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80results about How to "Meet high-end needs" patented technology

Polysiloxane, glycidol and quaternary ammonium salt-containing multifunctional gelatin leather finishing agent and preparation method

The invention relates to a polysiloxane, glycidol and quaternary ammonium salt-containing multifunctional gelatin leather finishing agent and a preparation method. The preparation method comprises the following steps: dissolving gelatin in water to prepare aqueous solution with mass concentration of 2-20 percent; adding epoxy quaternary ammonium salt into a first reaction flask under the conditions of temperature of 40-70 DEG C and pH of 6-12 to obtain solution 1; adding glycidol into a second reaction flask to obtain solution 2; adding a surfactant into a third reaction flask, and meanwhile adding Si-O-Si repetitive unit-containing epoxypolysiloxane in batches or continuously to obtain solution 3; mixing the solution 1, the solution 2 and the solution 3 in different proportions, weighing 15-20 g of the mixed solution to be placed in a mold of polytetrafluoroethylene, adding 5-10 mL of one or three or four of ethanol, tetrahydrofuran, acetone and methanol and drying in a normal pressure drying oven at the temperature of 40-80 DEG C to obtain the multifunctional gelatin leather finishing agent. The finishing agent has the characteristics of strong hydrophobicity, flexible film, antibacterial property, high heat stability, organic solvent resistance, wet scrubbing resistance and the like.
Owner:山东山科美谷科技发展有限公司

Polysiloxane and glycidol-containing strong-hydrophobicity gelatin leather finishing agent and preparation method

The invention relates to a polysiloxane and glycidol-containing strong-hydrophobicity gelatin leather finishing agent and a preparation method. The preparation method comprises the following steps: dissolving gelatin in water to prepare aqueous solution with mass concentration of 2-20 percent; adding glycidol into a first reaction flask under the conditions of temperature of 40-70 DEG C and pH of 6-12 to obtain solution 1; adding a surfactant into a second reaction flask, continuously stirring, and meanwhile adding Si-O-Si repetitive unit-containing epoxypolysiloxane in batches or continuously to obtain solution 2, wherein the using amount of the surfactant is 0.5-20 percent of the mass of the gelatin; mixing the solution 1 and the solution 2 in different proportions, weighing 15-20 g of the mixed solution to be placed in a mold of polytetrafluoroethylene, adding 5-10 mL of one or two or three of ethanol, tetrahydrofuran and methanol and drying in a normal pressure drying oven at the temperature of 40-80 DEG C to obtain the gelatin leather finishing agent with a superior function. The finishing agent has the characteristics of strong hydrophobicity, super extensibility, heat resistance, oxidation resistance, wet scrubbing resistance and the like.
Owner:QILU UNIV OF TECH

Mild makeup removing mousse and preparation method thereof

The invention discloses mild makeup removing mousse and a preparation method thereof. The mousse is prepared from the following components in percentage by weight: 30 to 70 percent of a solvent, 5 to30 percent of a propellant, 2 to 10 percent of an emulsifier, 2 to 15 percent of a skin moistening agent and 0.01 to 28 percent of a skin conditioning agent. The preparation method comprises the following steps: mixing the solvent with the emulsifier and part of the skin moistening agent and stirring until the materials are uniformly dispersed and dissolved; while stirring, adding the residual skin moistening agent and the skin conditioning agent; uniformly stirring until the materials are completely dispersed and dissolved to form material liquid; packaging the material liquid through an aerosol can and filling with the propellant; detecting that a product is qualified. According to the mild makeup removing mousse disclosed by the invention, a grease raw material is combined with aerosolpackaging and a unique emulsifying system; a material body is shown in a dense and elastic form; the mild makeup removing mousse has the advantages of no additives, easiness for washing and no residues; the dense makeup removing oil mousse can enter pores to dissolve makeup powder in the pores, so that a face is cleansed, and the makeup is more completely removed; the mild makeup removing mousse is convenient to use and easy to carry.
Owner:ZHONGSHAN TIANTU FINE CHEM CO LTD

