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211results about How to "Full reuse" patented technology

Device and method for refining and separating polyoxymethylene dimethyl ether containing formaldehyde

PendingCN107118083AReduce consumptionSolving Formaldehyde Polymerization ProblemsOrganic chemistryOrganic compound preparationPipingChemistry
The invention relates to a device and method for refining and separating formaldehyde-containing polyoxymethylene dimethyl ether, which mainly includes a separation system and a rinsing and condensation circulation system. The separation system mainly consists of reaction unit (I), deacidification device (II), first atmospheric fractionation column (III), second atmospheric fractionation column (IV), vacuum distillation column (IX), vacuum refining Distillation tower (X), dehydration device (VII); the main devices of the leaching condensation circulation system include the first rinsing absorption tower (V), the second leaching absorption tower (VI) and the eluent storage tank (Ⅷ ) and related piping components. The present invention effectively solves the problem of formaldehyde polymerization blocking the condenser and pipelines in the process of separating aldehyde-containing polyoxymethylene dimethyl ether products through the organic combination of separation and rinsing systems, and 100% recovery of formaldehyde in the separated products realizes The continuous separation process of formaldehyde-containing polyoxymethylene dimethyl ether products with DMM3-6 as the product is realized, which is energy-saving and environmentally friendly.
Owner:TIANJIN UNIV

Method for recovering tantalum-niobium, lepidolite and feldspar powder by utilizing difficult-to-treat mine solid waste

The invention discloses a method for recovering tantalum-niobium, lepidolite and feldspar powder by utilizing difficult-to-treat mine solid waste. The method is characterized in that the difficult-to-treat mine solid waste is taken as a raw material, wherein the difficult-to-treat mine solid waste is a valuable component material containing a trace of (Ta, Nb)2O5, lepidolite and feldspar, and themethod comprises the step of recovering the tantalum-niobium concentrate, the feldspar powder and the lepidolite, recovering of the tantalum-niobium concentrate is achieved though the following steps,the series-connection technology of weak magnetism, medium magnetism and strong magnetism is carried out on the difficult-to-treat mine solid waste raw material for separation of iron slag, magneticminerals and non-magnetic mineral so that the influence of iron minerals on the reselection of the tantalum-niobium ore can be eliminated, a tantalum-niobium ore waste stone raw material is obtained,the tantalum-niobium ore waste stone raw material undergoes classification by adopting a stage grinding-stage separation process method, coarse grains enter a ball mill for ore grinding, a high-frequency vibration fine sieve is adopted for carrying out intensifying classification on the fine fraction, and then the tantalum-niobium concentrate and the feldspar-lepidolite mixture with tailings beingiron-tantalum-niobium contained weak-magnetic impurities are prepared. The method has the advantages that the technology is simple, the efficiency is high, the economic and technical benefits are obvious, and the recovery rate of the tantalum-niobium and other mineral resource products is high.
Owner:江西金辉再生资源股份有限公司

PTA production method with low energy consumption, low material consumption andlow refuse discharge

The invention relates to a Purified Terephthalic Acidproduction method with low energy consumption, low material consumption and low refuse discharge. The PTA production method comprises the following steps: tail gas of an oxidation reactor is outputted and passes through by-product steam of a first stage steam generator and is sent to an acetic acid regeneration tower for recycling acetic acid; a refined mother liquor is returned to the acetic acid regeneration tower, the original vacuum filtration filter is replaced by a pressure filter, and filter cakes are directly pulped and supplied to a refining section; through recovered acetic acid recovery extraction, an oxidized mother liquor is processed by extraction, and an acetic acid methyl ester removed tower top backflow liquid of the acetic acid regeneration tower is used for oxidizing, washing filter cakes of the refining section and blending slurries of the refining section. The method and system provided by the invention can effectively control acetic acid consumption in tail gas and waste water, recycle organic matters of the refined mother liquid, realize reuse of water, reduce consumption of steam and electric energy, reduce refuse discharge, and also can supply benzoic acid, mixed phthalic acids and other by-products. The invention has the advantages of short process flow, good operationality, low production cost and low apparatus investment.
Owner:BC P INC CHINA NAT PETROLEUM CORP +1

