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144 results about "Liquid fraction" patented technology

Upgrading of low value lipid feedstocks for refinery processing

A process is provided for upgrading low value lipid feedstocks for refinery processing. The process includes (a) treating a lipid feedstock comprising at least one fatty acid with a metal oxide catalyst on an oxide support under treating conditions to produce a treated stream, wherein the treating conditions include a temperature in a range of from 400° C. to 700° C.; a pressure in a range of from 0 to 10 MPa; and a liquid hourly space velocity in a range of from 0.1 to 10 h−1; and (b) fractionating the treated stream to obtain a gaseous fraction and a liquid fraction comprising a bio-oil; wherein the bio-oil has a lower content of oxygen and impurities as compared to the lipid feedstock.
Owner:CHEVRON USA INC

Upgrading of low value lipid feedstocks for refinery processing

A process is provided for upgrading low value lipid feedstocks for refinery processing. The process includes (a) treating a lipid feedstock comprising at least one fatty acid with a metal oxide catalyst on an oxide support under treating conditions to produce a treated stream, wherein the treating conditions include a temperature in a range of from 400° C. to 700° C.; a pressure in a range of from 0 to 10 MPa; and a liquid hourly space velocity in a range of from 0.1 to 10 h−1; and (b) fractionating the treated stream to obtain a gaseous fraction and a liquid fraction comprising a bio-oil; wherein the bio-oil has a lower content of oxygen and impurities as compared to the lipid feedstock.
Owner:CHEVRON USA INC

Machine for treating food products of vegetable origin for producing juice and related method for treating

Machine (1) for treating a food product of vegetable origin comprising a treatment section (10) provided with an inlet (11) for feeding the food product of vegetable origin to be treated and at least an outlet (12) for discharging a treated product. The treatment section (10) is equipped with a fixed hollow body (20), cylindrical, or conical, shaped, and a rotor (30) substantially cylindrical shaped and having a predetermined diameter ϕr, or substantially conical shaped and having a predetermined minimum diameter ϕr. The rotor (30) is mounted within of the fixed hollow body (20), is provided with a plurality of blades (35), and is operatively connected to a motor group (80) configured to cause a rotation of the rotor (30) about a rotation axis (130) at a predetermined rotation speed vr expressed in r.p.m.. The fixed hollow body (20) has an internal surface (21) comprising a plurality of impact surfaces (24) against which the plurality of blades (35) of the rotor (30) push the treated food product for subjecting the same to a succession of collisions and to cause, this way, the containment part of the food product to be broken and the liquid fraction, or juice, which is contained in the same to exit outside. The plurality of impact surfaces (24) is connected by a plurality of connection surfaces (26), and is oriented, in such a way to define with each blade (35) of the rotor (30) a predetermined impact angle (α)..
Owner:BERTOCCHI ALESSANDRO

Lithium and graphite recycled from black mass

The present invention relates to a composition comprising lithium carbonate obtained from black mass. The composition can be obtained by a process comprising (i) mixing black mass with a liquid to provide black mass slurry; (ii) converting lithium into a lithium salt in and removing graphite from the black mass slurry of step (i); (iii) separating dissolved lithium carbonate from solids in the black mass slurry of step (ii) to provide a lithium-enriched liquid fraction and a lithium-depleted solid fraction; optionally, reducing the lithium salt in the lithium-enriched liquid fraction of step (iii) to provide elementary lithium; (v) optionally, purifying the lithium salt in the lithium-enriched liquid fraction of step (iii) or the elementary lithium of step (iv); and (vi) optionally, solidifying the lithium salt of step (iii) or (v) or the elementary lithium of step (iv) or (v).
Owner:TOZERO GMBH

