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341 results about "Dibasic ester" patented technology

Dibasic ester or DBE is an ester of a dicarboxylic acid. Depending on the application, the alcohol may be methanol or higher molecular weight monoalcohols. Mixtures of different methyl dibasic esters are commercially produced from short-chain acids such as adipic acid, glutaric acid, and succinic acid. They are non-flammable, readily biodegradable, non-corrosive, and have a mild, fruity odour.

Process for preparing dibasic acid ester

The invention relates to a method of preparing dibasic acid esters. Solid acid catalyst, dualistic carboxylic acid or dualistic carboxylic acid mixture, and low-carbon alcohol are added in a pre-esterification kettle; the addition amount of the solid acid catalyst is 1 to 10 percent of the quality of the dualistic carboxylic acid or the dualistic carboxylic acid mixture; the molar ratio of the alcohol and the dualistic carboxylic acid or the dualistic carboxylic acid mixture is 1 to 10:1; the reaction is performed under the normal atmosphere, wherein, the temperature ranges from 50 to 100 DEG C; the supernatant fluid of reaction products is delivered into the upper part of an esterification reactor; after the low-carbon alcohol is turned into vapour by passing through a carburetor, the low-carbon alcohol vapour enters into the lower part of the esterification reactor; the supernatant fluid and the low-carbon alcohol vapour effect the reflux reaction at a catalyst section of a continuous esterification reactor; reaction products are expelled from the bottom of the esterification reactor, and unreacted low-carbon alcohol and generated water are steamed from the top of the reactor; esterification reaction occurs under the normal atmosphere, the temperature ranges from 70 to 150 DEG C, the liquid airspeed is 0.1 to 0.7Kg / Kg*h, the airspeed of the low-carbon alcohol is 0.1 to 1.0Kg / Kg*h, and the percent conversion can reach more than 99 percent.
Owner:PETROCHINA CO LTD

Cleaning system utilizing an organic cleaning solvent and a pressurized fluid solvent

A cleaning system that utilizes an organic cleaning solvent and pressurized fluid solvent is disclosed. The system has no conventional evaporative hot air drying cycle. Instead, the system utilizes the solubility of the organic solvent in pressurized fluid solvent as well as the physical properties of pressurized fluid solvent. After an organic solvent cleaning cycle, the solvent is extracted from the textiles at high speed in a rotating drum in the same way conventional solvents are extracted from textiles in conventional evaporative hot air dry cleaning machines. Instead of proceeding to a conventional drying cycle, the extracted textiles are then immersed in pressurized fluid solvent to extract the residual organic solvent from the textiles. This is possible because the organic solvent is soluble in pressurized fluid solvent. After the textiles are immersed in pressurized fluid solvent, pressurized fluid solvent is pumped from the drum. Finally, the drum is de-pressurized to atmospheric pressure to evaporate any remaining pressurized fluid solvent, yielding clean, solvent free textiles. The organic solvent is preferably selected from terpenes, halohydrocarbons, certain glycol ethers, polyols, ethers, esters of glycol ethers, esters of fatty acids and other long chain carboxylic acids, fatty alcohols and other long-chain alcohols, short-chain alcohols, polar aprotic solvents, siloxanes, hydrofluoroethers, dibasic esters, and aliphatic hydrocarbons solvents or similar solvents or mixtures of such solvents and the pressurized fluid solvent is preferably densified carbon dioxide.
Owner:EMINENT TECHNOLOGY
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