover plate lifting operations, making the oil-water filter plate exposed outside the processing tank easier to disassemble and replace. After the oil-water filter plate is exposed, rotating the threaded rod causes the annular groove to rotate, winding or unwinding a pull rope. The pull rope controls the movement of the interlocking block, enabling the disassembly and assembly of the oil-water filter plate, facilitating its replacement.

This invention discloses a method for calculating the remaining oil saturation of water-flooded layers in old wells based on multi-viscosity oil-water phase permeability experiments, relating to the field of petroleum extraction technology. The method includes: generating resistivity reduction rate curves based on multi-viscosity oil-water phase permeability experiments; establishing a quantitative relationship model between water cut and resistivity reduction rate of crude oils of different viscosities; calculating the resistivity reduction rate according to the target layer water cut and crude oil viscosity type using the appropriate quantitative relationship model, and calculating the resistivity of the water-flooded layer by combining it with the original oil layer resistivity; and calculating the remaining oil saturation of the water-flooded layer using the saturation formula. This invention, based on comparative experiments of multiple viscosities of oil-water phase permeability, obtains a relationship between resistivity reduction rate and water cut, resulting in higher accuracy of the calculation results. The method for calculating the remaining oil saturation of water-flooded layers avoids statistical bias and production losses caused by shutting down production wells for post-casing saturation logging. It is applicable to crude oil reservoirs of different viscosities, and its large-scale application in water-drive oilfield development will improve development efficiency.

The application discloses a watered-out layer secondary interpretation method under the condition of small layer level oil-water interface understanding, and steps are as follows: step 1, small layer geological modeling and oil-water interface fine calibration; step 2, well logging data standardization and quality control; step 3, continuous calculation of small layer mixed formation water resistivity; step 4, completion of reservoir parameter quantitative calculation; step 5, obtaining of primary interpretation based on small layer oil-water interface; step 6, implementation of secondary iteration correction under the constraint of production dynamics; and step 7, output of interpretation results and application suggestions. The application belongs to the technical field of oilfield development well logging interpretation, and solves the problems that the prior art is not accurate in key parameter calculation, the interpretation process is single, and the precision and actual development demand are not matched.

The utility model relates to kitchen garbage waste liquid treatment technical field discloses a kind of kitchen garbage heating oil-water separation device, including box, the upper surface of the box is provided with filter screen, the inside sliding connection of the box has floating plate, the bottom fixed connection of the floating plate has oil suction pipe, the inside fixed connection of the box has heating rod, the lateral wall of the box is fixedly connected with oil collecting tank, the lateral wall of the oil collecting tank is fixedly connected with oil suction pump, the output end fixed connection of the oil suction pump has conveying hose, the upper surface of the floating plate is fixedly connected in the conveying hose one end, the lateral wall of the box is provided with vibration assembly, the lateral wall of the filter screen is provided with fixed component. In the utility model, by starting motor makes rotary disc rotation, let rotating strip rotate and pull vibration frame left and right slide, reach to filter screen vibration effect, prevent material to be accumulated on filter screen and cause the blockage of filter screen, improve the filtration effect by the above structure.

The utility model provides a kind of oil-water separation device, comprising: cavity, magnetic field generating module being arranged in the cavity, protective cover being oppositely arranged with magnetic field generating module and multiple wire bundles being rotationally arranged between magnetic field generating module and protective cover, protective cover is located at the top of cavity, magnetic induction space is formed between magnetic field generating module and protective cover, waste water in water inlet pipe enters magnetic induction space, and drive wire bundle to rotate to cut magnetic induction line.The utility model can improve the efficiency of demulsification and separation of oil and water at the same time, cut magnetic induction line movement using waste water kinetic energy, simplify power device, greatly reduce energy consumption.

This utility model discloses a novel hydrocyclone tube, relating to the field of hydrocyclone oil-water separation technology. It includes a hydrocyclone, an inlet connector, and an outlet pipe. The end of the outlet pipe is connected to an outlet passage, and the outlet pipe and outlet passage are interlocked with a first sealing element between them. A first convex ring is provided on the outlet pipe, and a second convex ring is provided on the outlet passage. The first and second convex rings are connected by a sealing connector, forming a sealed chamber. A second sealing element is provided between the first convex ring and the sealing connector, and a third sealing element is provided between the second convex ring and the sealing connector. This utility model achieves a stable sealed connection between the outlet pipe and the outlet passage, ensuring uniform liquid inflow and preventing inlet blockage. Several hydrocyclone plates are evenly arranged on the surface of the hydrocyclone, optimizing the hydrocyclone effect and achieving efficient oil-water separation. Furthermore, the hydrocyclone is connected to the inlet connector via a snap-fit ​​structure, facilitating disassembly and cleaning of the hydrocyclone.

