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152 results about "2-Ethylhexanoic acid" patented technology

2-Ethylhexanoic acid is the organic compound with the formula CH₃(CH₂)₃CH(C₂H₅)CO₂H. It is a carboxylic acid that is widely used to prepare lipophilic metal derivatives that are soluble in nonpolar organic solvents. 2-Ethylhexanoic acid is a colorless viscous oil. It is supplied as a racemic mixture.

D1369 d radiation curable secondary coating for optical fiber

InactiveUS20080226913A1Glass optical fibreGlass making apparatusTitanium butoxideMeth-
A new radiation curable Secondary Coating for optical fibers is described and claimed wherein said composition comprises a Secondary Coating Oligomer Blend, which is mixed with a first diluent monomer; a second diluent monomer; optionally, a third diluent monomer; an antioxidant; a first photoinitiator; a second photoinitiator; and optionally a slip additive or a blend of slip additives; wherein said Secondary Coating Oligomer Blend comprises:α) an Omega Oligomer; andβ) an Upsilon Oligomer;wherein said Omega Oligomer is synthesized by the reaction ofα1) a hydroxyl-containing (meth)acrylate;α2) an isocyanate;α3) a polyether polyol; andα4) tripropylene glycol; in the presence ofα5) a polymerization inhibitor; andα6) a catalyst;to yield the Omega Oligomer;wherein said catalyst is selected from the group consisting of dibutyl tin dilaurate; metal carboxylates, including, but not limited to: organobismuth catalysts such as bismuth neodecanoate; zinc neodecanoate; zirconium neodecanoate; zinc 2-ethylhexanoate; sulfonic acids, including but not limited to dodecylbenzene sulfonic acid, methane sulfonic acid; amino or organo-base catalysts, including, but not limited to: 1,2-dimethylimidazole and diazabicyclooctane; triphenyl phosphine; alkoxides of zirconium and titanium, including, but not limited to Zirconium butoxide and Titanium butoxide; and Ionic liquid phosphonium salts; and tetradecyl(trihexyl)phosphonium chloride; andwherein said Upsilon Oligomer is an epoxy diacrylate.
Owner:DSM IP ASSETS BV

Catalyst composition for ethylene oligomerization and the use thereof

The present invention relates to a catalyst composition for ethylene oligomerization and the use thereof. Such catalyst composition includes chromium compound, ligand containing P and N, activator and accelerator; wherein the chromium compound is selected from the group consisting of acetyl acetone chromium, THF-chromium chloride and Cr(2-ethylhecanoate)3; general formula of the ligand containing P and N is shown as:in which R1, R2, R3 and R4 are phenyl, benzyl, or naphthyl. R5 is isopropyl, butyl, cyclopropyl, cyclopentyl, cyclohexyl or fluorenyl; the activatior is methyl aluminoxane, ethyl aluminoxane, propyl aluminoxane and / or butyl aluminoxane; the accelerator is selected from the group consisting of 1,1,2,2,-tetrachloroethane, 1,1,2,2-tetrabromoethane, 1,1,2,2-tetrafluoroethane, and compounds having a formula of X1R6X2, in which X1 and X2 are F, Cl, Br, I or alkoxyl, R6 is alkylene or arylene group; the molar ratio of chromium compound, ligand containing P and N, activator and accelerator is 1:0.5˜10:50˜3000:0.5˜10. After mixing the four components mentioned previously under nitrogen atmosphere for 10 minutes, they are incorporated to the reactor, or these four components are incorporated directly into the reactor. Then ethylene is introduced for oligomerization. Such catalyst can be used in producing 1-octene through ethylene oligomerization. It is advantageous in high catalysing activity, high 1-octene selectivity, etc. The catalytic activity is more than 1.0×106 g product·ma−1 Cr·h−1, the fraction of C8 linear α-olefin is more than 70% by mass.
Owner:PETROCHINA CO LTD

Method for preparing 2-ethyl hexanoic acid by catalytically oxidizing 2-ethylhexanal by molybdovanadophosphoric acid

The invention discloses a method for preparing 2-ethyl hexanoic acid by catalytically oxidizing 2-ethylhexanal by molybdovanadophosphoric acid, and relates to a method for preparing a chemical preparation. The method comprises the following steps: weighing molybdovanadophosphoric acid and dissolving the molybdovanadophosphoric acid in distilled water at first and then in hydrochloric acid to prepare a catalyst solution; adding 2-ethylhexanal and the prepared catalyst in an ordinary-pressure reaction device, slowly heating and stirring the mixture, regulating oxygen flux, and starting to introduce oxygen when the temperature rises to the reaction temperature; after the reaction is ended, separating out the aqueous phase solution on the lower layer to obtain organic phase matter on the upper layer; and depressurizing and distilling the organic phase matter to obtain colorless transparent and pungent oily liquid, 2-ethyl hexanoic acid. By changing the ratio of molybdenum to vanadium of the catalyst and optimizing the reaction condition, the conversion rate of the 2-ethylhexanal reaches above 99%, and the selection and yield of the 2-ethyl hexanoic acid reach above 98% respectively.
Owner:SHENYANG INSTITUTE OF CHEMICAL TECHNOLOGY

