The invention discloses an
analysis method for detecting short-chain
fatty acid in table salt by headspace arrow-shaped
solid phase microextraction-
gas chromatography mass spectrometry, and belongs to the field of analysis and detection. According to the method, firstly, based on a headspace arrow-shaped
solid-phase microextraction technology, polar short-chain fatty acids are extracted and enriched by using an extraction head of 100 [mu] m Polyacrylate, and then
gas chromatography-
mass spectrometry is used for detection, so that qualitative and quantitative detection of nine short-chain fatty acids such as
acetic acid, propionic acid,
isobutyric acid,
butyric acid, 2-methylbutyric acid,
valeric acid, 2-methylvaleric acid, 4-methylvaleric acid and
hexanoic acid in the table salt can be realized. According to the method, the headspace arrow-shaped
solid-phase microextraction technology is used for extracting the short-chain
fatty acid in the table salt for the first time, the effects of interference removal, concentration and enrichment are achieved, and the
detection limit of the method is reduced by about 2 orders of magnitude compared with that of a headspace-
gas chromatography-
mass spectrometry method. The method is simple in
sample preparation, high in sensitivity, good in
recovery rate and stability and suitable for accurate detection of the short-chain
fatty acid in the table salt.