Patents
Literature
Patsnap Copilot is an intelligent assistant for R&D personnel, combined with Patent DNA, to facilitate innovative research.
Patsnap Copilot

244results about How to "Increase electrostatic repulsion" patented technology

Aqueous grinding fluid applied to super precision grinding of hard and brittle materials and application method thereof

The invention discloses an aqueous grinding fluid applied to super precision grinding of hard and brittle materials and an application method thereof. The grinding liquid contains chelant 0.1-5, a pH value regulator 5-15, a suspending agent 0.2-5, a dispersion stabilizer 0.5-10, a lubricant 5-20, an antirusting agent 0.5-5, fungicide 0-2, a defoamer 0-2 and deionized water compensating the balance of total amount of 100 parts. Under an alkali condition, the aqueous grinding fluid applied to super precision grinding of hard and brittle materials is beneficial for grinding materials with various sizes, has good suspension property and dispersion stability; when the aqueous grinding fluid is used for super precision grinding of various different hard and brittle materials, especially high-hardness materials, scratches, etching pits and other defects are not produced easily; and the grinding speed is high, the subsequent cleaning is convenient; and the aqueous grinding fluid has excellent lubricating property and antirusting property when in matched use with the grinding materials, and the mixing liquid is uniform in color and has no sediment in 48 h. When the aqueous grinding fluid is used for grinding a wafer on a grinding machine, the ground wafer is subjected to water-added ultrasonic washing, and the wafer has good surface smooth finish, no scales, etching pits and other defects, and the surface roughness can be within 2 microns.
Owner:AMER TECH CO LTD

Preparation method of ester type viscosity reduction type polycarboxylate superplasticizer

The invention discloses a preparation method of an ester type viscosity reduction type polycarboxylate superplasticizer. The method comprises the following steps: (1) preparing an esterified monomer; (2) conducting the copolymerization reaction; (3) conducting the neutralization reaction. According to the technical scheme of the preparation method, methyl methacrylate and dimethylaminoethanol, remaining after the preparation of the esterified monomer, are subjected to ester exchange in the same condition of preparing the esterified monomer so as to obtain dimethylaminoethyl methacrylate as a functional monomer. Therefore, the preparation method is cost-saving and simple in operation. In addition, the functional monomer is directly introduced into the copolymerization reaction to react with other cationic monomers. During the polymerization process, anions, cations and tertiary amine groups are attached to polycarboxylic acid molecular chains, so that the surface adsorbability of cement particles can be improved. The electrostatic repulsion effect between cement particles is improved. Not only the ester type viscosity reduction type polycarboxylate superplasticizer is good in anti-sludge effect for sand and gravel materials high in cement content, but also the ester type viscosity reduction type polycarboxylate superplasticizer is good in dispersibility and viscosity-reducing effect.
Owner:KZJ NEW MATERIALS GROUP CO LTD

Preparation method and application of pH sensitive type magnetic demulsifier with surface charges and hydrophilic-hydrophobic properties controlled

The invention provides a preparation method and application of a pH sensitive type magnetic demulsifier with surface charges and hydrophilic-hydrophobic properties controlled. Based on magnetic Fe3O4 nanoparticles, through surface modification with silicon dioxide and a grafting copolymerization reaction, surface active monomers and pH sensitive monomer copolymer chains are introduced on the surfaces of the nanoparticles, and the surface grafting structure and the pH value are further adjusted to control the surface charges and hydrophilic-hydrophobic properties of the magnetic nanoparticles. The reduction of the pH value can enhance the hydrophobic property of the magnetic nanoparticles and reduce negative charge repulsive interaction between the demulsifier and oil droplets so that the demulsifier can be absorbed onto the surfaces of the emulsified oil droplets and quickly isolate the emulsified oil droplets under the action of an external magnetic field. Recycling of the magnetic nanoparticles can be achieved, and the demulsifier is be unlikely to be affected by pollution of negative-ion surface active materials in emulsified oil wastewater. According to the magnetic demulsifier, the preparation method is simple, the recycling process is convenient and efficient, the recycling performance is excellent, and therefore the magnetic demulsifier has very board application prospects in the fields of emulsified oil wastewater treatment and oil-water separation.
Owner:HANGZHOU DIANZI UNIV