Cobalt salt adhesive for retreading radial wire cord tire and preparation method thereof

The invention discloses a cobalt salt adhesive for retreading a radial wire cord tire and a preparation method thereof. The adhesive comprises a composite adhesive, rubber and an addition agent, wherein the composite adhesive is mainly composed of a main adhesive and an auxiliary adhesive to form a component A; the main adhesive comprises cobalt boroacylate and cobalt neocaprate; the auxiliary adhesive is 2-vanadium ethylcaproate; the rubber comprises natural rubber and butadiene styrene rubber; the addition agent comprises an anti-ageing agent, a plasticizer, a reinforcing agent, an accelerant, an activating agent, a silane coupling agent and a vulcanizing agent. The cobalt salt adhesive for retreading the radial wire cord tire is prepared by the following steps of: dispersing the component A into a rubber carrier to be matched with the addition agent to form an adhesion master batch B; and dissolving the adhesion master batch B by a solvent gasoline to prepare adhesive slurry. The cobalt salt adhesive for retreading the radial wire cord tire provided by the invention has the advantages of good heat stability, good dynamic mechanic property, capability of being directly coated, low cost, and resource saving, and is applicable to the adhesion of new tread rubber and a previous belt compound in a retreading process of the radial wire cord tire, and the high-strength adhesion of the new tread rubber and polished belt steel wires.
Owner:镇江泛华新材料科技发展有限公司

High-solid, low-viscosity and quick-drying odor removal alkyd resin, method for preparing same and application of high-solid, low-viscosity and quick-drying odor removal alkyd resin

The invention discloses high-solid, low-viscosity and quick-drying odor removal alkyd resin, a method for preparing the same and application of the high-solid, low-viscosity and quick-drying odor removal alkyd resin. The high-solid, low-viscosity and quick-drying odor removal alkyd resin in a formula comprises, by weight, 15-20 parts of oleic acid, 2-4 parts of 3, 5, 5-trimethyl hexanoic acid, 2-4 parts of 2-ethylhexanoic acid, 2-4 parts of castor oil, 25-32 parts of polyacid, 18-26 parts of polyols, 3-5 parts of reflux solvents, 17-21 parts of diluting solvents and 0.5-2 parts of auxiliaries. The high-solid, low-viscosity and quick-drying odor removal alkyd resin, the method and the application have the advantages that the high-solid, low-viscosity and quick-drying odor removal alkyd resin has quick-drying and odor removal characteristics, the solvents can be quickly released when the high-solid, low-viscosity and quick-drying odor removal alkyd resin is coated, the high-solid, low-viscosity and quick-drying odor removal alkyd resin in construction sites rarely has odor and can be completely dried after being coated for 24 h, dried paint films hardly have odor, and people can hardly smell out smell and can have a sense of joy just like a sense of joy under the condition of water-based paint films; the solid content of the high-solid, low-viscosity and quick-drying odor removal alkyd resin prepared by the aid of the method is 80+/-2%, the viscosity of the high-solid, low-viscosity and quick-drying odor removal alkyd resin is 10000+/-2000 mpa.s/25 DEG C, accordingly, the high-solid, low-viscosity and quick-drying odor removal alkyd resin has high-solid and low-viscosity characteristics, the usage of diluents can be reduced when paint is prepared, the VOC (volatile organic compounds) content can be reduced and is only 350 g/L after the paint is manufactured, and tax exemption requirement on construction VOC content lower than 420 g/L after the paint is manufactured can be sufficiently met.
Owner:GUANGDONG MAYDOS BUILDING MATERIALS LTD CO

Process for treating and recycling industrial wastewater of peroxide-2-ethylhexoic acid tertiary butyl ester

The invention discloses a process for treating and recycling industrial wastewater of peroxide-2-ethylhexoic acid tertiary butyl ester (an initiator OT), belonging to the technical field of industrial wastewater treatment. In the process, the industrial wastewater of peroxide-2-ethylhexoic acid tertiary butyl ester is directly collected from a sewage draining port of a production device and is subjected to stabilization treatment so as to basically eliminate the risk that organic peroxides in the wastewater are heated and severely decomposed, and tertiary butanol-tertiary butyl peroxide mixtures, concentrated sulfuric acid, sodium hydroxide and sodium chloride, which are recyclable, are separated and recycled from the wastewater. The wastewater subjected to removal of most organic matters and recycling of sulfuric phosphate, caustic soda and sodium chloride is subjected to hydrolysis-contact oxidation treatment, and C-Fe is subjected to micro-electrolysis decoloration, so that main water discharge indexes meet the requirements in Discharge Standards of Water Pollutants for Pharmaceutical Industry of Chemical Synthesis Products Category (GB21904-2008) for discharge limits of water pollutants for new enterprises. Therefore, the treatment of the peroxide-2-ethylhexoic acid tertiary butyl ester and the recovering and recycling of pollutants in the wastewater are realized.
Owner:NORTHWEST NORMAL UNIVERSITY
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