The application discloses a shale oil reservoir core micro-percolation model and a preparation method and application thereof, and belongs to the technical field of oilfield development experiment researches.The core micro-percolation model comprises a rock sample and adhesive glass sheets used on two surfaces of the rock sample, and according to the oil-water flow direction in the rock sample, the side surface of the rock sample is set as an inflow end, an outflow end, a first end and a second end respectively, one or two needle heads are arranged close to the inflow end, one needle head is arranged close to the outflow end, and the core micro-percolation model is packaged through glue.The single-needle head and double-needle head micro-percolation models are prepared for different types of shale oil reservoir cores, and oil-water two-phase percolation experiments are carried out on typical rock samples; through the experiments, more accurate understanding of the percolation channels of oil and water in the shale reservoir core is obtained, the distribution states of residual oil and bound water in the core are accurately characterized in a visualized mode, and important references can be provided for the research on percolation curves, the understanding of percolation rules and the compilation of development schemes.

This utility model relates to the technical field of oil sludge separation devices, specifically to a solid-phase and liquid-phase separation device for oil sludge treatment. It includes an oil sludge crushing box, an oil-liquid separation box installed at the bottom of the crushing box, and a box cover installed at the top of the crushing box. A crushing mechanism is fixed to the top of the box cover and penetrates through the crushing box into the oil-liquid separation box. A separation mechanism is installed between the crushing box and the oil sludge crushing box, penetrating into the oil-liquid separation box. A filter plate is bolted to the inside of the crushing box. This utility model achieves crushing and stirring of the oil sludge through the cooperation of the internal parts of the crushing mechanism, and compresses the crushed sludge to better separate the oil and water within the sludge. The separation of oil and water is achieved through the cooperation of the internal parts of the separation mechanism, creating separate oil and water layers for easier separation and discharge.

The application discloses a water cutting device for cutting interlayer water, and an oil product storage tank and a method comprising the same, and belongs to the technical field of oil product storage tanks. The water cutting device for cutting interlayer water disclosed by the application can realize the cutting of interlayer water of oil-water stratification at different positions in the oil product storage tank by arranging an interlayer water cutting device in the water cutting line pipe and controlling the position of the interlayer water cutting device through a lifting device. Meanwhile, the water cutting device can be freely switched with the water cutting line pipe, and the cutting of interlayer water between tank bottom water and heavy oil and light oil can be realized at the same time. The technical problem that the existing water cutting device cannot simultaneously cut interlayer water between heavy oil and light oil is solved, the interlayer water in the oil product in the tank can be removed, and fluctuations or production accidents of downstream devices caused by water in the oil product are avoided.

The utility model discloses a powder spraying device capable of uniformly spraying powder, which comprises a bearing plate, a supporting box body is fixedly arranged above the bearing plate through a bolt fastener, a control box body is stably and fixedly arranged at the top of the supporting box body, an oil-water separator is arranged on one side of the supporting box body, and a water outlet is formed in the other side of the supporting box body. A main air inlet seat is specially arranged on the rear side of the control box body, an air inlet pipe is connected to the upper portion of the main air inlet seat, a vulcanizing powder barrel device is further placed on the upper portion of the bearing plate, a powder suction rod stretches into the vulcanizing powder barrel device to suck powder, the powder is conveyed to a spray gun through a wheel cylinder body and a powder conveying pipe, it is guaranteed that the powder is conveyed stably and continuously, and a foundation is laid for uniform powder spraying. The fluidizer enables powder to uniformly enter a gun and avoid caking, the adjusting static knob on the box body is controlled to accurately adjust static parameters, the powder is uniformly attached to a workpiece, the atomization adjusting valve accurately adjusts atomization parameters, the powder is atomized well and diffused uniformly, uniform distribution in the whole powder spraying process is achieved, and the powder spraying quality is improved.

