This invention discloses an apparatus and method for large-scale production of three-dimensional
graphene foam with controlled
pyrolysis temperature, relating to the field of carbon nanomaterial preparation technology. The apparatus comprises a
biomass feed
pyrolysis system, a purification
system, a
chemical vapor deposition (CVD) device, and an outlet
gas monitoring system, connected in sequence. This invention primarily addresses the problems of inaccurate
pyrolysis temperature control, low single-batch yield, and
high energy consumption in existing technologies. On one hand, the outlet
gas monitoring system provides real-time feedback on the composition of the
tail gas from the CVD process, dynamically and precisely controlling the
biomass pyrolysis temperature to directionally control product performance. On the other hand, by designing the
nickel foam substrate as a cylindrical or spiral roll, the space of the CVD
tube furnace is maximized, significantly increasing the single-batch yield and enabling large-scale production. This invention features a stable process, high efficiency, and low
energy consumption, making it suitable for large-scale industrial production of high-performance three-dimensional
graphene foam, with broad application prospects in
electrochemical energy storage,
thermal conductivity, and electrical
conductivity.