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47results about How to "Suppressed ionization" patented technology

Flaky iron phosphate, and preparation method and application thereof

ActiveCN110357057AModerate particle size distributionEasy to processPhosphorus compoundsPhosphoric acidSlurry
The invention discloses flaky iron phosphate, and a preparation method and application thereof. The microscopic morphology of the flaky iron phosphate is a primary particle in a sheet shape with a thickness of 10 to 50 nm, a length of 100 nm to 3 [mu]m and a width of 100 nm to 3 [mu]m. The preparation method comprises the following steps of: weighing a ferrous ion solution and adding phosphoric acid and a crystal modifier; weighing a phosphorus salt solution and adding an oxidizing agent; carrying out mixing to obtain a mixed solution C, controlling the pH value of the mixed solution C to be 1.5-2.2, and carrying out a reaction to obtain pale yellow iron phosphate slurry; converting the iron phosphate slurry into white or pink-white iron phosphate slurry containing crystal forms under theconditions of stirring and heating, reducing a stirring speed by 20%-50% after the completion of the conversion, and carrying out ageing and heat preservation; performing solid-liquid separation, andcollecting a solid portion to obtain a crystalline iron phosphate precipitate; and washing the precipitate and then performing calcination to obtain the flaky iron phosphate. The iron phosphate of theinvention can be used for preparing lithium iron phosphate with high compaction density.
Owner:HUNAN YACHENG NEW MATERIAL CO LTD

High-concentration wastewater resource utilization method

The invention discloses a high-concentration wastewater resource utilization method. The high-concentration wastewater resource utilization method comprises the following steps: adding a cation exchanger in wastewater, and carrying out stirring reaction to enable extractable substances in the wastewater to be exactly condensed into insoluble fine and small solid particles; separating out the cation exchanger, slowly adding a proper amount of chemical agent in the wastewater to generate small air bubbles, and enabling the air bubbles to adhere to the fine and small solid particles in the wastewater so as to reduce viscosity of the wastewater; heating to the temperature which is higher than a connecting material softening point by 0-30 DEG C, and enabling the fine and small solid particles to adhere to one another so as to form large-particle solids; carrying out insulation treatment for a certain time so that a blocky extract is formed; cooling the extract with a saturated potassium hydroxide solution; and carbonizing and activating the pulverized and dried blocky extract at one step for 1-4 h at the temperature of 700 DEG C under the protection of nitrogen, and breaking the blockyextract to obtain an adsorbent. The adsorption capacity of the adsorbent prepared by the method to cationic dyestuff can reach 450 mg / g or above.
Owner:QINGDAO UNIV

High-concentration wastewater pollutant extracting and utilizing method

The invention discloses a high-concentration wastewater pollutant extracting and utilizing method. The high-concentration wastewater pollutant extracting and utilizing method comprises the following steps: adding a proper amount of cation exchange material in wastewater, and carrying out stirring reaction to enable an extractable substance in the wastewater to be exactly condensed into insoluble fine and small solid particles; separating out the cation exchange material, adding a proper amount of chemical agent in the wastewater while stirring to generate small air bubbles, and enabling the air bubbles to adhere to the fine and small solid particles in the wastewater so as to reduce viscosity of the wastewater; carrying out ultrasonic treatment, heating to the temperature which is higher than a connecting material softening point by 0-20 DEG C, and enabling the fine and small solid particles to adhere to one another so as to form large-particle solids; carrying out ultrasonic insulation treatment for a certain time so that a blocky extract is formed; cooling the extract with a saturated potassium hydroxide solution; and carbonizing and activating the dried blocky extract at one step for 1-4 h at the temperature of 700 DEG C under the protection of nitrogen, and breaking the dried blocky extract to obtain an adsorbent. The adsorption capacity of the adsorbent prepared by the method to cationic dyestuff can reach 450 mg / g or above.
Owner:QINGDAO UNIV