This invention relates to a microwave multi-mode flow measurement method for horizontal oil-water two-phase flow, employing a combination of a coplanar waveguide-excited helical microwave sensor and a dual-coaxial microstrip antenna sensing unit. The method includes: constructing a relationship between the mixing dielectric constant and water holdup of the horizontal oil-water two-phase flow based on the phase output signal of the coplanar waveguide-excited helical microwave sensor, thereby obtaining formulas for predicting water holdup and oil holdup using the dielectric constant of the oil-water mixture in a horizontal pipe; utilizing the upstream and downstream phase output signals of the dual-coaxial microstrip antenna sensing unit; constructing a correlation velocity model for the horizontal oil-water two-phase flow under different operating conditions based on experimental data, obtaining the functional relationship between the correlation velocity of the mixed fluid in the pipe and the mixing velocity and the phase-separated apparent velocity; and constructing a drift model for the horizontal oil-water two-phase flow under different flow patterns, obtaining functions relating the mixing velocity, the oil phase apparent velocity, and the oil holdup. This invention offers high measurement accuracy.

This invention provides an underwater oil storage system, method, and medium, relating to the field of offshore oil development technology. The system includes: an interconnected underwater oil storage unit, a data acquisition unit, and a control unit, all located in an underwater environment. The underwater oil storage unit includes several oil tanks for storing crude oil. The data acquisition unit is used to acquire first parameters of the crude oil, second parameters of the oil-water separation layer in the oil tanks, and third parameters of the underwater environment. The control unit is used to regulate the underwater oil storage unit based on the first, second, and third parameters. The first parameters include temperature and content; the second parameters include pressure difference; and the third parameters include flow velocity and wave height. In this way, the data acquisition unit can monitor the oil-water separation and underwater environment conditions in real time, enabling the control unit to regulate the underwater oil storage unit. This allows for the timely detection and resolution of potential underwater safety hazards, ensuring the safety of underwater oil storage.

This invention discloses an anti-sloshing device and its control method for an oil-water separator tank on an offshore platform, belonging to the field of offshore oil and gas development equipment. The device includes a tank body, a condition monitoring component (DVL flow meter and wave height meter), symmetrically arranged liftable wave generators, and a control unit. Based on the monitored fluid direction and wave height data, the control unit drives the wave generator on the same side as the flow direction to generate reverse waves with opposite propagation directions and matching wave heights, actively counteracting sloshing. This invention dynamically suppresses liquid sloshing through a closed-loop control system of "monitoring-analysis-reverse wave generation," significantly improving separation stability and efficiency while reducing structural load.

The present application relates to the technical field of oily sewage treatment, in particular to an oil-water separation tank for oily sewage, comprising a tank body and an oil-water separator arranged in the tank body. The tank body is sequentially provided with an inlet groove, a distribution groove, an overflow groove and a water storage groove along the water flow direction, and the oil-water separator is arranged between the inlet groove and the distribution groove and is internally formed by a plurality of partition plates to form a continuous flow channel. The oil-water separator sequentially comprises a horizontal separation section, a twist conversion section and a vertical stratification section, and the partition plates are arranged in a horizontal, inclined or vertical state according to the structure requirements in different sections, so as to guide the oil droplets to gradually gather, float up and realize effective oil-water separation. The present application has compact structure, improves the separation efficiency by using the geometric design of the flow channel, and improves the liquid flow direction to improve the liquid flow rate in the flow channel. It is suitable for the pretreatment or reuse system of oily wastewater in the fields of industry and environmental protection.

The utility model discloses a continuous layered oil separator, the continuous layered oil separator includes the main part, the feed inlet of setting in the upper portion one side of main part and setting in the lower portion of main part another side water phase discharge gate, the main part is separated through a plurality of baffle in the inside and is separated a plurality of separating chambers, and the one side of separating chamber is provided with oil phase chamber and water phase chamber, and each separating chamber and water phase chamber are connected with oil phase chamber through pipeline, and one end of each baffle is contacted with the inner wall of main part, and is equipped with the liquid discharge port in the other end near the inner wall of main part, and the liquid discharge port on any two adjacent baffle is staggered setting, the utility model discloses a continuous layered oil separator, makes oil -water mixture slowly flow in each chamber, makes oil -water completely delaminates, and oil phase is gathered to oil phase chamber finally and is discharged through the oil outlet of each chamber, and water phase flows to water phase chamber, and is discharged through water phase discharge gate, and realizes the continuous separation of material light and heavy components under the closed environment.

