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148 results about "Isooctanes" patented technology

Extraction tower and process for removing methanol from residual C4 of etherification reaction

The invention relates to an extraction tower and a process for removing methanol from residual C4 of an etherification reaction. The extraction tower comprises a tower body which is internally provided with a plurality of supporting beams; each group of supporting beams corresponds to one layer of tower plate in parallel; a plurality of grooves are formed in each supporting beam at intervals; liquid flow holes communicated with the adjacent lower layer of tower plate are formed in the bottom surfaces of the grooves; each layer of tower plate is formed by splicing a plurality of secondary tower plate pieces; the supporting beams in each two adjacent groups are arranged in a staggered manner; a washing liquid inlet is formed in the upper part of the tower body and a C4 inlet is formed in the lower part of the tower body; a gas-phase outlet is formed in the tower top, and a liquid-phase outlet is formed in the tower bottom. Desalted water which is taken from the outside and has the temperature of 35-45 DEG C enters the tower body from the washing liquid inlet through a desalted water pump, residual C4 of the etherification reaction, which has the temperature of 35-45 DEG C, enters the tower body from the C4 inlet, and the flow ratio of the washing liquid to residual C4 of the etherification reaction is 1 to (20-25). Methanol in mixed C4 with the low methanol content can be removed and the content of methanol in processed mixed C4 is not more than 50ppm so that the consumption amount of a sulfuric acid catalyst in an isooctane device, the energy consumption of the device and the amount of waste acids can be reduced.
Owner:NINGBO HAIYUE NEW MATERIAL

Super-hydrophilic/underwater super-oleophobic copper net and preparation method thereof, and application of super-hydrophilic/underwater super-oleophobic copper net in separation of emulsified oil-in-water

The invention discloses a super-hydrophilic / underwater super-oleophobic copper net and a preparation method thereof, and application of the super-hydrophilic / underwater super-oleophobic copper net inseparation of emulsified oil-in-water. The preparation method comprises the following steps: ultrasonically cleaning a copper net with acetone, ethyl alcohol and deionized water separately, and then drying the copper net; preparing a composite dip-coating solution of polydopamine, polyethyleneimine and aminated carbon nanotubes; immersing the whole pre-cleaned copper net into the dip-coating solution; then putting the whole dip-coating solution system including the copper net on a shaking table for horizontal-rotary coating operation; and taking out the copper net, cleaning the copper net withdeionized water, and drying the copper net. The preparation method has the advantages of simple preparation technology, low raw material consumption, mild reaction conditions and harmlessness to theenvironment, and the obtained super-hydrophilic / underwater super-oleophobic copper net is resistant to physical wear and chemical corrosion and has the function of quickly and efficiently separating various emulsified oil-in-water such as methylbenzene, petroleum ether, isooctane and 1,2-dichloroethane.
Owner:SOUTH CHINA UNIV OF TECH

Primary oil aid, and primary oil and preparation method thereof

The invention belongs to the field of petrochemical industry, and particularly relates to a primary oil aid, and primary oil and a preparation method thereof, wherein the primary oil aid comprises anantioxidant, a corrosion inhibitor, a detergent dispersant and a cosolvent, has good corrosion resistance, can be adsorbed on the inner surface of an engine so as to prevent the corrosive components in an oil product from corroding the engine, protect the engine and prolong the service life of the engine, and has good oxidation resistance. According to the invention, by combining the primary oil aid, isopentane, isohexane, isooctane, alkylated gasoline, methyl tert-butyl ether, raffinate oil and toluene to obtain primary oil, the primary oil aid can react with the unstable free radicals in theprimary oil to terminate the chain reaction in the fuel oxidation process and eliminate the free radicals, so that the primary oil is in a stable state, the storage time of the engine and the oil product is prolonged, and the good cold starting performance, the combustion performance and the power performance are achieved; and after the primary oil is combusted, the combustion efficiency of the engine is high, the oil consumption is low, and the tail gas emission is little.
Owner:SHANDONG EFIRM BIOCHEMISTRY & ENVIRONMENTAL PROTECTION CO LTD

Superposition oil hydrogenation device and method capable of producing isooctane

The invention discloses a superposition oil hydrogenation device and method capable of producing isooctane, and belongs to the technical field of petrochemical engineering. The device comprises a catalytic distillation hydrogenation column, a condenser, a reflux tank, a reboiler, a first compressor and a hydrogenation reactor; the top of the catalytic distillation hydrogenation column is connectedwith the condenser, the condenser is connected with one inlet of the reflux tank, one outlet of the reflux tank is connected with the first compressor, and the other outlet of the reflux tank is connected with the catalytic distillation hydrogenation column; the reboiler is arranged at the bottom of the catalytic distillation column; and the bottom of the hydrogenation reactor is connected with the catalytic distillation hydrogenation column. According to the superposition oil hydrogenation device and method capable of producing the isooctane, olefin in superimposed oil can be saturated, requirements of the superposition oil as a vehicle gasoline blending component are met and the isooctane is produced as needed, a hydrogenation reaction is separately carried out on different components in the superimposed oil through the catalytic distillation column and the hydrogenation reactor, the equipment and operation costs can be reduced, and the purpose of energy saving and flexible operation is achieved.
Owner:BC P INC CHINA NAT PETROLEUM CORP +1

