The invention relates to the technical field of
amide compound
crystallization, in particular to a
crystallization process of N, 2, 3-trimethyl-2-
isopropyl butyramide, which comprises the following steps: S1, decoloring a produced N, 2, 3-trimethyl-2-
isopropyl butyramide crude product, concentrating under reduced pressure, cooling with
chilled water for the first time to crystallize, and stirring for 1-5 hours under the condition of heat preservation to obtain a pre-crystallized solution; s2, adding the pre-crystallized solution into an
alcohol solvent, carrying out secondary cooling
crystallization, and carrying out heat-preservation stirring for 1-3 hours, so as to obtain a wet product of N, 2, 3-trimethyl-2-
isopropyl butyramide; and S3,
drying the N, 2, 3-trimethyl-2-isopropyl butyramide wet product, so as to obtain an N, 2, 3-trimethyl-2-isopropyl butyramide
crystal finished product. According to the invention, the needle-shaped
crystal is obtained through a crystallization process, and the cross section area of the needle-shaped
crystal is relatively small, so that the contact area at the contact point of the crystal is obviously reduced, the interaction force between the crystals is reduced, and the possibility of
caking is reduced especially under a wet condition.