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754results about "Fibrous raw materials" patented technology

Organic biomass fractionation process

A method for fractionating fibrous biomass comprising cellulose, hemicellulose and lignin components to separate said lignin, cellulose and hemicellulose from one another comprises: (a) shredding said fibrous biomass; (b) concurrently with or subsequent to said shredding, contacting said biomass with an aqueous solution of a nitrate ion source at a concentration of about 0.1-0.3% at a temperature in the range of about 60° to about 80° C. to initiate nitration of the lignin component of said biomass; (c) submerging said partially nitrated biomass in an aqueous solution of a nitrate ion source in the presence of an aluminum compound at a temperature within the range of about 75-100° C. for a time sufficient to complete the nitration of said lignin component; (d) contacting the nitrated biomass produced in step (c) with an alkaline extraction liquor comprising NH4OH at an initial concentration sufficient to solubilize said nitrated lignin component and said hemicellulose component from said cellulose component of said biomass; e) recovering said cellulose from said extraction liquor containing said solubilized nitrated lignin and hemicellulose components, wherein said cellulose comprises at least about 88% alpha cellulose; (f) treating said extraction liquor with an acid to precipitate lignin contained therein, and (g) separating said lignin from soluble hemicellulose in said extraction liquor. The recovered cellulose component comprises at least 88% alpha cellulose and is useful as a starting material for the production of ethanol.
Owner:PRIOR ERIC S

Method for preparing cellulose nano-fibril film by utilizing wood powder

The invention relates to a method for preparing a cellulose nano-fibril film by utilizing wood powder, which comprises the following steps: 1) chemically pre-processing; 2) mechanically separating; and 3) preparing a film. The method has the advantages: the acid-base pre-processing is combined with wood powder grinding and is adopted for preparing; the lignin in the wood powder is removed by mainly utilizing sodium chlorite under an acidic condition; the half-fibril is removed by using the diluted potassium hydroxide and the remained substrate is cellulose; and the diluted hydrochloric acid is used for splitting the cellulose. The acting force of hydrogen bonds in the fibril is reduced by adopting the splitting treatment, so that the biomass cellulose nano-fibril at high length-diameter ratio is obtained; the mineral substance in the fiber is removed by utilizing HCl treatment, the alkali insoluble half-cellulose in the purified cellulose is influenced and the effect of purifying the cellulose fiber is achieved; the chemical constituents are detected through Fourier transform infrared; the grinding treatment is simple and easy to operate and the mass production is performed; the modulus of elasticity is 3105.27MPa; and the tensile strength is 64.24MPa.
Owner:襄垣县鑫瑞达连氏塑木制造有限公司 +1

Paper-making grade softwood pulp plate modifying production technique

The invention provides a denaturizing production technique of paper making needle wood pulp plate, which solves the problems of uneven dipping, slow hemicelluloses stripping, difficult accumulation descending, uneven cooking, single cooking method, single bleaching method and violent conditions existing in denaturizing production technique of wood pulp in the prior art. The invention comprises the following steps: wood pulp plate paging, alkali soaking, pressing, untwining and dispersion, cooking, washing, impurity removal, bleaching, a secondary washing and pulping; wherein, the wood pulp plate paging, alkali soaking, pressing, untwining and dispersion are to send papers into a alkali dipping barrel with concentration of 6 percent to 18 percent after the paper making bleaching wood pulp plates are separated by a paging device. When the wood pulp plates are changed into pulp with concentration of 3 percent to 6 percent, the pulp with concentration of 3 percent to 6 percent is sent to a squeezer to be squeezed and to untwine and disperse fiber. By adopting the invention, the quality of the dissolved viscose fiber wood pulp can be better and more stable; furthermore, the invention provides wider selection range of raw material.
Owner:YIBIN GRACE GROUP CO LTD

Bamboo chemimechanical pulp bioenzyme pretreatment method

The invention discloses a bamboo chemimechanical pulp bioenzyme pretreatment method. The bamboo chemimechanical pulp bioenzyme pretreatment method comprises the following steps: feeding bamboo pieces into a steaming cabin for normal-pressure pre-steaming after screening the bamboo pieces, and then carrying out first-stage screw extrusion; adding bioenzyme in an extruded material for pretreatment, then carrying out high-temperature deactivation, washing and dewatering, then carrying out first-stage and second-stage chemical pre-impregnating in sequence, then carrying out first-stage high-consistency normal-pressure pulp grinding by using a high-consistency disc refiner of which rho is 300, and completing bleaching reaction by enabling pulp to stay in a high-consistency reaction cabin for about 50 to 60 minutes; then carrying out follow-up pulp grinding by using a disc refiner, preparing pulp samples in different Canadian freeness degrees by controlling and inputting different pulp grinding energy consumptions, respectively recording the pulp grinding energy consumption needed for preparing each pulp sample, and using the different pulp samples for paper pulp performance testing after respectively carrying out latent elimination, acidification, washing, screening and dewatering concentration. According to the bamboo chemimechanical pulp bioenzyme pretreatment method disclosed by the invention, by carrying out pretreatment on bamboo bioenzyme, compared with a traditional PRC (Preconditioning Refiner Chemical)-APMP (Alkaline Peroxide Mechanical Pulping) technology, the difference in respects of pulp grinding energy consumption and pulp performance can be observed, and a reference technology is provided for preparing chemimechanical pulp by using bamboos as raw materials.
Owner:INST OF CHEM IND OF FOREST PROD CHINESE ACAD OF FORESTRY
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