The invention discloses a research method and a
solvent recovery device for an automotive scratch-resistant
epoxy polysiloxane assistant, and belongs to the technical field of automotive interior material assistants.The research method comprises the steps that S1, an earlier-stage
preparation stage is conducted, specifically, allyl butyl
glycidyl ether (the
epoxy equivalent is 230-250 g / eq), C12-C18
epoxy-terminated olefin,
hydrogen-containing polysiloxane (the
hydrogen content is 0.12-0.15 wt%) and a
platinum catalyst (3-5 ppm) are prepared; s2, an auxiliary agent synthesis and
solvent recovery stage: introducing
nitrogen into the reaction kettle to form a protective
atmosphere, adding allyl butyl
glycidyl ether accounting for 60% of the total amount, and starting a stirring device to enable the allyl butyl
glycidyl ether to be uniformly distributed; after the reaction is finished, detecting that the free epoxy value of a product is greater than or equal to 95%, feeding the product into a film
evaporator, removing low-boiling-point substances under the condition of 120 DEG C / 5kPa until volatile components are less than or equal to 0.8% to obtain an epoxy polysiloxane auxiliary agent, purging equipment by using
nitrogen after the
recovery is finished, and regularly
pickling a condenser
pipe for maintenance; the method has the technical effects that the
surface energy and the
friction coefficient of the material are optimized at the same time, and the
solvent recovery efficiency is high.