Slow-release polycarboxylate superplasticizer and preparation method thereof

The invention discloses a slow-release polycarboxylate superplasticizer and a preparation method thereof. The preparation method comprises specific steps as follows: firstly, small unsaturated carboxylic acid monomers and diphenylphosphinyl chloride are subjected to a partial reaction, and small unsaturated monomers containing phosphate ester groups are obtained; then 2-phenylethylamine and phosphate ester groups are added to a reaction system and subjected to a reaction, and small unsaturated monomers containing amide groups are obtained; the small unsaturated monomers containing the amide groups are subjected to an oxidation-reduction free radical polymerization reaction with unsaturated polyether macromonomers under the action of an initiating agent, a reducing agent and a chain transfer agent, and a copolymerization product is obtained; pH value is adjusted to 6-7 after the reaction, water is added, and the polycarboxylate superplasticizer is obtained. The amide groups containing benzene rings are introduced to side chains of the prepared polycarboxylate superplasticizer, so that the dispersibility of the polycarboxylate superplasticizer for cement is improved, the polycarboxylate superplasticizer has good slump retaining performance on the premise of water reduction, and besides, the yield of the polycarboxylate superplasticizer containing the amide groups can reach 94% or higher.
Owner:JIANGSU CHINA RAILWAY ARIT NEW MATEIRALS CO LTD

Magnetic iron-oxide nanoparticle covering method using silicon dioxide

The invention relates to a magnetic iron-oxide nanoparticle covering method using silicon dioxide and belongs to the technical field of nano material preparation. The magnetic iron-oxide nanoparticle covering method using the silicon dioxide mainly comprises preparing water-soluble magnetic iron-oxide nanoparticles through a known method; adding appropriate surface modifier into water base dispersion liquid to form into stable water base dispersion liquid; adding simple substance metal silica powder into the water base dispersion liquid, heating and stirring, enabling the silica powder to hydrolyze under catalysis of alkaline substance to generate into silicon dioxide to be deposited on surfaces of the magnetic iron-oxide nanoparticles and obtaining the silicon dioxide covered magnetic iron-oxide nanoparticles. The magnetic iron-oxide nanoparticle covering method using the silicon dioxide has the advantages of being simple in preparation technology, green and environmental friendly, easily available in material and low win cost and achieving large-scale industrialized production due to the fact that organic solvent and surface active agent are not required in the preparation process and the covering reaction is performed in water solution; enabling obtained products to be strong in morphology controllability, high in purity degree and particularly suitable for biomedical application; being widely applied to silicon dioxide covering of other nanocrystallines such as quantum dots and precious metal nano particles.
Owner:QINGDAO UNIV OF SCI & TECH

High-slump-loss-resistant synergist and preparation method and application thereof

The invention belongs to the technical field of concrete, and provides a high-slump-loss-resistant synergist, which is prepared from 40 to 60 parts of slump maintainers, 6 to 30 parts of thickening agents, 8.5 to 25 parts of polyhydroxyl retarders, 12 to 50 parts of excitants, 9 to 38 parts of sodium acetate or sodium silicate and 10 to 100 parts of hydramine or simethicone, wherein the slump maintainers are prepared from 300 to 450 parts of polyether, 20 to 45 parts of unsaturated acid, 30 to 80 parts of acrylic ester, 1.1 to 3.8 parts of chain transferring agents and 0.5 to 1.5 parts of reducing agents. A preparation method comprises the following steps of adding polyether into water; performing heating dissolution; then, dripping a material A and a material B; performing reaction for one hour to obtain the slump maintainers; adding water into thickening agents for dissolution; sequentially adding the polyhydroxyl retarders, the excitants, sodium acetate or sodium silicate; after thedissolution, adding hydramine or simethicone; adding the slump maintainers; performing uniform mixing to obtain the high-slump-loss-resistant synergist applied to concrete preparation. By using the technical scheme, the high-slump-loss-resistant synergist solves the problem of fast concrete slump loss in the prior art; meanwhile, the intensity is improved.
Owner:兰州同邦建材有限公司

