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178results about How to "Good emulsification and dispersion" patented technology

Synthetic method for preparing colorless transparent alkyl polyglucoside

The invention relates to a synthetic method for preparing colorless transparent alkyl polyglucoside, which comprises the following steps: adding glucosum anhydricum or glucose containing one crystal water and aliphatic alcohol with 8 to 20 carbon atoms into a reaction kettle in the weight ratio of 1:2.8-6.5; adding a composite catalyst containing dodecyl benzene sulfonic acid under the agitation of an emulsifying agitator; after undergoing a reaction for 4 to 8 hours at a temperature of between 80 and 120 DEG C under the vacuum condition of between -0.093 and -0.098 MPa, reducing the temperature to between 70 and 80 DEG C; adding neutralizer alkaline hydroxide, adjusting the pH value between 6 and 8 to obtain a flaxen mixture of alkyl polyglucoside and the aliphatic alcohol; and performing dealcoholization and blanching on the mixture to obtain a product of the colorless transparent alkyl polyglucoside. The method has a simple process and convenient operations. The process of the method not only can use the glucosum anhydricum, but also can use the glucose containing one crystal water, has a low cost and good quality; and the method adopts the composite catalyst, has a mild temperature, smooth water yielding and no phenomenon of foam overflow.
Owner:石家庄金莫尔化学品有限公司

High-functionality hydroxyl-terminated polyurethane aqueous dispersion as well as preparation method and application thereof

InactiveCN106866923AIncreased average hydroxyl functionalityIncrease crosslink densityPolyurea/polyurethane coatingsEthylenediamineNitrogen gas
The invention discloses a high-functionality hydroxyl-terminated polyurethane aqueous dispersion as well as a preparation method and application thereof. The preparation method comprises the following steps: adding aliphatic diisocyanate, polyvalent alcohol, a hydrophilic chain-extending agent and a catalyst into a reaction kettle; carrying out temperature rise reaction under the protection of nitrogen gas and cooling when the NCO percent of a system reaches a theoretical value; dropwise adding an acetone solution of a dihydric alcohol chain-extending agent and a crosslinking agent, continuously reacting and diluting with acetone when the NCO percent of the system reaches the theoretical value; cooling, and adding triethylamine for neutralizing; adding water for dispersing, and adding alcamines compounds for terminating; finally, carrying out post chain extending by using ethidene diamine to obtain the hydroxyl-terminated polyurethane aqueous dispersion. According to the high-functionality hydroxyl-terminated polyurethane aqueous dispersion disclosed by the invention, an alcamines terminating agent with polyhydroxy functionality is adopted, and a polyhydroxy functional group is introduced on a polyurethane chain segment by a terminating reaction of an amine group and an NCO group; the obtained aqueous dispersion has the advantages of high solid content, small particle size and stable storage; a two-component waterborne polyurethane coating prepared by the high-functionality hydroxyl-terminated polyurethane terminating dispersion has the characteristics of high drying speed of the coating, excellent medium resistance and environment friendliness of a product.
Owner:SOUTH CHINA UNIV OF TECH

High-efficiency safe environment-friendly all-synthetic cutting fluid and preparation method thereof

InactiveCN104479833AImprove the lubrication effectExcellent rust and corrosion inhibition performanceLubricant compositionEnvironmental resistanceWork in process
The invention discloses a high-efficiency safe environment-friendly all-synthetic cutting fluid and a preparation method thereof. The cutting fluid consists of the following components in percentage by weight: 20-30% of synthetic ester, 4-8% of surfactant, 5-15% of antirust agent, 2-10% of pH regulator, 0-3% of corrosion inhibitor and the balance of deionized water. The preparation method comprises the following specific steps: adding the pH regulator into part of the deionized water and stirring uniformly; adding the corrosion inhibitor and the antirust agent in turn and stirring until solid powder is completely dissolved; after uniformly mixing and stirring the synthetic ester, adding the surfactant of the proportion and stirring for 15 minutes till uniformity; pouring a semi-finished product into the reaction system and stirring uniformly; repeatedly flushing the preparation container with the rest deionized water, and completely beating the flushing liquid back into the reaction system; and continuously stirring the reaction system until the solution is uniform and transparent to obtain a finished product. In the invention, the prepared all-synthetic cutting fluid has excellent lubricating and antirust and corrosion inhibition properties as well as good stability at high and low temperature to avoid color change, and avoids stimulation to the skin of a human body; and moreover, the all-synthetic cutting fluid has good biological stability and is safe, environment-friendly and non-irritant.
Owner:JIANGSU XINLU NEW MATERIALS CO LTD

Dyeing and retanning tanning process

The invention relates to a dyeing and retanning tanning process, which comprises a softening and through-dyeing process and a color fixing and fixing process. The dyeing and retanning tanning process is characterized in that: the softening and through-dyeing process comprises the steps of adding normal-temperature water, wet blue leather, MND1717, MND3009, MND2031, MND2010, MND7010, sodium formate or sodium acetate, sodium bicarbonate, ammonium bicarbonate and dye by weight into a revolving drum, revolving for more than 2 hours, checking that the center of the obtained product is penetrated, stopping the drum, and keeping stand the obtained product overnight; and the color-fixing and fixing process comprises the steps of adding methanoic acid and MND1717 into a drum provided with a leather blank subjected to softening and through-dyeing treatments in the softening and through-dyeing process, in the same bath, adjusting the pH value, adding a chrome tanning agent, MND3009, MND2031, MND2010, glutaraldehyde or fatty aldehyde, and a mildew inhibitor into the drum, revolving for more than 4 hours, rinsing, taking the obtained product out of the drum, coating and finishing according to the conventional process. Compared with the prior art, the dyeing and retanning tanning process has the advantages of simple process, wide scope of application, capability of improving the quality of finished leather, raw material and labor saving, reduction of labor intensity, energy saving, effective reduction of wastewater discharge, and lower manufacturing cost.
Owner:禾瑞(漳州)助剂有限公司
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