776results about "Distillation in boilers/stills" patented technology

A process arrangement for distilling fuel grade ethanol includes a fermentation portion, a distillation portion, a condensation and dehydration portion, a separation and drying portion and an evaporation portion. The fermentation portion produces beer. The distillation portion, the condensation and dehydration portion and the separation and drying portion receives beer from the fermentation portion and produces hot ethanol vapor and thin stillage. In the evaporation portion, a set of first effect evaporators which are heated either by plant steam or hot ethanol vapor, concentrate thin stillage into mid stillage while producing first effect steam. The first effect steam from the first effect evaporators provides heat to a set of second effect evaporators which concentrate the mid stillage into a syrup for further drying. The second effect evaporators produce second effect steam which is used to heat the distillation portion of the process arrangement. The multiple evaporators of the first and second effects of the evaporation portion can be selectively taken off-line for maintenance while the evaporation portion and the remainder of the process arrangement continue to operate at full capacity.

A desalination apparatus capable of obtaining fresh water stably at low cost by utilizing low-temperature waste, wherein the desalination apparatus including a heat exchanger 92 cooperating with an evaporation can 60 so as to subject a low-temperature waste heat 11 and raw water 62 in the evaporation can 60 to heat exchange and generate water vapor 63 in the evaporation can 60; a condenser 98 cooperating with a raw water tank 72 so as to receive the water vapor 63 from the evaporation can 60, cool the water vapor 63 by subjecting the water vapor 63 and raw water 71 in the raw water tank 72 to heat exchange and obtain distilled water 76; a distilled water tank for storing the distilled water 76; vacuum means for evacuating the evaporation can 60 and depressurizing the inside thereof so as to promote generation of water vapor 63 in the evaporation can 60; and raw water supply means for supplying raw water to the evaporation can.

Apparatus and process are disclosed for the distillation separation of styrene monomer from ethylbenzene utilizing a split feed to two distillation columns in conjunction with cascade reboiling utilizing thermal energy from the overhead of one column to supply heat to the second.

The present invention relates to a system for producing ethanol from an organic source and that operates to purify and dry ethanol from a beer source. The system for producing substantially anhydrous ethanol comprises: (a) a first distillation stripping column that operates between 160 to 220 degrees F.; (b) a second distillation rectifying column having a higher operating temperature than said stripping column; (c) a molecular sieve dehydration means in fluid communication with said rectifying column; and (d) an energy control means.

Systems and methods for separating an alcohol, and in particular butanol, from a fermented feed and concentrating thin stillage into syrup includes operation of one or more alcohol recovery distillation columns using the heat supplied by steam generated from concentration of the thin stillage in a multi-train, multi-effect evaporation system.

A heat sink or heat transfer device particularly for integrated circuits, uses a phase change working fluid in a cyclic flow path having at least one evaporator that serves multiple heat sources. The evaporator can be an integral vessel made of thermally conductive material to which the multiple heat sources are coupled, preferably at evaporation points that are placed on opposite sides of a fluid reservoir for the liquid phase of the working fluid that feeds the evaporation points via capillary flow through a picking material.

A process is disclosed for recovering 1-butene from a feed steam comprising n-butane, isobutane and butene isomers using a single, divided wall distillation column. The disclosed process includes introducing the feed steam into an inlet of a first side of a distillation column, wherein the distillation column comprises a top, a bottom and a center dividing wall extending between the bottom and the top of the column and dividing the column into the first side and a second side. The process includes taking off an isobutane stream from the top of the second side of column, taking off a 1-butene stream as a bottoms stream from the second side of the column, and taking off a combination 2-butene and n-butane stream as a bottom stream from the first side of column.

The present invention in a first aspect provides a method and a system for stripping volatile compounds such as ammonia from e.g. fermentation liquids. Part of the ammonia is stripped from the liquid in a stripper system comprising a shunt through which liquid such as e.g. fermentation medium comprising a biomass can be diverted in the form of a side stream in liquid contact with a main fermentor(s). The stripper system is connected to an evaporator. In the evaporator aqueous liquid is heated at a pressure below atmospheric pressure whereby vapour is developed at a temperature below 100° C. The vapour from the evaporator is directed to the liquid medium comprising ammonia and this results in ammonia being stripped from the liquid and transferred to the vapour phase. The vapour phase is condensed in a first condenser at a low pressure, e.g. a pressure well below 1 bar, and the liquid thus obtained is further treated in a stripper unit at a higher pressure, such as e.g. a pressure at or above 1 bar, to obtain a more concentrated solution of ammonia. When stripped for at least part of the ammonia the liquid initially obtained from the biogas reactor and diverted to the shunt can be returned to the reactor.

