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1874 results about "Potassium iodine" patented technology

Potassium iodide is a chemical compound, medication, and dietary supplement. As a medication it is used to treat hyperthyroidism, in radiation emergencies, and to protect the thyroid gland when certain types of radiopharmaceuticals are used.

Preparation method of rare-earth element doped modified hollow microsphere bismuth oxyiodide photocatalyst

The invention relates to a preparation method of a rare-earth element doped modified hollow microsphere bismuth oxyiodide photocatalyst. The preparation method comprises the following steps: adding bismuth nitrate pentahydrate and nitrate of a rare-earth element into a solvent and sufficiently dissolving to obtain a bismuth nitrate solution containing the rare-earth element; under magnetic stirring, dropwise adding a potassium iodide solution at a uniform speed drop by drop; after finishing dropwise adding, continually carrying out the magnetic stirring to obtain a precursor solution; puttingthe precursor solution into a reaction kettle to react by adopting a solvothermal method; after finishing the reaction, cooling a product to room temperature and taking out the product; washing, drying in vacuum and grinding to obtain the rare-earth element doped modified hollow microsphere bismuth oxyiodide photocatalyst. The method provided by the invention is simple and feasible and has the characteristics of simple process, good experiment reproducibility, low production cost and the like; the prepared rare-earth element doped composite photocatalyst has good photocatalytic degradation performance on organic pollutant and a good application prospect.
Owner:DONGHUA UNIV

Gold nanoparticle triangular plate preparing method and method for preparing gold nanoparticle discs and gold nanoparticle hexagonal pieces on basis of gold nanoparticle triangular plate preparing method

The invention provides a gold nanoparticle triangular plate preparing method and a method for preparing gold nanoparticle discs and gold nanoparticle hexagonal pieces on the basis of the gold nanoparticle triangular plate preparing method, relates to the technical field of gold nanoparticle preparing, and aims at providing the method which is easy and convenient to operate, high in repeatability and efficiency and is used for preparing gold nanoparticle triangular plates, gold nanoparticle discs and gold nanoparticle hexagonal pieces. The gold nanoparticle triangular plate preparing method includes the steps of preparing a gold nanoparticle seed solution through a sodium citrate aqueous solution, a tetrachloroauric acid aqueous solution and a sodium borohydride aqueous solution, preparing a gold nanoparticle triangular plate solution through the preapraed seed solution, a cetyl trimethyl ammonium bromide aqueous solution, a tetrachloroauric acid aqueous solution, a potassium iodide or sodium iodide aqueous solution, a sodium hydroxide aqueous solution and a ascorbic acid aqueous solution, and obtaining gold nanoparticle triangular plates after the liquid supermatant is abandoned. The method is easy and convenient to operate and high in repeatability and controllability, the prepared gold nanoparticle plates are unified in size, gold nanoparticle plates of different types and sizes can be synthesized, and the purity reaches 95% or higher.
Owner:NANOSEEDZ

Preparation method of acidizing corrosion inhibitor in high-temperature and concentrated acid environment

The invention relates to a preparation method of acidizing corrosion inhibitor in a high-temperature and concentrated acid environment. The preparation method is used for an acidification technology in carbonate oil reservoir exploration and overcomes the problem that existing high-temperature acidification corrosion inhibitor is poor in solubility and dispersion in use and prone to coking. According to the technical scheme, firstly, formaldehyde, benzene methanamine, absolute ethyl alcohol and concentrated hydrochloric acid are added into a three-necked flask, and then the three-necked flask is placed into an oil bath pan with the temperature being 110 DEG C for conducting a reaction for 2 hours; then, acetophenone is added, the pH is adjusted to 4 through concentrated hydrochloric acid, a reaction is conducted for 4 hours, and a coarse mannich base is obtained; thirdly, a vacuum rotary evaporation instrument is utilized for purification, separation is conducted, and a mannich base intermediate is obtained; fourthly, after the intermediate obtained in step 3 is washed, benzyl chloride is added, a reaction is conducted for 6 hours at the temperature of 110 DEG C, evaporation and separation are conducted through the vacuum rotary evaporation instrument, and mannich base quaternary ammonium salt is obtained; finally, potassium iodide is added in the mannich base quaternary ammonium salt stirring process for conducting mixed distribution, and the high-temperature acidizing corrosion inhibitor is obtained. The acidizing corrosion inhibitor has good solubility and dispersion, can further improve corrosion inhibition efficiency and is good in stability.
Owner:SOUTHWEST PETROLEUM UNIV
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