6results about How to "Morphological rules" patented technology

The invention discloses battery-grade lithium carbonate as well as a preparation method and application thereof, and the preparation method comprises the following steps: synchronously introducing a lithium-containing solution and carbon dioxide bubble water into a reaction device, and reacting to obtain lithium carbonate; the carbon dioxide bubble water is prepared by adopting the following method: simultaneously introducing carbon dioxide and water into a shear pump, and shearing and mixing to prepare the carbon dioxide bubble water. According to the method, the traditional gas-liquid reaction that carbon dioxide is directly introduced into the lithium-containing solution is creatively transformed into a gas-liquid-liquid reaction system that carbon dioxide bubble water prepared in advance and the lithium-containing solution are synchronously introduced, so that the product purity and stability are remarkably improved, and the bottleneck of a traditional intermittent process is broken through; the preparation method is simple, the production capacity and efficiency are remarkably improved, industrial large-scale production is easy to realize, and the obtained product lithium carbonate crystal is complete in growth, concentrated and controllable in particle size distribution and regular in morphology, and meets the processing requirements of high-end battery materials.

This invention discloses an in-situ surface-coated LiF-coated water-resistant 4.7V lithium cobalt oxide cathode material, its preparation method, and its applications. The chemical formula of the cathode material of this invention is Li. 1‑2x‑2y Co 1‑ z Mg x Ni y Al z O2@LiF, where 0≤x≤0.05, 0≤y≤0.05, 0≤z≤0.05, and x, y, and z cannot all be 0; LiF is Li 1‑2x‑2y Co 1‑z Mg x Ni y Al z O2 material coating layer. This invention mixes lithium metal salts, cobalt compounds, and an F-containing dopant to obtain a mixture; the mixture is sintered once at a high temperature, then cooled and ground uniformly, followed by a second sintering and cooling to obtain the in-situ surface-coated water-resistant 4.7V lithium cobalt oxide material. This invention constructs a complete, continuous, and uniformly distributed hydrophobic protective layer on the surface of lithium cobalt oxide particles through in-situ coating technology, effectively blocking the corrosion of the material by electrolyte and moisture; the simultaneously formed elemental doping enhances the metal-oxygen bond binding energy, synergistically improving the bulk structural stability and jointly ensuring the long cycle life of the electrode material.

The invention discloses a preparation method of conductive paste for a solar cell, and relates to the technical field of solar cell preparation. The preparation method comprises the following steps: adding a copper source, a surfactant, a dispersant and a brightness modifier into a solvent to obtain a first mixed solution; adding a reducing agent and a chelating agent into a solvent to obtain a second mixed solution; the first mixed solution and the second mixed solution are mixed according to the preset volume ratio, a third mixed solution is obtained, and seed copper powder with the preset mass fraction is added into the third mixed solution; the third mixed solution after the reaction is sequentially subjected to sedimentation cooling treatment, centrifugal treatment, drying treatment and grinding treatment, micron-sized copper powder is prepared, a conductive silver layer is deposited on the surface of the micron-sized copper powder through chemical reduction reaction, silver-coated copper powder is prepared, and the conductive paste is prepared through the silver-coated copper powder. The micron-sized copper powder prepared through the method can meet the high target size interval yield, the preparation cost is low, and the process compatibility is high.

This invention discloses a BN@EVA composite pour point depressant and its preparation method, belonging to the petrochemical field. The invention improves the compatibility of nano-hexagonal boron nitride (BN) with ethylene-vinyl acetate copolymer (EVA) by hydroxylation and amination, and then uses a solvent blending method to composite BN-NH2 and EVA in xylene to prepare the BN@EVA pour point depressant. The mass fraction of BN in the composite pour point depressant is 1-3 wt%, with an optimal value of 2 wt%. When the addition amount is 500 mg / kg, the pour point of crude oil can be significantly reduced from 19℃ to -7℃, a reduction of 26℃. FT-IR and SEM characterization confirmed that BN was successfully modified and uniformly dispersed in the EVA matrix; DSC curves showed a decrease in crystallization temperature and a bimodal synergistic effect; microscopic observation showed that the wax crystal morphology changed from a dense network to a dispersed spherical shape, effectively improving low-temperature fluidity. This invention has the advantages of good pour point depressant effect, simple process, and low cost, and is suitable for the extraction and pipeline transportation of high-wax crude oil.

The application provides a cysteine grafted polyurethane, comprising a polyurethane backbone and cysteine grafted on the polyurethane backbone. The application also provides a preparation method of the cysteine grafted polyurethane, and a cysteine grafted polyurethane nanoparticle and a preparation method thereof. The cysteine grafted polyurethane and the nanoparticle thereof provided by the application can be used for non-surgical treatment of congenital subluxation of the lens, repair of the zonular ligament to reduce the degree of lens dislocation, long-term and local immune microenvironment remodeling through inherent biological activity of the material itself, inhibition of M1 macrophage polarization from the source of the pathological loop, inhibition of the NF-κB pathway and reduction of degradation of the ECM core structure protein (such as FBN1 and MFAP2) of the zonular ligament of the lens, thereby promoting the repair of the zonular ligament, and avoiding or reducing the risk related to surgery.

This invention relates to the field of nanomaterial synthesis, and particularly to an ultrafine MoO2 nanowire bundle exhibiting surface-enhanced Raman (SEPA) effect, its preparation method, and its applications. The preparation method includes the following steps: 1) A sol-gel reaction is carried out using P123, water, n-butanol, concentrated hydrochloric acid, and TEOS as raw materials. The reaction product is then heated and aged, followed by washing, filtration, drying, and calcination to obtain a hexagonal porous template. The aging temperature is 60–140°C. 2) Ammonium molybdate is dissolved in water and mixed with the template obtained in step 1). After stirring and standing, the mixture is dried for the first time, calcined under a hydrogen-containing inert atmosphere, and then the template is removed with hydrofluoric acid. After washing and a second drying, the final product is obtained. The ultrafine MoO2 nanowire bundle has a diameter of approximately 5 nm, a regular and controllable morphology, good repeatability and stability, and exhibits a strong localized surface plasmon resonance effect and outstanding SEPA effect.