Thermal oscillation systems

A method and system for modulating vapor and liquid fractions of a cycling liquid-vapor fluid operating within its phase transition envelope by creating forced oscillating heat transfer between liquid and vapor fractions of the cycling stream. A liquid stream segment is expansion cooled and brought into thermal communication with a vapor stream segment. The contact with the expansion-cooled liquid enables intermolecular forces to drive condensation and release condensation heat at a condensation temperature higher than the temperature of the expansion-cooled stream segment. The resulting temperature gradient enables the expansion-cooled segment held at constant volume to capture the condensation heat and isochorically vaporize into a vapor stream segment that again is forced to condense so as to form an oscillating thermal cycle within the cycling liquid-vapor fluid.
Owner:EXENCY LTD

Green method for obtaining isothiocyanates from cruciferous vegetables

PCT designated stage expiredWO2025078970A1Vapor condensationEvaporationBrassicaceaeOrganic chemistry
The presently disclosure relates to a method of obtaining isothiocyanates (ITC) from frozen cruciferous vegetables using microwave gravity hydrodiffusion (MHG) technique, a solvent-free extraction technique. The advantages of this method are obtaining two liquid fractions (PLF + WLF) that can be used in different applications and a solid fraction (plant biomass) that can be reused, contributing to the preservation of biodiversity.
Owner:UNIVE CATOLICA PORTUGUESA

Albumin rich pea protein isolate and process for production thereof

The present disclosure provides an albumin enriched PPI extraction process and albumin enriched PPI produced by the process and use of albumin enriched PPI. The albumin enriched PPI extraction process comprises steps of a) protein extraction from aqueous solution comprising pea flour, b) separation of solids from the aqueous solution, producing a protein-rich liquid fraction, and c) precipitation of protein by use of Na, Ca, or Mg salt or combination thereof, thereby producing an albumin enriched PPI.
Owner:LOUIS DREYFUS CO PLANT PROTEINS LLC

Systems and devices and methods of making and using the same to prepare nut milk products

Systems and devices and methods of making and using the same to prepare nut milk products. An exemplary system of the present disclosure includes a blending device capable of blending a quantity of nuts with a quantity of a liquid to break down the quantity of nuts into pieces to generate a blended product, a porous vessel defining an opening and configured to strain the blended product so that when the blended product is introduced into the opening, at least part of a solid fraction of the blended product remains within the porous vessel, and at least part of a liquid fraction of the blended product passes through the porous vessel which is collected as a filtered or strained product, and a non-porous vessel configured to receive at least part of the porous vessel therein and further configured to receive the filtered or strained product.
Owner:ELEMENTAL DEVICE DESIGN LLC

System and method for determining at least one operating parameter of a biological treatment plant for biogas production with recovery of nitrogenous nutrients

The invention describes the coupling of a digester (110) with a bioelectrochemical system (120) in order to intensify the operation of the digester and recover the ammoniacal nitrogen contained in the digestate (3). The invention determines at least one operating parameter of the digester as a function of a value of a characteristic ratio of the digestate (3) or of the liquid fraction (3a) thereof, representative of an amount of biodegradable organic matter relative to an amount of ammonium ions. The value of this ratio is determined as a function (bi) of a target yield of ammonium ions extracted from the bioelectrochemical treatment system or of a target concentration of separated ammonium ions present in the bioelectrochemical treatment system, and (bii) of the value of at least one operating parameter of the bioelectrochemical treatment system representative of the capacity of the electrochemical treatment system to separate the ammonium ions and of the value of at least one quality parameter of the digestate or of the liquid fraction thereof.
Owner:SUEZ INTERNATIONAL

Plant for the thermal depolymerization of plastic waste

The invention relates to a system (1) for the thermal depolymerization of plastic waste, comprising a primary reactor (2) equipped with a heating device, an inlet (3) for feeding plastic waste, an outlet (27) for discharging an aerosol mixture, and an outlet (5) for discharging the solid residue, and the first condensation unit (4), which is equipped with the first primary vessel (10) and connected to the outlet (27) for discharging the aerosol mixture and is equipped with the outlet (6) for the liquid fraction and the outlet (7) for the gaseous fraction, further comprising a secondary reactor (8) equipped with a heating device and a catalyst and connected to the first condensation unit (4) via the outlet (6) for the liquid fraction, and further comprising the second condensation unit (9) which is connected to the secondary reactor (8).wherein a siphon-like pressure barrier (26) is arranged between the primary reactor (2) and the secondary reactor (8) and is placed in the first primary vessel (10).
Owner:ENRESS SRO