A system and process for the recovery of oil from the pyrolysis of material containing hydrocarbons such as shredded vehicle tires. The system utilizes a pair of sequentially positioned packed towers to recover at least 95% of the oil contained in the pyrolysis gases. The first packed tower operates above the dew point of the water vapor in the pyrolysis gases to insure that no water is condensed and obtain a primary oil fraction having oil with a high flash point of about 60° C. or greater and a primary vapor fraction containing additional oils, fuel gases and water vapor. The primary vapor fraction is fed to the second packed tower which operates below the dew point of the water vapor to condense the water and oil having a low flash point of 34° C. or below, and provide a secondary vapor fraction containing valuable fuel gases.

In accordance with particular embodiments, a desalination system includes a plurality of evaporators. The plurality of evaporators includes at least a first evaporator and a last evaporator. The plurality of evaporators are arranged in cascading fashion such that a concentration of salt in a brine solution increases as the brine solution passes through the plurality of evaporators from the first evaporator towards the last evaporator. The desalination system also includes a plurality of heat exchangers. An input of each evaporator is coupled to at least one of the plurality of heat exchangers. The system also includes a vapor source coupled to at least one of the plurality of evaporators.

The salt water distillation system includes a sprinkler to form a mist of salt water over a distillation plate. The distillation plate is heated by applying electrical current to a heating coil. The steam is transferred to a condensation chamber and condensed fresh water is collected. During the desalination process, salt impurities are deposited on the hot distillation plate. A sludge remover, i.e., a steam head and movable ram, is provided to clean the distillation plate of the salt impurities. An exhaust fan is provided to cool fresh water condensate and lower air pressure in the system. Heat transferred from the steam during condensation is used to pre-heat the salt water to increase efficiency of the system.

A novel apparatus for producing sweet synthetic crude from a heavy hydrocarbon feed comprising: an upgrader for receiving said heavy hydrocarbon feed and producing a distillate fraction including sour products, and high-carbon content by-products; a gasifier for receiving the high-carbon content by-products and producing synthetic fuel gas and sour by-products; a hydroprocessing unit for receiving the sour by-products and hydrogen gas, thereby producing gas and sweet crude; and a hydrogen recovery unit for receiving said synthetic fuel gas and producing further hydrogen gas and hydrogen-depleted synthetic fuel gas, said further hydrogen gas being supplied to said hydroprocessing unit.

Turbulent mixing condensation devices, methods, and systems adapted to condense a working fluid on particles from a sample gas to enlarge the particles for subsequent detection are provided. The device includes a vapor generator adapted to produce a working-fluid saturated carrier gas and a condensation chamber. The working-fluid saturated carrier gas is mixed with a sample gas containing particles to be detected and is then introduced to the condensation chamber. The operating conditions are controlled to enhance the condensation of the working fluid on the particles. The particles are typically forwarded to a particle detection device to detect at least one characteristic, for example, the size, of the particles. The flow of carrier gas to the vapor generator may be regulated to vary the degree of saturation of the carrier gas with working fluid.

A system and method of producing a blended extract of cannabinoids and terpenes, which extracts terpenes using supercritical CO2, and extracts a cannabinoid concentrate from the residual material using a cold ethanol flush followed by distillation; the CO2-extracted terpenes are then added back to the cannabinoid concentrate in a final blending step. Blending terpenes at the end of extraction may enhance the flavor and effectiveness of the cannabinoid concentrate. By separately extracting terpenes and cannabinoids, optimal processes and parameters may be used for each step. Blending may combine terpenes and cannabinoids in any desired ratio; for example, a terpene-to-cannabinoid ratio of approximately 1:10 may be used. The ethanol used in the cold ethanol extraction of cannabinoids may be recovered and reused for subsequent batches. Cannabinoid concentrates may be redistilled multiple times to enhance their concentration, followed by terpene blending.