Large-scale piggery dung treatment ecological circulation system

The invention discloses a large-scale piggery dung treatment ecological circulation system which comprises a dung collection unit, a solid-liquid separation unit, an anaerobic fermentation unit, a biogas utilization unit and a biogas slurry utilization unit. The dung collection unit comprises a slurry collection tank, a dung accumulation tank, a settling tank and a slurry storage tank, the solid-liquid separation unit comprises a solid-liquid separator and an organic fertilizer treatment device, the anaerobic fermentation unit is a multistage anaerobic reaction device and comprises a primary anaerobic reaction tank and a secondary anaerobic reaction tank, the biogas utilization unit comprises a biogas cabinet, a biogas purification device and a biogas power generation device, the biogas slurry utilization unit comprises a biogas slurry storage tank, a forestry irrigation device and a farmland irrigation device, and high-temperature oxidation resistant plastic soft protection layers are arranged above the dung accumulation tank and the slurry storage tank. Dung water is fermented to generate biogas and biogas slurry, organic fertilizers are generated after solid-liquid separation, the possibility of secondary pollution caused by waste gas is avoided, waste is effectively and sufficiently reused, and comprehensive utilization rate is increased.
Owner:MUYUAN FOODS CO LTD

Carbon quantum dot fluorescence labeling material with orange peels used as carbon source as well as preparation method and application of carbon quantum dot fluorescence labeling material

The invention relates to a carbon quantum dot fluorescence labeling material with orange peels used as a carbon source as well as a preparation method and an application of the carbon quantum dot fluorescence labeling material. The orange peels are used as a raw material, and a simple method for one-step synthesis of a high-fluorescence-quantum-efficiency carbon quantum dot is established. The method comprises steps as follows: the orange peels are mixed with water; then a mixed liquid is mixed with concentrated sulfuric acid; the pH is adjusted by the aid of NaOH, and undissolved residues are removed in a centrifugal manner; then dichloromethane is added to a centrifuged supernate, and a non-fluorescence fat-soluble substance is removed in the centrifugal manner; finally, the centrifuged supernate passes through a film, and the fluorescence labeling material is prepared. According to the method, high-temperature and high-pressure reactions are not required to be performed by equipment such as plasma emitters, hydrothermal reaction kettles, muffle furnaces and the like during synthesis, reaction conditions are mild, operations are simple and convenient, the cost is very low, the method can be implemented in ordinary laboratories, the synthesized fluorescence labeling material lays a foundation for the further application to work such as bio-labeling, heavy metal analysis, antibody labeling, cell staining and the like.
Owner:INST OF AGRO FOOD SCI & TECH CHINESE ACADEMY OF AGRI SCI

Separation and purification system of organic synthesis feed liquid and separation and purification method thereof

The invention aims at the field of chemical industry and relates to a separation and purification system of organic synthesis feed liquid and a separation and purification method of the organic synthesis feed liquid. The separation and purification system comprises a crystallization system and a solid-liquid separation system which are sequentially arranged from front to back, wherein the crystallization system comprises a mixed suspension-mixed product-removal (MSMPR) crystallizer and a draft-tube-baffled (DTB) crystallizer which are connected with each other in series; the separation and purification system also comprises a liquid processing system used for processing waste liquid produced by the solid-liquid separation system; the liquid processing system comprises a desalting device and a membrane concentration device which are sequentially arranged from front to back. By virtue of the separation and purification system of the organic synthesis feed liquid and the separation and purification method thereof, the organic synthesis feed liquid is separated and purified by using a continuous crystallization technology, an electrodialysis technology and a membrane separation and concentration technology; the produced waste liquid is fully recycled and used, so that the separation and purification efficiency is improved, the purity and the yield of products are improved and the discharge of the waste liquid is reduced; the separation and purification system of the organic synthesis feed liquid and the separation and purification method thereof are strong in production industrialization and low in costs, and are especially suitable for producing iminodiacetonitrile.
Owner:CHONGQING UNISPLENDOUR CHEM

