The invention relates to a preparation method of a homogenized fine nano-
cellulose fiber. The preparation method can solve the problems of uniform
diameter distributor of
biomass nano-
cellulose prepared by the existing strong
acid hydrolysis method and the high-strength mechanical shearing method, easy gathering among the nano-
fiber and a
narrow range of applications of the TEMPO
catalytic oxidation method. The preparation method comprises the following steps: 1) extracting
biomass fiber with
benzyl alcohol solution; 2) carrying out treatment by using acidified
sodium chlorite; 3) carrying out gradient treatment with alkaline liquor; 4) using TEMPO,
sodium bromide and
sodium hypochlorite for
catalytic oxidation treatment; 5) using
sodium chlorite for treatment; and 6) carrying out nano-scale
processing by using the long-term stirring method, the ultrasonic method or the high-pressure homogenization method,
drying, and then obtaining the homogenized fine nano-
cellulose fiber. The fiber has the uniform
diameter distribution, the
diameter is 3-5nm, the length-
diameter ratio is not less than 500, the fiber is mutually interwoven into a mesh snarling structure, and the method is applicable to preparing the nano-
cellulose fiber by using wood pulp, paper-making pulp, wood, bamboo and
crop straw.