System and method for determining at least one operating parameter of a biological treatment plant for biogas production with nitrogen nutrient recovery

The invention describes the coupling of a digester (110) with a bioelectrochemical system (120) to intensify the operation of the digester and recover the ammoniacal nitrogen contained in the digestate (3). The invention determines at least one operating parameter of the digester as a function of a value of a ratio characteristic of the digestate (3) or its liquid fraction (3a), representative of a quantity of biodegradable organic matter relative to a quantity of ammonium ions.The value of this ratio is determined based on (bi) a target yield of ammonium ions extracted from the bioelectrochemical treatment system or a target concentration of separated ammonium ions present in the bioelectrochemical treatment system, and (bii) the value of at least one operating parameter of the bioelectrochemical treatment system representative of the electrochemical treatment system's capacity to separate ammonium ions, and the value of at least one quality parameter of the digestate or its liquid fraction. (Shorthand figure: Figure 1.)
Owner:SUEZ INTERNATIONAL

Liquid phase fraction collecting valve with liquid leakage detection and overpressure alarm device

The utility model discloses a liquid-phase fraction collecting valve with a liquid leakage detection and overpressure alarm device, which is integrally of a box structure and specifically comprises a case, a partition plate is arranged in the case and divides the case into a dry area and a wet area, and the partition plate and the case are sealed; the liquid leakage sensor is mounted in a liquid accumulation disc in a wet area on the front side of the case body; the liquid substrate is provided with a liquid inlet, a plurality of collection ports, a waste liquid port and an expansion port; wherein the liquid inlet is located at the foremost end, the collection opening is formed behind the liquid inlet, the collection opening is normally opened behind the collection opening, the waste liquid opening is closed only in a suction mode in a collection task, and the waste liquid opening is normally opened in other working stages; the plurality of electromagnetic valves are respectively connected with the plurality of collection ports and the waste liquid port, and the opening and closing of the collection ports and the waste liquid port are controlled through power-on opening and closing; and the pressure sensor is mounted on the liquid substrate and is positioned behind the liquid inlet and in front of the collecting opening. The liquid leakage alarm device has the functions of liquid leakage detection and overpressure alarm, and the safety and the reliability of laboratory equipment can be remarkably improved.
Owner:BEIJING QINGBOHUA TECH CO LTD

MILLERS' TALE OF THE DARKENBURY

Mealworm Larvae Protein Pate A mealworm larvae protein pate is prepared by heating blanched larvae. A pulp and a first separate liquid fraction, produced by placing the heated blanched larvae in a juice extractor, are then separated. The pulp is mixed with boiling water to create a diluted pulp. The diluted pulp is pulverized, preferably using a high-speed blender, until a homogeneous texture and color are achieved. A second extraction is carried out to produce a second separate liquid fraction. The first and second separate liquid fractions are combined to produce mealworm larvae protein juice, which can then be cooked with butter, egg yolks, and dry ingredients to produce mealworm larvae protein pate.
Owner:9326-2061 QUEBEC INC

Albumin rich pea protein isolate and process for production thereof

The present disclosure provides an albumin enriched PPI extraction process and albumin enriched PPI produced by the process and use of albumin enriched PPI. The albumin enriched PPI extraction process comprises steps of a) protein extraction from aqueous solution comprising pea flour, b) separation of solids from the aqueous solution, producing a protein-rich liquid fraction, and c) precipitation of protein by use of Na, Ca, or Mg salt or combination thereof, thereby producing an albumin enriched PPI.
Owner:LOUIS DREYFUS CO PLANT PROTEINS LLC