Wet gradient honeycomb structure fiber membrane for medical and health protection and preparation method thereof

The invention relates to a wet gradient honeycomb structure fiber membrane for medical and health protection and a preparation method thereof. The preparation method comprises the steps that firstly,electrostatic spinning is carried out on a first spinning solution composed of a hydrophilic polymer, a nanoscale metal organic framework, a first cross-linking agent and a first solvent, and an insulating material subjected to charge elimination treatment is taken as a receiving base material to obtain a first membrane; a second spinning solution composed of an intermediate polymer, a second cross-linking agent and a second solvent is then subjected to electrostatic spinning, and the first membrane is taken as a receiving base material to obtain a second membrane; and a third spinning solution composed of a hydrophobic polymer, a third cross-linking agent and a third solvent is subjected to electrostatic spinning, the second membrane is taken as a receiving base material to obtain a thirdmembrane, the composite fiber membrane is obtained, and finally, the composite fiber membrane is subjected to heat treatment to obtain the wet gradient honeycomb structure fiber membrane for medicaland health protection. The finally prepared membrane has a three-layer composite structure, the microstructure is in a three-dimensional honeycomb communication channel structure, and the single-direction moisture conductivity and the reverse barrier liquid penetration performance are excellent.
Owner:DONGHUA UNIV

Preparation method of ether ester copolymerization type polycarboxylic acid water reducing agent capable of improving rheological behavior

The invention discloses a preparation method of an ether ester copolymerization type polycarboxylic acid water reducing agent for improving a rheological behavior. The water reducing agent is preparedthrough a copolymerization reaction of a first mixture, unsaturated polyether with the molecular weight of 4000-6000, unsaturated acid, a compound A, an initiator, a molecular weight regulator and deionized water, wherein the first mixture is prepared through an ester exchange reaction of methoxypolyethylene glycol with the molecular weight of 1000-4000, alkylphenol polyoxyethylene ether, unsaturated carboxylic ester and a polymerization inhibitor. According to the invention, a benzene ring and an imide structure are introduced, and the introduction of the benzene ring structure can effectively improve the adsorption efficiency and the thickness of an adsorption layer of polymer molecules on the surface of cement particles, so that the space stability effect of the water reducing agent ismore obvious; by means of introducing the imide structure, the adsorbability on the surface of the cement particles, the electrostatic repulsion effect among the cement particles, and the stability and the fluidity of the cement paste can be improved.
Owner:KZJ NEW MATERIALS GROUP CO LTD +1

High-molecular-weight lignin pesticide dispersant with high carboxyl group content and preparing method thereof

The invention discloses a high-molecular-weight lignin pesticide dispersant with high carboxyl group content and a preparing method thereof. The preparing method includes the steps that after lignin and catechol are mixed evenly, concentrated sulfuric acid is added, and after reactions, the product is cooled to the room temperature, purified and dried to obtain phenolated lignin; the phenolated lignin and alkenyl succinic anhydride are placed in a reactor, and organic solvent and a sodium hydroxide solid are added and stirred; the temperature is raised to 80 DEG C-95 DEG C to conduct reactions, and carboxylation lignin is obtained after filtering, washing and drying; the carboxylation lignin is added into water to form a water solution under the stirring condition, the pH value is adjusted to 10-12, epoxy chloropropane is added to conduct a polycondensation reaction, and the pH value of a reaction solution is adjusted to 6-7 to obtain the lignin pesticide dispersant. The weight-average molecular weight of the obtained dispersant is larger than 15000, and the carboxyl group content is 3.2-4.0 mmol / g. The high-molecular-weight lignin pesticide dispersant is suitable for various kinds of pesticide wettable powder and water dispersible granules and has excellent dispersibility, stability, wettability and heat storing performance.
Owner:图们市华威友邦化工有限公司
Who we serve
  • R&D Engineer
  • R&D Manager
  • IP Professional
Why Eureka
  • Industry Leading Data Capabilities
  • Powerful AI technology
  • Patent DNA Extraction
Social media
Try Eureka
PatSnap group products