Car active noise reduction method based on heuristic dynamic programming

The invention discloses a car active noise reduction method based on heuristic dynamic programming, and belongs to the field of active noise reduction methods of noise in car rooms. According to the car active noise reduction method, massive data in a large database of noise information in a virtual environment of a cloud server are initiatively fitted, the rule of noise frequency spectrum characteristics in the database is looked for through a model network and an execution network trained by heuristic dynamic programming, the noise data with the similar frequency spectrum characteristics arefitted together, an off-line expert library having the less data size and reduced and generated from a huge database is established, so that optimization of the noise data is achieved, and the optimal control quantity is provided for a system. According to the innovative mode, the method can overcome the drawback that an existing car active noise reduction method needs to conduct one-by-one real-time operation on the massive data, and through practical testing, the method can fully meet requirements of noise reduction of an actual traffic car under a real road condition, so that the car active noise reduction method has great market prospect and potential economic value.
Owner:长春一汽四环汽车管路有限公司

Preparation process of high-thermal-conductivity extruded aluminum alloy profile

ActiveCN110343884ASimple preparation processOptimizing aging process parametersSolution treatmentHardness
The invention discloses a preparation process of a high-thermal-conductivity extruded aluminum alloy profile. The preparation process comprises the following steps of 1) extrusion, 2) refining, 3) extruding, and 4) effectiveness and the like. An online air cooling technology is adopted, the process of solid solution treatment is omitted, so that the production efficiency is improved; and optimization is carried out on various parameters, especially effective parameters in the preparation process so as to obtain an optimal scheme. According to the preparation process, the formula of the aluminum alloy is improved, the content of Mg and Si in the aluminum alloy component is reduced, Mg / Si ratio is controlled, so that the type of the alloy is in a slightly excess type of Si, and the harmful effect of V is eliminated by adding the boron adding element. On the premise of keeping the hardness, the conductivity of the product is improved. Through verification, the vickers hardness of the product can reach more than 11 Hw or above, the tensile strength is higher than 215 Mpa, the electric conductivity at 20 DEG C is higher than 56% IACS, and the heat conductivity coefficient can reach 220W / mK or above, and all technical parameters reach the world leading level.
Owner:JIANGSU WEITENG COPPER CO LTD

Method for preparing diisopropanolamine

The invention relates to a method of manufacturing diisopropanolamine. Liquid ammonia and water are mixed to form ammonia water which is fully mixed with propylene oxide; the mixed solution is preheated until the temperature reach 140 to 145 DEG C and then is delivered into a reactor for reacting, the temperature is controlled within 148 to 155 DEG C when in reacting, the pressure is controlled within 16.0 to 18.0MPa, the inputting molar ratio of the ammonia and the propylene oxide is controlled within 5 to 8, and the reaction is fully performed for 1.5 to 3 hours; the mixture products obtained in the reaction are separated to obtain isopropanolamine products, diisopropanolamine products and triisopropanolamine products through flash evaporation and rectification in a stepwise way. In the diisopropanolamine products which are manufactured by adopting the method, the component of 1, 1<1>-nitrousalkyl-dipropyl-2-alcohol accounts for more than 99 percent (hereinafter referred to as mass percent), and the isomeride thereof is less than 1 percent. In addition, the cost of the production operation in the method is less, the production cost is low, the product quality is high, and the high-end requirement of products such as synthetic medicine, farm insecticide, etc. is satisfied.
Owner:NANJING BAOCHUN CHEMICAL INDUSTRY CO LTD

High-toughness heat-resistant Mg-Gd alloy suitable for gravity casting and preparation method thereof

The invention provides a high-toughness heat-resistant Mg-Gd alloy suitable for gravity casting and a preparation method thereof. The alloy comprises the following chemical components of, in percentage, 4.0-10.0% of Gd, 2.0-6.0% of Zn, 0.5-1.2% of Al, 0.1-0.3% of Mn, 0.01-0.08% of M, and the balance Mg, wherein the M is one or two elements of Ti and B; the preparation method comprises the following steps that (1) burdening is performed according to a Mg-Gd alloy component; (2) an industrial pure magnesium ingot is melted; (3) heating is performed to 700 DEG C, and industrial pure zinc, an Mg-Gd and Mg-Mn intermediate alloy are melted; (4) heating is performed to 730 DEG C, after an industrial pure aluminum ingot, Al-Ti, Al-Ti-B and Al-B intermediate alloys added are all melted, refining isperformed to obtain a magnesium alloy melt; (5) gravity casting is performed; and (6) secondary solid solution and artificial aging treatment are performed. According to the high-toughness heat-resistant Mg-Gd alloy and the preparation method, after the alloy is subjected to the gravity casting, the secondary solid solution treatment and the artificial aging heat treatment, the tensile strength at room temperature is 300 MPa, the elongation percentage is 15%, the high-temperature tensile strength at 200 DEG C is 218 MPa, the elongation percentage is 20%, and the high-end requirement for lightweight development in the industries of aerospace, automobiles, telecommunication and the like is met.
Owner:NANJING UNIV OF AERONAUTICS & ASTRONAUTICS