Pollution-free production process of plant fiber pulp

The invention provides a pollution-free production process of plant fiber pulp. The method is characterized by obtaining the bleached fine pulp with concentration being 30-40% through coarse pulp preparation, defibrination treatment, desanding treatment, screening treatment, concentration and shoving treatment. The process has the following beneficial effects: the auxiliary has strong wetting and infiltrating functions, promotes the sodium hydroxide to rapidly wet the surface of the fibers and be infiltrated into the fibers with the reactive agent generated by hydrogen peroxide in the presence of the decomposing agent and ensures the chromophore in the lignin to be decomposed into low molecular colorless substances while the lignin is degraded and dissolved out; the stabilizing agent can complex and shield chromogenic metal ions and is characterized by reducing generation of the chromophoric groups, thus improving the whiteness of the pulp; under the action of the surfactant in the auxiliary, the dissolved lignin, colloid and the like can be uniformly dispersed in the water to be prevented from being adsorbed by the plant fibers again; and the pulp washing and bleaching procedures are omitted in the method, and at the same time, the waste water in the pulping process can be fully reused through simple treatment, thus not producing pulping back liquor causing serious pollution.
Owner:深圳市美中现代科技发展有限公司

Double-floor type structure dry-mixed mortar station and construction method thereof

The invention provides a double-floor type structure dry-mixed mortar station and a construction method thereof. The double-floor type structure dry-mixed mortar station comprises a drying system, a sieving system, a material supplying system, a storage system, a main body structure, a metering system, a stirring system, a packaging system, a bulking system, a dust-removing system, an electric system, a pneumatic system and an outer packaging system. The double-floor type structure dry-mixed mortar station is characterized in that a variable-frequency feeding device is additionally arranged on a coal cabin charging belt machine in the drying system; aggregates are sieved at a plurality of grades; a primary sieving segregation and sand feeding manner is adopted before bucket lifting; a secondary sieving segregation and sand feeding manner is adopted after the bucket lifting; a sieving machine is provided with an elastic vibration support; a gas tank pulse type automatic dust collector is adopted; a main body adopts a double-floor type structure; two sets of large cubic horizontal double-shaft spiral belt agitating main engines are arranged, one set is standby and the two sets can also be turned on at the same time to use; a multi-finished-product cabin with a manual gate valve and a double-bagging machine are adopted to rapidly bulk and bag to deliver products; and the pneumatic system has bidirectional self-control and self-locking functions so as to guarantee the safety and the reliability of the work of double gas paths and improve the intelligent degree of the whole system.
Owner:上海鸿得利重工有限公司

Retired lithium iron phosphate and ternary lithium battery hybrid coordination control method and system

The invention discloses a retired lithium iron phosphate and ternary lithium battery hybrid coordination control method and system. The control method comprises the following steps: screening retiredbatteries, screening and grouping the retired batteries of the same type which meet the requirement that the residual life is close to the residual capacity; connecting different types of battery packs in series to form a battery module, wherein the different types of battery packs in the battery module meet the following conditions: the number of the different types of battery packs, the total capacity of the battery packs and the average service life of battery cells in the battery packs are equal; monitoring and arranging the performance of the battery in the battery module, monitoring andanalyzing the performance of the module, and then managing and controlling the battery module, wherein the retired battery comprises lithium iron phosphate and a ternary lithium battery. The lithium iron phosphate battery and the ternary lithium battery of a retired electric vehicle are used as objects, the advantages of the two lithium batteries are fully played, the raw material cost of the power battery is saved, the service life of the retired batteries is prolonged, and the performance of the power battery is fully utilized.
Owner:CHANGSHA UNIVERSITY OF SCIENCE AND TECHNOLOGY