Process for treating lignocellulosic biomass

The invention relates to the treatment of lignocellulosic biomass: a) a pre-treatment step (2) to obtain pre-treated biomass (3), b) a first solid / liquid separation step of solid / liquid separation of the pre-treated biomass (3) obtained in step a) into a first solid fraction (7) of the pre-treated biomass and a first liquid fraction (6) comprising a compound mixture, the present invention relates to a method for preparing a biomass solid fraction (7), comprising the steps of: a) pre-treating a compound mixture comprising C5 and C6 sugars in part in monomeric form and in part in oligomeric form, c) a first enzymatic hydrolysis step (14) of a first pre-treated biomass solid fraction (7) obtained in step b) to obtain a hydrolysis product (15) in sugar form, d) a step (24) of treating the first liquid fraction (6) obtained in step b) by hydrolysis, e) a second enzymatic hydrolysis step (24) of a second pre-treated biomass solid fraction (7) obtained in step b) to obtain a hydrolysis product (15) in sugar form, and d) a third enzymatic hydrolysis step (24) of the second pre-treated biomass solid fraction (7) obtained in step b). To obtain a treated fraction enriched in monomeric form of C5 sugars and / or monomeric form of C6 sugars (26).
Owner:IFP ENERGIES NOUVELLES

Lithium and graphite recycled from black mass

The present invention relates to a composition comprising lithium carbonate obtained from black mass. The composition can be obtained by a process comprising (i) mixing black mass with a liquid to provide black mass slurry; (ii) converting lithium into a lithium salt in and removing graphite from the black mass slurry of step (i); (iii) separating dissolved lithium carbonate from solids in the black mass slurry of step (ii) to provide a lithium-enriched liquid fraction and a lithium-depleted solid fraction; optionally, reducing the lithium salt in the lithium-enriched liquid fraction of step (iii) to provide elementary lithium; (v) optionally, purifying the lithium salt in the lithium-enriched liquid fraction of step (iii) or the elementary lithium of step (iv); and (vi) optionally, solidifying the lithium salt of step (iii) or (v) or the elementary lithium of step (iv) or (v).
Owner:TOZERO GMBH

Process for purifying a reaction mixture obtained by an alkoxylation reaction

A reaction mixture (1) is obtained by an alkoxylation reaction of a nitrogenous compound selected from ammonia and amines, with an alkylene oxide. The reaction mixture (1) contains nitrogenous alkoxylation products and unreacted nitrogenous compound. A process for purifying the reaction mixture (1) comprises the steps of (1) introducing the reaction mixture (1) into a distillation tower (101), (2) providing thermal energy to the distillation tower (101) via a bottom reboiler (102) heated by medium pressure pressurized steam (2), (3) providing additional thermal energy to the distillation tower (101) by heating and partially evaporating a liquid in a reboiler (103) heated by low pressure pressurized steam (3), and directing the heated, partially evaporated liquid (4) to the distillation tower (101), wherein the liquid is the reaction mixture (1) to be introduced into the distillation tower (101) and / or a liquid fraction (5) withdrawn from the distillation tower (101) via a sidedraw (104), (4) withdrawing an unreacted nitrogenous compound stream (6) at the top (105) of the distillation tower (101), and (5) withdrawing an alkoxylation products stream (7) at the bottom (106) of the distillation tower (101). The process can use low temperature level heat to contribute to the heating of the reaction mixture in the distillation tower.
Owner:BASF SE

Quantitating corrosive naphthenic acids in crude oil

Processes for quantitating the corrosivity of naphthenic acids in a sample comprising crude oil or a liquid fraction thereof by reacting the sample with a metal comprising iron to produce iron naphthenates that are then stabilized by a ligand. The stabilized iron naphthenates are then analyzed by mass spectrometry to accurately quantitate the percentage of total naphthenic acids in the sample that are iron-reactive naphthenic acids associated with metal corrosion.
Owner:PHILLIPS 66 CO

Method and facility for treating an organic effluent for the production of biogas