Method for manufacturing civil high-grade anti-theft door plank

The invention relates to a method for manufacturing a civil high-grade anti-theft door plank. The method comprises the steps of (1) obtaining a continuous casting slab by molten iron desulphurization, converter smelting, RH vacuum treatment and continuous casting for forming blanks; heating the continuous casting slab; carrying out high-pressure water descaling, rough rolling, finish rolling, laminar cooling and reeling on the heated slab after discharging from a furnace; and (2) uncoiling, pickling and trimming a hot rolled coil obtained in the step (1), rolling the rolled coil into cold-strip steel by a reversing cold rolling machine with a single frame, carrying out hood annealing treatment after degreasing, and finally carrying out smoothing, finishing and electrostatic oiling to obtain the civil high-grade anti-theft door plank. The method disclosed by the invention is stable to operate, convenient to use, free of new introduction of any production equipment, and free of increase the technological process of production; the production cost is not increased; the defect that a closed-loop vortex wave is generated when the surface of an ultra-low carbon cold-roll steel sheet is close to the edge part of the steel sheet can be effectively overcome; and the demand of the civil high-grade anti-theft door plank on high surface quality is met.
Owner:NINGBO IRON & STEEL

High-toughness heat-resisting pressure casting Mg-Gd alloy and preparation method thereof

ActiveCN109807302AEasy to prepareGood stability at high temperatureDuctilityPressure casting
The invention provides a high-toughness heat-resisting pressure casting Mg-Gd alloy and a preparation method thereof. The high-toughness heat-resisting pressure casting Mg-Gd alloy comprises components including, by stoichiometric ratio, 4.0%-8.0% of Gd, 1.2%-4.8% of Zn, 0.5%-1.2% of Al, 0.1%-0.3% of Mn, 0.01%-0.08% of M and the balance Mg, wherein M is one or two elements of Ti and B. The preparation method comprises the steps that firstly, materials are prepared according to Mg-Gb alloy components; secondly, industrial pure magnesium ingots are melted; thirdly, the temperature is raised to 720 DEG C, industrial pure zinc, Mg-Gd and Mg-Mn intermediate alloys are added and stirred to be completely melted; fourthly, the temperature is raised to 730 DEG C, after industrial pure aluminum ingots, Al-Ti, Al-Ti-B and Al-B intermediate alloys are sequentially added, magnesium alloy melt is obtained after refining; and fifthly, the magnesium alloy melt is cooled to a pressure casting temperature so as to be subjected to pressure casting, and a pressure casting alloy is obtained. The strength of extension of the alloy in a pressure casting state at the room temperature reaches 318 MPa, thestrength of extension of the alloy at the high temperature of 200 DEG C reaches 218 MPa, the room temperature ductility reaches 12.0%, the high-toughness heat-resisting pressure casting Mg-Gd alloy can be used without aging or solution heat treatment, and the high-end requirement of aerospace and other industries for light weight is met.
Owner:JIANGSU FAVOUR AUTOMOTIVE NEW STUFF SCI TECH +1