Recycling system and recycling method for waste liquor produced in separation and purification of organically synthesized feed liquid

The invention relates to a recycling system and a recycling method for waste liquor produced in separation and purification of an organically synthesized feed liquid, and belongs to the field of chemical engineering. The recycling system for the waste liquor comprises a filter device, a desalting device and a membrane concentrating device which are arranged from the front to the rear in sequence, or the filter device is replaced with a filtrate collecting slot, wherein the filter device is used for filtering and collecting the waste liquor; the filtrate collecting slot is used for stewing and collecting the waste liquor; the desalting device is used for desalting the collected waste liquor; the membrane concentrating device is used for concentrating a liquid which is desalted by virtue of the desalting device; and the desalting device is preferably an electrodialysis device. According to the recycling system and the recycling method, a membrane separating and concentrating technology, an electrodialysis technology and the like are comprehensively utilized to separate and purify the organically synthesized feed liquid, and the produced waste liquor is sufficiently recycled, the separating and purifying efficiency and the purity and the yield of products are improved, discharge of the waste liquor is reduced, the production industrialization is strong and the cost is low, and thus, the recycling system and the recycling method are especially suitable for being applied in production of iminodiacetonitrile.
Owner:CHONGQING UNISPLENDOUR CHEM

Heightened construction method for active service stone building bank protecting wall

The invention relates to a heightened construction method for an active service stone building bank protecting wall. The heightened construction method includes the following steps that (1) an original bank protecting slope is cleaned and repaired; (2) anchor rod construction is carried out; (3) lattice girder construction is carried out; (4) foam concrete construction is carried out; (5) pavement construction is carried out; (6) newly-increased protection bank construction is carried out; and (7) concrete curing is carried out. A structure related in the heightened construction method comprises angle iron arranged at the top of an original protection bank according to a certain distance, the angle iron and embedded steel bars at the top of the original protection bank are connected in a welded manner, and a foam concrete sea side formwork and a newly-increased protection bank side mold are connected with the angle iron in a fastened manner through screws; prefabricated slabs are evenly inserted and piled on the foam concrete bank side, a foam concrete bank side formwork is arranged to be in a separated manner and is connected with the prefabricated slabs in a fastened manner through box iron, the screws and nuts; and newly-increased protection bank framework reinforcing steel bars and original protection bank embedded steel bars are connected through a direct threaded sleeve. The heightened construction method for the active service stone building bank protecting wall has the beneficial effects of being reliable in structure, convenient to construct, short in time limit for a project, environment-friendly and good in concrete appearance quality.
Owner:ZHEJIANG UNIV CITY COLLEGE

Method for preparing anhydrous sodium sulfate from chromium-containing mirabilite

The invention relates to the field of a chemical industry and particularly relates to a method for preparing anhydrous sodium sulfate from chromium-containing mirabilite as a by-product in the production process of sodium dichromate. The method comprises dissolving a certain concentration of chrome-containing mirabilite in chromium-containing waste water, adding quantitative sodium thiosulfate into the waste water to promote reduction of hexavalent chromium into trivalent chromium under 0.1-1 Mpa at 80-190 DEG C, wherein the trivalent chromium in a form of chromium trioxide hydrate is precipitated, adding a small amount of sulfuric acid to neutralize, filtering to acquire the chromium trioxide hydrate, removing impurities, carrying out decoloration, evaporating to precipitate anhydrous sodium sulfate crystals, and carrying out continuous centrifugal separation and drying. The method is simple and easy, utilizes cheap raw materials, has low energy consumption and a high automation degree and is suitable for large-scale production. The quality of the industrial anhydrous sodium sulfate product obtained by the method meets the requirements of class I products in the GB / T 6009-2014 industrial anhydrous sodium sulfate standard.
Owner:陕西省商南县东正化工有限责任公司
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