The invention discloses a preparation method of low-gas high-purity
chromium. The preparation method comprises the following steps: S1, preparing part of
metal chromium by adopting an aluminothermic method, and crushing the
metal chromium into
powder with the particle size of 60-200 meshes; preparing the other part of
metal chromium by adopting an electrolytic method, and crushing the metal chromium into
powder with the particle size of 60-200 meshes; s2, the two parts of metal chromium
powder and
graphite powder are mixed and pressed into a round
ingot of 30 mm * (18 + / -2) mm, the round
ingot is loaded into a
graphite crucible, and the
graphite powder accounts for 0.5%-2% of the total
mass of the round
ingot; s3, the
graphite crucible containing the round ingot is put into a
vacuum furnace to be smelted; heating is started when the vacuum degree in the
vacuum furnace is smaller than or equal to 5 Mpa, the temperature is increased to 1400-1600 DEG C and kept for 10-15 h, then cooling is conducted, when the temperature is reduced to 1200-1100 DEG C,
hydrogen is charged into the
vacuum furnace to 15-20 Pa, and pressure is kept for 1 h; and S4, after pressure maintaining is finished, the temperature is increased to 1400-1600 DEG C, heat preservation is carried out for 2 h, then cooling is carried out, and when the temperature is reduced to the
room temperature, discharging is carried out.