The invention relates to a method for preparing high-purity crystalline
flake graphite through two-stage low-temperature
roasting and water leaching. The method comprises the following steps: crushing natural crystalline
flake graphite raw ore with the
fixed carbon content of 60-95%, mixing the crushed natural crystalline
flake graphite raw ore with composite alkali according to a
mass ratio of
graphite to total alkali of 1: (1.5-3), heating to 300-500 DEG C in an
inert atmosphere, carrying out heat preservation for 1-4 h, carrying out furnace cooling, carrying out
water immersion and
solid-liquid separation at 40-90 DEG C in a
solid-
liquid ratio of 1: (20-100), and carrying out
solid-liquid separation to obtain the crystalline flake
graphite. The method comprises the following steps: mixing
graphite with
potassium pyrosulfate according to a
mass ratio of graphite to
potassium pyrosulfate of 1: (0.8-2.0), heating to 250-400 DEG C in an
inert atmosphere, carrying out heat preservation for 1-3 hours, cooling, carrying out
water immersion and solid-liquid separation, and
drying to obtain a high-purity graphite product. The method is simple and controllable in process, high in adaptability to raw materials and convenient for industrial application.