The invention relates to the technical field of
polymer materials, and particularly discloses a three-dimensional raspberry-shaped CdS (at) MXene
microsphere, a multi-
pollution-resistant polyarylene
ether nitrile membrane material containing the three-dimensional raspberry-shaped CdS (at) MXene
microsphere, a preparation method and application of the three-dimensional raspberry-shaped CdS (at) MXene
microsphere and the multi-
pollution-resistant polyarylene
ether nitrile membrane material aiming at the problem of dense stacking of adopted two-dimensional MXene lamellar material in the existing
composite membrane material for
oily wastewater treatment. The preparation method comprises the following steps: mixing a
polymethyl methacrylate aqueous solution with an MXene suspension, carrying out a stirring reaction, and after the reaction is finished, carrying out separation, washing and
drying to obtain three-dimensional MXene microspheres; and mixing the three-dimensional MXene microspheres with a CdCl2
aqueous solution, magnetically stirring, then adding
thiourea, continuously stirring, placing at 160-200 DEG C, carrying out a
hydrothermal reaction, and after the reaction is finished, separating, washing and
drying to obtain the three-dimensional raspberry-shaped CdS-coated MXene microspheres. The three-dimensional raspberry-shaped CdS-coated MXene microspheres are introduced into a polyarylene
ether nitrile membrane material, so that the problems of dense stacking and complex membrane
pollution of the existing two-dimensional MXene sheet layer can be effectively solved, and the limitation of separation flux is broken through.