The invention relates to a method for treating an organic effluent comprising a solid fraction and a liquid fraction, the method comprising the following steps: - digesting the organic effluent in a main anaerobic digester (6) at a temperature of between 5°C and 35°C to produce biogas, a main effluent and a main digestate; - degassing the main effluent in a main degassing module (10) to extract biogas present in dissolved form in the main effluent and produce a degassed main effluent; - biologically treating the degassed main effluent in a biological treatment unit (12) to produce a biological sludge; and - digesting the biological sludge in a secondary anaerobic digester (26) at a temperature of between 20°C and 65°C to produce biogas, a secondary effluent and a secondary digestate.
Owner:SUEZ INTERNATIONAL

Method for synthesizing low-viscosity PAO from coal-based α-olefins

The invention discloses a method for synthesizing low-viscosity PAO from coal-based alpha-olefins. The method comprises the following steps: S1, introducing Lewis acid gas BF3 into a coal-based alpha-olefin fraction section, carrying out a complex reaction between BF3 and oxygen-containing compounds in a coal-based alpha-olefin liquid fraction section at a pressure of 0.05 to 1 MPa to form a heterogeneous system of a BF3 complex and a coal-based alpha-olefin liquid, and then separating and removing the BF3 complex in the system to obtain a deoxidized coal-based alpha-olefin fraction section; S2, adding alcohol to the deoxidized coal-based alpha-olefin fraction section to carry out a polymerization reaction; and S3, separating the polymerization reaction mixture to obtain a polymer product and a BF3 complex, removing residual BF3 from the polymer product by flash evaporation and / or steam stripping, separating BF3 gas from the BF3 complex by gas-liquid separation, and returning the BF3 gas separated from the polymer product and the BF3 complex to step S1 for reuse.
Owner:PETROCHINA CO LTD

Fcc product vapor separation process for improved product recovery

This document discloses a system and method for separating cracked hydrocarbon mixtures. A main fractionation column separates the cracked hydrocarbon mixture into top, side, and bottom fractions containing C1 to C6+ hydrocarbons. A top condenser and high-pressure separation system partially condenses the top fraction and compresses the uncondensed vapor to produce a compressed gas fraction and a compressed liquid fraction. A first distillation column receives the compressed liquid fraction and separates it into a first top vapor and a first bottom fraction. A second distillation column separates the first bottom fraction into a second top fraction and a second bottom fraction. An absorber receives a portion of the second bottom fraction and the side liquid fraction and contacts it in countercurrent flow with the compressed gas fraction, thereby producing an absorber top fraction and absorber bottom fraction containing exhaust gas. Such a system can be used to integrate existing FCC / RFCC units with petrochemical complexes.
Owner:LUMMUS TECHNOLOGY INC

Method for separating material flows

Methods for separating a first material flow containing a dissolved substance are already known in which said first material flow is divided into a second material flow and a third material flow such that the third material flow has an increased concentration of the dissolved substance compared to the second material flow. In such methods, this is achieved by means of a freezing process in which the first material flow is pre-cooled in a heat exchanger and solidified in a heat pump, whereupon the ice is mechanically crushed and centrifuged, allowing the extraction of a liquid fraction containing the dissolved substance which does not integrate into the ice lattice. In such a method, the invention provides a second heat pump which only takes over the heat transfer in the region of the freezing point, meaning that its efficiency is particularly high due to the substantially constant temperature on both sides.
Owner:LÜDTKE NORMAN

Process for producing a membrane protein

A process for the production of a membrane protein is provided. The process including the steps of: expressing a membrane protein in a host organism present in an aqueous medium, liberating the membrane protein from the host organism, adding a detergent solution to solubilize the membrane protein, recovering a liquid fraction of the solubilized membrane protein, subjecting the liquid fraction to chromatography to bind or retain the membrane protein on a stationary phase, and eluting the stationary phase with an elution buffer to produce the membrane protein. The process can produce relatively large amounts of membrane proteins in an efficient way without compromising the quality of the end product.
Owner:E & J GALLO WINERY

