The invention relates to the technical field of nano
cerium oxide production, in particular to a self-collision dispersion process without destroying the morphology of nano
cerium oxide, which comprises the following steps: S1, material pretreatment: S1.1,
impurity removal treatment: according to production requirements, obtaining a
cerium carbonate / cerium
silicate raw material, then crushing the cerium
carbonate / cerium
silicate raw material by air flow until D50 is 3-5 microns, then putting into a
nitric acid solution for ultrasonic cleaning, and
drying to obtain a
cerium oxide / cerium
silicate powder; neutralizing with
ammonia water until the pH value is 6.0 + / -0.5, centrifugally separating, weighing the material, and ensuring that the purity of the cerium compound in the
raw material is greater than or equal to 99.9%; according to the method, the dispersing-
drying-magnetizing-calcining multi-stage joint control technology is adopted, the technological process is shortened, the efficiency is improved, the
viscosity of homogeneous
slurry is controlled through high-speed dispersing and synchronous stepped
vacuum drying, secondary agglomeration is avoided, segmented calcining is combined with
nitrogen-
hydrogen mixed gas and the nucleating agent,
lattice defects can be reduced,
energy consumption can be reduced, and the method is suitable for large-scale production. Automatic parameter matching is achieved through
magnetic field-flow velocity formulation linkage, the
impact precision is improved, and the process stability is remarkably improved.