The application discloses a kind of calcined coal gangue composite clinker low-carbon preparation system and preparation method based on cement production line, including cooling machine, vertical cylinder preheater, cyclone separator, prehydroxyl removal device, condenser and oil-water separator;The application proposes to use prehydroxyl removal device, combined with cooling machine to prepare composite clinker by calcining coal gangue, and the removed water does not enter the cement kiln firing system, and the prehydroxyl removal high-temperature coal gangue is calcined and activated in the cooling machine, the method is simple, has little effect on the cement kiln firing system, and the prepared calcined coal gangue active material has good quality and low cost, the coal gangue disposal amount is large, the heat value utilization rate is high, can reduce the energy consumption and carbon emission of cement industry, and has good economic benefit and social benefit.

This invention discloses a nitrogen-free atmospheric pressure superconducting heater, which relates to the field of heaters. The heater includes a heater body, within which an oil-water coil, an oxygen preheating pipe, a natural gas preheating pipe, and a combustion chamber are arranged. A superconducting heat pipe is installed at the top of the combustion chamber. A pure oxygen generator is installed at one end of the oxygen preheating pipe, and a natural gas source is installed at one end of the natural gas preheating pipe. An oxygen-enriched burner is installed on the side of the heater body. This nitrogen-free atmospheric pressure superconducting heater integrates environmental protection, energy saving, and safety. It solves the problems of inaccurate nitrogen control and inability to ensure long-term stable NOx compliance in existing heaters with low-NOx burners; it also solves the problem of existing heaters using conventional low-NOx burners generating large amounts of sulfurized condensate that corrodes the chimney; and it addresses the issues of existing heaters operating under closed pressure, being pressure vessels requiring mandatory annual inspections of the equipment and safety accessories, posing high-pressure risks and complex maintenance requirements.

The utility model discloses a small -size mining rock drilling jumbo rear suspension, including rear suspension bottom plate, both sides of rear suspension bottom plate all are fixedly installed with rear suspension side plate, and the rear suspension tailboard is fixed between two rear suspension side plates, and rear suspension tailboard is located rear suspension bottom plate upside tail part, rear suspension tailboard side face upper portion fixedly installed with reel fixed base, reel fixed base side fixedly installed with oil -water separator mounting plate. Small -size mining rock drilling jumbo rear suspension, adopts welding mode and concentrates the spare part on rock drilling jumbo together, and the collective overhaul of staff is convenient, improves the overhaul efficiency, and can effectively reduce the volume of rear suspension after the concentration of spare part, and the rock drilling jumbo of equipping this rear suspension is convenient in the mine roadway and moves operation, reduces the harm and loss caused by collision.

The utility model discloses an underground oil sleeve intercommunication valve, including sleeve and the upper joint and lower joint of fixed in the upper and lower ends of sleeve respectively, the upper joint is connected with the lower end of oil pipe, and the inner seal sliding sleeve is arranged in the middle part of the cavity of sleeve, and the sucker rod is arranged in the sleeve and is through the sleeve and inner seal sliding sleeve, and the lower part side of sucker rod is connected with control coupling, and the bottom of the upper joint in the sleeve is provided with upper card station, and the upper and lower ends of inner seal sliding sleeve are provided with elastic inner clamping claw, and elastic inner clamping claw is matched with upper card station and lower card station respectively, the utility model is used for the oil and water well workover operation process, and when lifting oil pipe, the oil and water in the oil pipe are arranged back to the well, and when the oil well needs to be washed hot, the sucker rod is lifted to open the oil discharge passage, and the oil sleeve space is communicated, can be washed well, and after well washing, the sucker rod is lowered, the passage is closed, and the oil is pumped normally, preventing the environmental pollution caused by falling.