Method for treating a petrol containing sulphur compounds

A process for treating a gasoline containing sulfur compounds, olefins and diolefins comprises step a) bringing into contact the gasoline, hydrogen and a hydrodesulfurization catalyst, in at least one reactor. In step b) effluent from a), hydrogen, and a hydrodesulfurization catalyst are brought into contact in at least one reactor. In step c) effluent from b) is sent to a separation drum operating at a pressure of between 1.0 and 2.0 MPa to obtain a gaseous fraction containing H2S and hydrogen and a liquid fraction containing desulfurized gasoline and a fraction of dissolved H2S. In step d), the liquid fraction is sent to a stabilization column to obtain at the top a stream comprising residual H2S and C4- hydrocarbon compounds and at the bottom a stabilized gasoline. In step e), the gaseous fraction is recycled at least in part to at least one of steps a) and / or b).
Owner:IFP ENERGIES NOUVELLES

Reuse of bioplastics in polymerisation

The present invention relates to a process for reusing a polymer composition comprising at least one biodegradable polyester, starch and / or additives, comprising the steps of: (1) contacting said biodegradable polymer composition with a first solvent comprising from 50 to 100% by weight of cyclopentanone, obtaining a liquid fraction comprising at least one biodegradable polyester and a solid fraction comprising insoluble starch and / or additives; (2) separating said liquid fraction comprising at least one polyester from said solid fraction; (3) at least partially removing said first solvent from said liquid fraction; (4) reusing the polyester obtained from said liquid fraction in a polymerisation or thermoplastic transformation process, thereby obtaining a biodegradable polymer composition. Biodegradable polyesters obtained by means of the said reutilisation process, biodegradable polymer compositions comprising them, and biodegradable articles obtained therefrom constitute further objects of the invention.
Owner:NOVAMONT SPA

Method for recovering ammonia in a biogas plant and biogas plant

The present invention is intended to lower the FOS / TAC ratio of the material to be stripped, thereby enabling a higher pH of the material, and to enhance the stripping conditions of the material in an ammonia recovery unit (4) of a biogas plant having at least one ammonification reactor (1) for processing an input raw feedstock into a pretreated feedstock, and at least one biogas reactor (2) for fermenting the pretreated feedstock into biogas and a fermentation digestate, the fermentation digestate being separated into a solid fraction and a liquid fraction in a fermentation digestate separator (5). At least a portion of the separated liquid fraction is directed as a return liquid having a low FOS / TAC ratio via a return liquid conduit (10) to a pretreated feedstock blending device (12) where the return liquid is mixed with a pretreated feedstock having a higher FOS / TAC ratio, and / or to a liquid blending device (13) where the return liquid is mixed with a separated liquid from the pretreated feedstock, and this mixed material having an intermediate FOS / TAC ratio is then fed to the ammonia recovery unit (4).
Owner:DUCTOR

Method for controlling the internal pressure of a cryogenic tank

The invention relates to a method for controlling the internal pressure of a cryogenic tank (100) containing a liquid fraction (1002) and a gaseous fraction (1004) of a fluid whose enthalpy can decrease during isothermal compression in the liquid phase. Figure for the abstract: Figure 3
Owner:ALFA LAVAL SWITZERLAND AG

Mealworm spread

A mealworm larvae protein spread is prepared by reheating blanched larvae. A pulp and a first separated liquid fraction produced by placing the reheated blanched larvae in a juice extractor are then separated. The pulp is mixed with boiling water, creating a diluted pulp. The diluted pulp is pulverized, preferably using a high shear mixer, until it acquires a homogeneous texture and color. A second extraction is performed producing a second separated liquid fraction. The first separated liquid fraction and the second separated liquid fraction are combined, producing the mealworm larvae protein juice which may then be cooked with butter, egg yolks and dry ingredients to produce the mealworm larvae protein spread.
Owner:9326-2061 QUEBEC INC

