The invention relates to a testing method for measuring the content of
metal elements in a chlorinated
butyl rubber plug, and belongs to the technical field of chlorinated
butyl rubber plug testing. Comprising the following steps: S1,
cutting a rubber plug into pieces, S2, adding concentrated
sulfuric acid, S3, putting the rubber plug into a
muffle furnace, S4, setting the temperature of the
muffle furnace, S5, heating and cooling the
muffle furnace, S6, observing an
ashing state, S7, carrying out secondary
ashing, S8, transferring a sample to a constant volume, S9, transferring the sample to a constant volume, and S10, carrying out measurement on a
machine. Volatile
metal chlorides and oxides are converted into sulfates with stable chemical properties by concentrated
sulfuric acid, and the sulfates are not volatile or decomposed even at the high temperature of 600 DEG C, so that the total amount of
metal elements is completely locked; according to the present invention, the accurate
ashing at 600 DEG C can completely remove the
organic matrix, the interference of the
organic matter is avoided, the loss of the metal element is ensured, the determination value of the same standard rubber sample is 0.048-0.052 mg / kg, and the accuracy is significantly improved.