Sample processing method for determining residual lithium salt on surface of battery shell in flame atomic absorption spectroscopy method

The invention discloses a sample processing method for determining residual lithium salt on a surface of a battery shell in a flame atomic absorption spectroscopy method. The method comprises the following steps: cleaning and extracting the surface of a battery shell by using dimethyl carbonate, continuously performing ultrasonic immersion for a battery eluted by the dimethyl carbonate by using a nitric acid solution to extract the lithium salt, concentrating a dimethyl carbonate extract solution, adding a nitric acid solution, performing oscillation extract, and transferring a nitric acid phase into the nitric acid extract solution; heating to remove the acid, transferring the residual solution into a volume bottle after the acid removal, adding 1ml of 1 percent cesium chloride, fixing the volume by using deionized water to obtain a solution to be detected; and performing the blank treatment by adopting a same method, and determining the sample to be detected and the blank sample by directly using the flame atomic absorption spectroscopy method. By adopting a combined pretreatment means for dissolving the residual lithium salt on the surface of the battery shell by using the dimethyl carbonate and the nitric acid solution, and the lithium salt in the dimethyl carbonate is extracted into the nitric acid solution by using a liquid-liquid extraction method, so that the interference of organic solvents is effectively avoided.
Owner:HEFEI GUOXUAN HIGH TECH POWER ENERGY

Dephenolization extraction agent as well as preparation method and application thereof

The invention provides a dephenolization extraction agent as well as a preparation method and application thereof. The dephenolization extraction agent comprises a combination of methyl isobutyl ketone, a synergistic extraction agent and an antioxidant, wherein the antioxidant comprises C6-C9 saturated aliphatic ketone and/or C7-C9 saturated aliphatic alcohol. According to the dephenolization extraction agent, through compounding of specific components, on one hand, synergistic interaction is achieved on the dephenolization efficiency, on the other hand, ionization and oxidation of phenolic substances in the extraction process can be effectively inhibited, and the content of pollutants such as phenoxy anions, quinones and derivatives thereof which are higher in removal difficulty and higher in toxicity in wastewater is remarkably reduced. The dephenolization extraction agent is used for treating phenol-containing wastewater, the volume ratio range and the pH application range are wide, industrial operation is easy to achieve, the extraction efficiency of monohydric phenol and polyhydric phenol is high, the single-stage total phenol extraction efficiency reaches 97.4% or above, the concentration of an oxidation product benzoquinone in the extracted wastewater is extremely low, the biotoxicity of the wastewater is reduced, and the subsequent biochemical treatment is facilitated.
Owner:INST OF PROCESS ENG CHINESE ACAD OF SCI

Method for measuring urotropine content of rice and flour and rice-flour product

The invention provides a method for measuring urotropine content of rice and flour and a rice-flour product. The method comprises the following steps: 1, making a product to be measured into a sample;2, weighing the sample to a centrifuging tube, adding ammonium acetate for performing ultrasonic extraction and centrifuging, and placing supernatant into a volumetric flask; 3, continuously adding the ammonium acetate into the centrifuging tube, performing ultrasonic extraction and centrifuging, placing the supernatant into the volumetric flask used in step 2, and metering the volume of the supernatant to 10 mL with the ammonium acetate to obtain a clear sample liquid; 4, performing filtering with a water-phase microfiltration membrane to obtain a sample liquid to be measured; 5, measuring peak areas of a urotropine standard working liquid and the sample liquid to be measured with an efficient liquid phase chromatograph to obtain a standard curve equation; 6, calculating the urotropine content in the product to be measured. The method has the characteristics of high urotropine extraction efficiency, easiness in operation, high accuracy, high stability and high repeatability, so thata stable and reliable method for detecting urotropine in the rice-flour product is provided.
Owner:GUANGZHOU INST FOR FOOD INSPECTION(GUANGZHOU INSPECTION CENT FOR WINE & SPIRITS)
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