A system for producing a blended extract of cannabinoids and terpenes, which extracts terpenes using supercritical CO2, and extracts a cannabinoid concentrate from the residual material using a cold ethanol flush followed by distillation; the CO2-extracted terpenes are then added back to the cannabinoid concentrate in a final blending step. Blending terpenes at the end of extraction may enhance the flavor and effectiveness of the cannabinoid concentrate. By separately extracting terpenes and cannabinoids, optimal processes and parameters may be used for each step. Blending may combine terpenes and cannabinoids in any desired ratio; for example, a terpene-to-cannabinoid ratio of approximately 1:10 may be used. The ethanol used in the cold ethanol extraction of cannabinoids may be recovered and reused for subsequent batches. Cannabinoid concentrates may be redistilled multiple times to enhance their concentration, followed by terpene blending.

A method and apparatus for separating draw solution solutes and product solvent from a draw solution using a plurality of distillation columns. In one embodiment, the draw solution is used in a Forward Osmosis (FO) water desalination process. In this embodiment, the draw solution is directed to the plurality of distillation columns in parallel while the energy stream (heat) is directed to the plurality of distillation columns in series such that the efficiency of heat use is improved and in turn the cost of the heat is reduced.

The solar-powered humidification-dehumidification desalination system includes a supply of saline / brackish water passing through a dehumidifier / condenser. The saline / brackish water is preheated in the dehumidifier / condenser due to the condensation process. A plurality of humidifying stages includes respective humidifiers and respective solar collectors. The solar collectors heat air, and the heated air passes through respective humidifiers to evaporate the preheated saline / brackish water, separating pure water from the brine. The humid air is reheated and recirculated through the humidifying stages and the dehumidifier, and the desalinated water from the dehumidifier via condensation is collected to and processed. The system recirculates the brine successively from each humidifier to the next for more efficient evaporation and less energy consumption.

The present invention relates to a system for producing ethanol from an organic source and that operates to purify and dry ethanol from a beer source. The system for producing substantially anhydrous ethanol comprises: (a) a first distillation stripping column; (b) a second distillation rectifying column having a higher operating temperature than said stripping column; (c) a molecular sieve dehydration means in fluid communication with said rectifying column. Heat from the overhead of the second distillation rectifying column and the molecular sieve dehydration are used to heat the first distillation stripping column.

A method and system for treating feedwater includes evaporating a portion of the feedwater in a first evaporation chamber so as to separate water vapor from the remaining feedwater. Droplets of the remaining feedwater are dispersed into a stream of hot air produced in a second evaporation chamber. The droplets evaporate and solids in the feedwater precipitate. The precipitated solids are collected in the lower section of the second evaporation chamber. Water vapor discharged from both evaporation chambers can be treated in a cyclone separator to remove residual solids therefrom. The cleansed water vapor output from the cyclone separator can be condensed to recover clean water. Dry solids can be discharged from the second evaporation chamber and the cyclone separator for recovery.

A system for recovering glycol from glycol and brine mixtures produced from oil or natural gas wells that combines energy efficiency with a capability for handling salt and other solids contained in the mixture. The system comprises three effect evaporator systems in series. Each effect evaporator system comprises an evaporator, a separator vessel, product pumps, and a solids removal system.The process utilizes the system to remove salt and other solids as well as excess water leaving a glycol stream that can be reused as a hydrate inhibitor. The process begins by preheating a glycol / brine stream comprising approximately fifty percent (50%) glycol. The stream is then subjected to three evaporation cycles. The first evaporation cycle comprises introducing the preheated stream into a suppressed boiling point evaporator where the stream is heated under a constant pressure. The stream pressure is then dropped to cause a portion of the water contained in the stream to vaporize or flash. The flashing stream is then introduced into a separator vessel where the water vapor is separated from the remaining liquid stream. The water vapor is removed from the separator and condensed. The remaining liquid glycol / brine stream is then pumped from the separator vessel through a solids removal system where precipitated salts and solids are removed. These steps are repeated two additional times. Each time the remaining liquid stream becomes more concentrated with glycol until the finished product is approximately ninety percent (90%) glycol.