Chromatographic method for determining content of EPA, DHA and total w-3 acids in fish oil

The invention discloses a chromatographic method for determining the content of EPA, DHA and total w-3 acids in fish oil. The method comprises the following steps: 1, esterifying; 2, preparing a sample solution; 3, preparing a standard substance solution; 4, setting chromatographic conditions; 5, sequentially introducing samples; and 6, comparing the relation between the retention time and the peak area of a sample to be determined with that of a standard substance to determine the content in the sample. In the w-3 fatty acid-containing fish oil sample treatment process, unsaturated fatty acids is saponified, saponified unsaturated fatty acids and a methanol solution of boron trifluoride directly undergo an ester formation reaction, and unsaturated fatty acid esters are directly extracted by a BHT-containing isooctane solution to obtain a solution used as the sample to be determined. The method adopting the appropriate ester formation process and the sample post-treatment process has the advantages of short test operation cycle, effective avoiding of volatilization and other problems in the operation, and accurate and reliable determination result, and is especially suitable for industrial production and other occasions needing large scale determination.
Owner:JIANGSU ALAND NOURISHMENT

High-octane-value oil product composition, primary oil and preparation method of primary oil

The invention relates to the field of petroleum products, and specifically discloses a high-octane-value oil product composition, primary oil and a preparation method of the primary oil. The oil product composition is prepared from the following raw materials in parts by weight: 62-86 parts of isooctane, 12-21 parts of methyl tert-butyl ether and 2-17 parts of benzene-making raffinate oil, the research octane number of the oil product composition is greater than or equal to 97.6, and the motor octane number of the oil product composition is not greater than 91.0; the invention further discloses the primary oil, which comprises the high-octane-value oil product composition and further comprises 0.0002-0.002 part by weight of an antistatic agent. The preparation method of the primary oil comprises the following steps: uniformly mixing the raw materials according to the proportion to obtain the primary oil. The oil product composition and the primary oil prepared in the invention have thecharacteristics of high octane number, especially high motor octane number, stable quality and clean combustion, and meet the use requirements of a high compression ratio engine, and the preparationmethod has the characteristics of simple and convenient operation and stable finished product.
Owner:北京中燕恒成能源有限公司

Method for detecting residue amount of fenvalerate pesticide in tea

The invention relates to a method for detecting the residue amount of fenvalerate pesticide in tea. The method comprises the first step of preparing a sample, wherein tea is dried, ground and screened; the second step of rough extracting of fenvalerate, wherein tea powder is put into a centrifuge tube, water is added for wetting, petroleum ether and mixture interior label working solution are added, vibrating for mixing is conduced, anhydrous magnesium sulfate, sodium chloride, sodium citrate, sodium hydrogen citrate and toluene are added, uniform vibrating is conducted, and centrifugation is conducted; the third step of purifying rough extract of fenvalerate, wherein supernate is placed into the centrifuge tube, anhydrous magnesium sulfate and N-propyl ethylenediamine bonding solid-phase adsorbent are added, uniform vibrating is conducted, and centrifugation is conducted; the fourth step of extracting fenvalerate, wherein supernatant is taken, toluene-isooctane mixed solution is used for extraction, concentration and filtration on a Florisil column; the fifth step of detection of chromatography. The extracting method is simple, the effect is good, and result integrals are processed more easily, conveniently and accurately. According to the method, the average recovery rate ranges from 93.21% to 103.75%, the relative standard deviation ranges from 3.28% to 6.20%, requirements are met, and accuracy and reliability are achieved.
Owner:周德志

Measurement method for the cyfluthrin pesticide residue in tea

The invention relates to a measurement method for the cyfluthrin pesticide residue in tea. The method comprises the following steps: firstly, sample preparation is carried out, namely, tea is dried, ground and sieved; secondly, cyfluthrin crude extraction is carried out, namely, the tea powder is placed in a centrifuge tube, water is added for infiltration, petroleum ether and a mixed internal standard operating fluid are added, the mixture is shocked and mixed uniformly, anhydrous magnesium sulfate, sodium chloride, sodium citrate, sodium hydrogencitrate and methylbenzene are added, and the mixture is shocked uniformly and centrifuged; thirdly, cyfluthrin crude extract product purifying is carried out, namely, the supernate is taken and placed in a centrifuge tube, anhydrous magnesium sulfate and N-propylethylenediamine bonding solid adsorbents are added, the mixture is shocked uniformly and centrifuged; fourthly, cyfluthrin extraction is carried out, namely, the supernate is taken, extraction, condensation and filtering are carried out in a Florisil column by utilization of the toluene-isooctane mixed solution; fifthly, chromatographic detection is carried out. The extraction method is simple, the effects are good, and result integration processing is simple and accurate. The average recovery rate of the method is 93.21%-103.75%, the relative standard deviation is 3.28%-6.20%, the average recovery rate and the relative standard deviation meet requirements and the method is accurate and reliable.
Owner:周德志
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