Hydroliquefaction of carbonaceous feedstock

Herein is described a method for the production of liquid hydrocarbon composition, comprising i) providing carbonaceous feedstock (a); ii) subjecting the carbonaceous feedstock (a) to catalytic hydroliquefaction (10) in the presence of hydrogen to obtain a product mixture comprising liquid hydrocarbons and off-gas; iii) separating (20) the liquid hydrocarbons and the off-gas to obtain a first liquid fraction (b-1) and a first gaseous fraction (c-1) iv) converting (30) in gas phase at least part of the light oxygenates comprised in the first gaseous fraction (c-1) and v) converting in the presence of water steam at least part of the carbon monoxide (CO) comprised in the first gaseous fraction (c-1) and / or produced in step iv) to carbon dioxide (CO2) and hydrogen (H2) by water gas shift reaction, to obtain a CO2 and H2 enriched first gaseous fraction (c-1e); and vi) separating (40) non-condensables from the CO2 and H2 enriched first gaseous fraction (C-1e) to obtain a second gaseous fraction (c-2) and a second liquid fraction (b-2); vii) recovering (50) at least part of H2 from the second gaseous fraction (c-2) and recirculating at least part, of the recovered H2 to step ii); viii) recovering the first liquid fraction (b-1) and / or the second liquid fraction (b-2) to provide a liquid hydrocarbon composition.
Owner:NESTE OYJ

Method and apparatus for purifying ethylene carbonate

The present invention relates to a process for purifying ethylene carbonate from a crude ethylene carbonate composition, said process comprising the steps of: a) subjecting a crude composition comprising ethylene carbonate to at least one distillation step to obtain a pre-purified composition comprising at least 99.5% by weight of ethylene carbonate; and b) subjecting the pre-purified composition obtained in step a) to at least one melt crystallization step to obtain a purified ethylene carbonate composition wherein the process is carried out in a plant comprising at least one distillation column, one vessel, at least one crystallizer and a feed line for a crude composition containing ethylene carbonate, wherein, if the apparatus comprises one distillation column, the distillation column, or, if the apparatus comprises two or more distillation columns, the first distillation column, comprising a top outlet line, a bottom outlet line and a side outlet line, wherein the at least one crystallizer comprises an inlet line for the pre-purification of the composition and an outlet line for the purification of the ethylene carbonate composition, and wherein the side outlet line of the distillation column is directly or indirectly connected to the inlet line of the at least one crystallizer for the pre-purification of the composition, wherein i) or the vessel is connected to the feed line for the crude composition containing ethylene carbonate and to an inlet line, where the inlet line is connected to a gas outlet of a first reboiler, where the first reboiler is further connected to a bottom outlet line of the distillation column, where the vessel further comprises an outlet line, where the outlet line is connected to a gas outlet of a second reboiler, where the first reboiler is further connected to a bottom outlet line of the distillation column. The outlet line leads to the inlet line of the distillation column via a second reboiler, in which a bottom fraction of the distillation column withdrawn from the distillation column via the bottom outlet line is partially evaporated in the first reboiler to obtain a gas fraction and a liquid fraction, or ii) the feed line for the crude composition containing ethylene carbonate is introduced into the distillation column, where the bottom outlet line of the distillation column leads to the vessel via a first reboiler, where the vessel comprises a gas outlet connected to the inlet line of the distillation column, where the bottom outlet line of the distillation column leads to the vessel via a second reboiler, where the gas outlet is connected to the inlet line of the distillation column. And the container comprises a liquid outlet which is connected with a pipeline leading into a second reboiler, the second reboiler comprises a gas outlet which is connected with an inlet pipeline of the distillation column, and the gas outlet is connected with a gas outlet of the distillation column. Wherein a bottom fraction of the distillation column withdrawn from the distillation column via the bottom outlet line is partially evaporated in the first reboiler, and wherein at least a portion of a gas fraction obtained in the first reboiler is recycled to the distillation column via the inlet line.
Owner:SULZER MANAGEMENT AG