Method of synthesizing monoisopropanolamine

The invention relates to a synthesis method of isopropanolamine. The synthesis method comprises the following steps: (1) liquid ammonia and water are mixed to form ammonia water which is mixed with propylene oxide; mixed solution is preheated until the temperature reaches 120 to 125 DEG C, and the inputting molar ratio of the ammonia and the propylene oxide is controlled within 10 to 15; (2) the materiel after preheating is delivered into a reactor, the reaction temperature ranges from 128 to 138 DEG C, the pressure ranges from 12.6 to 13.8MPa, and the reaction time ranges from 1.5 to 3 hours; (3) the surplus unreacted ammonia is separated from the obtained mixture after the reaction by using a flash distillation column, the pressure in the flash distillation column ranges from 0.6 to 1.6MPa, and the temperature of a column kettle ranges from 140 to 160 DEG C; (4) the mixture which is separated through the flash distillation column is delivered into a leading tower for rectification dehydration, the pressure in the leading tower ranges from minus 0.080 to minus 0.085MPa, the temperature at the top of the leading tower is 45 to 55 DEG C, and the temperature at the bottom in a towerkettle ranges from 110 to 130 DEG C; (5) the mixture after dehydration is delivered into a rectification column for rectification, the pressure in the rectification column ranges from minus 0.095 to minus 0.099MPa, the temperature in the column kettle ranges from 135 to 160 DEG C, the temperature at the top of the rectification column ranges from 60 to 70 DEG C, isopropanolamine products are obtained at the top of the rectification column, and the mixture composed of diisopropanolamine and triisopropanolamine is obtained in the column kettle. The synthesis method has simple production procedure, little equipment investment, and high product quality.
Owner:NANJING BAOCHUN CHEMICAL INDUSTRY CO LTD

Preparation of mono-epoxy-terminated polysiloxane-modified gelatin gradient membrane by freeze-drying method

The present invention relates to preparation of a mono-epoxy-terminated polysiloxane-modified gelatin gradient membrane by a freeze-drying method. Surfactant sodium alkyl sulfate is dissolved in water and formulated into an aqueous solution, the aqueous solution is stirred for 1-2h at 40-60 DEG C under the condition of pH of 8 to 11, gelatin is added, stirring is performed for 4-8h, and mono-epoxy-terminated polysiloxane with the molecular weight of 500 is added to obtain a mono-epoxy-terminated polysiloxane-modified gelatin solution. The mono-epoxy-terminated polysiloxane-modified gelatin solution is centrifuged at a low temperature, after layering, water is added into an intermediate layer for even mixing, ethanol is added, after even mixing, 0.5-0.8ml of the mixture is measured and dropwise added into a gelatin substrate, standing is performed for 12-18h, liquid nitrogen is used for freezing, and the freeze-drying method is used for drying to obtain the mono-epoxy-terminated polysiloxane-modified gelatin gradient membrane. The mono-epoxy-terminated polysiloxane-modified gelatin gradient membrane has the characteristics that component concentration change is gradient in longitudinal section, and the mono-epoxy-terminated polysiloxane-modified gelatin gradient membrane is high in tensile strength, good in hydrophobicity and soft, and so on.
Owner:山东山科美谷科技发展有限公司

Modified gelatin gradient film prepared from mixed glycidol and single-epoxy-terminated polysiloxane

The invention relates to a modified gelatin gradient film prepared from mixed glycidol and single-epoxy-terminated polysiloxane. A method for preparing the modified gelatin gradient film includes dissolving surfactants in water to prepare aqueous solution; adding gelatin into the aqueous solution under the conditions of the temperatures of 40-60 DEG C and the pH (potential of hydrogen) of 8-11; stirring the gelatin and the aqueous solution for 4-8 h and then adding the single-epoxy-terminated polysiloxane into the gelatin and the aqueous solution continuously or in batches to obtain mixtures; carrying out reaction for 12-30 h and then adding glycidol into the mixtures; continuing to carry out reaction at the temperatures of 40-60 DEG C for 6-12 h to obtain milk white turbid liquid; adding ethyl alcohol into the milk white turbid liquid and uniformly mixing the ethyl alcohol with the milk white turbid liquid to obtain mixed liquid; dripping 0.5-0.8 ml of the measured mixed liquid on gelatin substrates; allowing the gelatin substrates to stand still for 12-18 h and then freezing the gelatin substrates by the aid of liquid nitrogen; drying the gelatin substrates by the aid of a freeze dryer to obtain the gradient film. The dosage of the gelatin is 1-10% of the mass of the aqueous solution. The dosage of the single-epoxy-terminated polysiloxane is 0.2-1.0 times the molar weight of the gelatin. The dosage of the glycidol is 0-1 times the mass of the single-epoxy-terminated polysiloxane. A volume ratio of the ethyl alcohol to reaction liquid is (3-5):1. The modified gelatin gradient film has the advantages that the concentration of components of the modified gelatin gradient film changes in longitudinal sections in a gradient manner, the modified gelatin gradient film is high in tensile strength and good in hydrophobic property and is soft, and the like.
Owner:山东山科美谷科技发展有限公司