The application discloses a waste oil and fat biological continuous skid-mounted type biodiesel preparation equipment, which comprises a casing, a stirring barrel is rotationally connected to the top surface of the casing, a feeding hole is formed in the top surface of the stirring barrel, a plurality of first heaters are installed on the circumferential outer side of the stirring barrel, and a plurality of stirring assemblies are installed in the stirring barrel. The application realizes the purposes of efficient crushing, uniform fusion and sufficient reaction of soapstock, and also realizes the purposes of slowly eccentric rotating of the sedimentation barrel driven by the eccentric shaft, forming an alternating flow field, promoting the three-phase separation of oil, water and slag, and strengthening the sedimentation effect, shortening the sedimentation period through the micro-vibration mechanism. The knocking vibration mechanism is used for reducing the hanging material of the barrel wall, improving the stirring efficiency and guaranteeing the sufficiency of the reaction. The hollow rotating shaft, the transfer cylinder and the nozzle are used for guaranteeing the accurate dispersion of the reagent, saving the reagent consumption and improving the reaction quality.

The present invention provides a maintenance method and apparatus for separation tanks, electronic equipment, and a storage medium that can reduce the consumption of lubricating oil and lower costs. [Solution] The maintenance of the separation tank includes injecting new lubricating oil into the separation tank based on a predetermined oil injection valve, discharging the emulsified lubricating oil in the sealed chamber of the sealed oil vacuum pump into the separation tank based on a predetermined oil discharge valve, mixing the new lubricating oil with the emulsified lubricating oil, and injecting clean lubricating oil into the oil-water separator to a predetermined liquid level. By discharging the emulsified lubricating oil into the separation tank and adding new lubricating oil, the two are mixed, then oil-water separation is performed, thereby realizing the recycling and reuse of the lubricating oil.

The application provides a kind of anti-toppling aromatherapy machine, including base, fan, liquid storage tank and atomizer;The base has containing cavity and air inlet groove in it;Air inlet groove protrudes from the bottom of base, and first liquid leakage hole and first liquid blocking piece are arranged in air inlet groove;Fan is installed in containing cavity;Liquid storage tank is installed above base, and air guide pipe is arranged in liquid storage tank, and air inlet end of air guide pipe extends into containing cavity;Air inlet groove is communicated with air inlet end of air guide pipe and air outlet end of fan;First liquid blocking groove is formed between first liquid blocking piece, air inlet groove and air guide pipe, and first liquid leakage hole is located in first liquid blocking groove;Atomizer is arranged in containing cavity and connected with liquid storage tank.In the application, when aromatherapy machine is in toppling state, oil-water mixture flows into air inlet groove from air guide pipe, is blocked by first liquid blocking piece, and flows out through first liquid leakage hole, effectively preventing oil-water mixture from accumulating and leaking in aromatherapy machine, thereby avoiding damage and pollution problems caused by toppling of aromatherapy machine.

This utility model discloses an oil-water separation device for wastewater treatment, relating to the field of oil-water separation technology. It includes a separation tank with a first and second partition fixed inside. The first and second partitions are fixedly connected and divide the interior of the separation tank into upper and lower parts. A through hole is formed on the first partition, and a sliding groove is formed on the second partition, with the through hole communicating with the sliding groove. A hydraulic cylinder is installed on the right side of the separation tank. Oily wastewater is pumped into the separation tank using a pumping component. After all the oil in the wastewater floats to the surface, the lower layer of wastewater is discharged using a pumping component. When the water-oil boundary line in the separation tank approaches the first partition, a push plate is inserted into the through hole by the hydraulic cylinder to engage with it. Complete oil-water separation is achieved using a hydrophobic membrane, allowing the oil to be discharged along the oil drain pipe, while the wastewater is completely discharged by the pumping component.

The utility model discloses a production device of triazinone belongs to triazinone production technical field, including the separation tank, the separation tank top is connected with hydrolytic kettle, acid supply jar and alkali supply jar respectively, be equipped with stirring subassembly on the separation tank, the separation tank lower end side wall is equipped with the liquid outlet, be equipped with filter screen on the liquid outlet, the liquid outlet is connected with waste liquid jar through the liquid outlet pipeline, along liquid flow direction, first liquid pump, first three -way valve are equipped with in proper order on the liquid outlet pipeline, one port of first three -way valve is connected with oxidation kettle through the liquid distribution pipeline, the oxidation kettle is connected with cyclization kettle, the utility model adds the separation tank between hydrolytic kettle and oxidation kettle, keeps oil phase and oil -water mixture in the separation tank, utilizes solubility and separates the material of separation tank with oil phase, and material is discharged into oxidation kettle and reacts, shortens production time, reduces material waste and equipment floor area.