A large and economical type of multi-stack vertical tube evaporator (MS-VTE) is disclosed having units of multiple stacks of vertical tube bundles or stages mounted in a single vessel, and having its liquid feed pumped to the uppermost VTE bundle stack or stage and having the feed then cascading downward through the lower bundle stacks in series flow, and wherein all the tube bundles are heated with the same waste steam of no or low $-value, e.g. with turbine reject steam in parallel flow under vacuum into the steam-sides of all tube bundles in the unit through a common steam conduit; and wherein the feed liquid is progressively evaporated from stage to stage or stack to stack and the vapors produced in the tubes of each bundle during the partial evaporation of the feed are separated between the stacks and condensed by parallel flow into one or more condensers. Applied to seawater desalination in a co-generation procedure with a coastal power plant, this evaporator produces about one pound of distilled water per pound of turbine reject steam used under vacuum and applied to single-effect mode in one evaporator unit or several units mounted in a single vessel with a condenser, to substantially reduce the cost of such useful distilled water. When applied in a similar cogeneration procedure but in a multi-effect series mode of several such units, or multiple units, the rate of distilled water production can be increased several-fold based on the amount of turbine reject steam applied.

A method and apparatus for desalinating water combined with power generation, comprising a desalination system used for desalinating coastal seawater and comprising a power generation system, wherein such dual purpose co-generation facility captures the heat vapor exhausted or a steam turbine generator's condenser is replaced by the desalination plant's heat exchanger enabling such captured heat energy to reduce the energy requirements of the desalination plant, and wherein brine solution being treated by the desalination plant is pumped from the substrata sea water table wells having low salt content brackish water.

System and process for producing no-salt water by desalination of salt water, by heating salt water directly with heated synthetic gas produced in a gasification reaction or by using steam produced using heated synthetic gas, to evaporate the salt water and produce no-salt water.

According to one embodiment of the invention, a vapor-compression evaporation system includes a plurality of vessels in series each containing a feed having a nonvolatile component, a mechanical compressor coupled to the last vessel in the series and operable to receive a vapor from the last vessel in the series, a pump operable to deliver a cooling liquid to the mechanical compressor, a tank coupled to the mechanical compressor and operable to separate liquid and vapor received from the mechanical compressor, a plurality of heat exchangers coupled inside respective ones of the vessels, the heat exchanger in the first vessel in the series operable to receive the vapor from the tank, at least some of the vapor condensing therein, whereby the heat of condensation provides the heat of evaporation to the first vessel in the series, and wherein at least some of the vapor inside the first vessel in the series is delivered to the heat exchanger in the next vessel in the series, whereby the condensing, evaporating, and delivering steps continue until the last vessel in the series is reached.

According to one embodiment of the invention, a vapor-compression evaporation system includes a plurality of vessels in series each containing a feed having a nonvolatile component, a mechanical compressor coupled to the last vessel in the series and operable to receive a vapor from the last vessel in the series, a pump operable to deliver a cooling liquid to the mechanical compressor, a tank coupled to the mechanical compressor and operable to separate liquid and vapor received from the mechanical compressor, a plurality of heat exchangers coupled inside respective ones of the vessels, the heat exchanger in the first vessel in the series operable to receive the vapor from the tank, at least some of the vapor condensing therein, whereby the heat of condensation provides the heat of evaporation to the first vessel in the series, and wherein at least some of the vapor inside the first vessel in the series is delivered to the heat exchanger in the next vessel in the series, whereby the condensing, evaporating, and delivering steps continue until the last vessel in the series is reached.

A rotary multi-stage distiller for recovery of water from wastewater is provided. The rotary multi-stage distiller of the present invention can recover water from a wide variety of aqueous wastewaters such as, but not limited to, urine, condensate from air conditioning systems, wash water containing foaming soaps, seawater or polluted water. The multi-stage distiller can operate under vacuum conditions permitting the distillation to occur at low temperatures. The multi-stage distiller uses centrifugal forces for fluid pumping and for vapor / liquid separation. The multi-stage distiller comprises hydraulic seals for each stage which eliminate contamination of clean, recovered water by condensed waste water during the regeneration process. The multi-stage distiller also comprises a stationary shaft of stacked segments where each segment is associated with an individual stage of the multi-stage distiller. The number of stages therefore, of the multi-stage distiller of the present invention can be readily adjusted as needed by either adding a segment with a stage to the stationary shaft or removing a segment of the shaft with a stage to decrease the number of stages.

This invention describes a low temperature, self-sustainable desalination process operated under natural vacuum conditions created and maintained by barometric pressure head.

A heat sink or heat transfer device particularly for integrated circuits, uses a phase change working fluid in a cyclic flow path having at least one evaporator that serves multiple heat sources. The evaporator can be an integral vessel made of thermally conductive material to which the multiple heat sources are coupled, preferably at evaporation points that are placed on opposite sides of a fluid reservoir for the liquid phase of the working fluid that feeds the evaporation points via capillary flow through a picking material.