Pressure casting Mg-Er alloy with high strength, high toughness and heat resistance and preparation method thereof

The invention provides a pressure casting Mg-Er alloy with high strength, high toughness and heat resistance and a preparation method thereof. The alloy is composed of, by mass, 4.0-8.5% of Er, 1.2-5.1% of Zn, 0.5-1.2% of Al, 0.1-0.3% of Mn, 0.01-0.08% of M, and the balance Mg, wherein the M is one or two elements of Ti and B. The preparation method comprises the following steps of (1), proportioning according to the composition of the Mg-Er alloy; (2), melting industrial pure magnesium ingots; (3), heating up to 720 DEG C, adding industrial pure zinc, Mg-Er and Mg-Mn master alloys, and stirring to melt completely; (4), heating up to 730 DEG C, and totally melting the industrial pure aluminum ingots, Al-Ti, Al-Ti-B and Al-B master alloys added in sequence to obtain a magnesium alloy melt;and (5) cooling the magnesium alloy melt to pressure casting temperature to carry out pressure casting to obtain the pressure casting alloy. After the die casting of the alloy, the tensile strength ofthe pressure casting alloy reaches 302 MPa at room temperature, the tensile strength reaches 205 MPa at the high temperature of 200 DEG C, the room temperature elongation reaches 15.0%, and the alloycan be used without aging and solid solution heat treatment to meet the high-end requirement of lightweight in aerospace and other industries.
Owner:FENGYANG L S NET FORMING CO LTD

Press molding technology for petroleum coke

InactiveCN108101017ATo achieve the purpose of secondary granulationEase of embedding - de-embeddingCell electrodesSecondary cellsLithiumCrucible
The invention discloses a press molding technology for petroleum coke. The technology comprises steps as follows: air-drying, drying, grinding, preheating, stirring, prepressing and pressure maintaining. According to the technology, the petroleum coke is subjected to grinding and extrusion molding, the purpose of secondary granulation of an anode material is achieved, more holes and channels can be formed in the anode material after secondary granulation, embedding-disembedding of lithium in the anode material is facilitated; meanwhile, after the petroleum coke is subjected to grinding and press molding, a molded sheet product can be directly placed in a graphitizing furnace for graphitizing treatment, so that a crucible used in the production process of anode powder can be omitted, then production cost is saved, degree of graphitization of the petroleum coke can be remarkably increased and is increased to 93 or higher from 90, quality of the anode material is improved, and electric capacity of the product is improved. The morphology of the anode material obtained after grinding and press molding is better than an anode material without being subjected to grinding and press molding, and the high-end demand of the market for the anode material is met.
Owner:吉林市松江炭素有限责任公司

Method for preparing diisopropanolamine

The invention relates to a method of manufacturing diisopropanolamine. Liquid ammonia and water are mixed to form ammonia water which is fully mixed with propylene oxide; the mixed solution is preheated until the temperature reach 140 to 145 DEG C and then is delivered into a reactor for reacting, the temperature is controlled within 148 to 155 DEG C when in reacting, the pressure is controlled within 16.0 to 18.0MPa, the inputting molar ratio of the ammonia and the propylene oxide is controlled within 5 to 8, and the reaction is fully performed for 1.5 to 3 hours; the mixture products obtained in the reaction are separated to obtain isopropanolamine products, diisopropanolamine products and triisopropanolamine products through flash evaporation and rectification in a stepwise way. In thediisopropanolamine products which are manufactured by adopting the method, the component of 1, 1<1>-nitrousalkyl-dipropyl-2-alcohol accounts for more than 99 percent (hereinafter referred to as mass percent), and the isomeride thereof is less than 1 percent. In addition, the cost of the production operation in the method is less, the production cost is low, the product quality is high, and the high-end requirement of products such as synthetic medicine, farm insecticide, etc. is satisfied.
Owner:NANJING BAOCHUN CHEMICAL INDUSTRY CO LTD
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