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42 results about "Unsaponifiable" patented technology

Unsaponifiables are components of an oily mixture that fail to form soaps when blended with sodium hydroxide. Since saponifiable components of the original oil mixture do form soaps, the result of a soap making procedure is a mixture of soaps and other, frequently oily, materials. Unsaponifiable constituents are an important consideration when selecting oil mixtures for the manufacture of soaps. Unsaponifiables can be beneficial to a soap formula because they may have properties such as moisturization, conditioning, vitamins, texture, etc. On the other hand, if the proportion of unsaponifiables is too high, or the specific unsaponifiables present do not provide significant benefits, a defective or inferior soap product can result.

Method for extracting unsaponifiable matters from shea butter oil

ActiveCN103445996AImprove nutritional application valueReduce cosmetic effectCosmetic preparationsFatty acid esterificationShea butterChemistry
The invention provides a method for extracting unsaponifiable matters from shea butter oil. The method comprises the steps of ester exchange, molecular distillation, crystallization and the like. An unsaponifiable matter composition with high purity can be obtained by adopting the method. The content of the unsaponifiable matters in the composition can reach 60%, 70% or even higher; the composition contains high contents of triterpene alcohols and sterol which can exist in the form of solids; the shelf life of the unsaponifiable matters is prolonged; the unsaponifiable matters can be applied to various purposes.
Owner:WILMAR SHANGHAI BIOTECH RES & DEV CENT

Process for the isolation of oryzanols from rice bran oil soap stock

The present invention relates to a process for the isolation of oryzanols from rice bran oil soap stock by (a) saponifying the oil present in soap stock with an alkali followed by neutralisation of the excess alkali, (b) converting the soap stock into anhydrous, porous soap noodles, (c) extracting the soap noodles with an organic solvent, (d) crystallising the crude unsaponifiable matter to remove impurities, (e) subjecting the residue to column chromatography to obtain an oryzanol rich fraction, and (f) recrystallising the oryzanol rich fraction using an organic solvent to obtain pure oryzanol.
Owner:COUNCIL OF SCI & IND RES

Process for preparing vegetable oil fractions rich in non-tocolic, high-melting, unsaponifiable matter

A vegtable oil fraction rich in non-tocolic, high-melting, unsaponifiable matter is prepared by the following steps: A vegetable oil having a slip melting point of not more thatn 30° C. and a content of unsaponifiable matter of at least 0.5% by weight is hydrongenated to fully saturate the fatty acids of the glycerides and to reach a slip melting point of at least 57° C. To the hydrongenated oil is added from 1 to 75% by weight of the unhydrogenated starting oil or another oil having a slip melting poing of not more than 30° C. in order to act as a carrier and vehicle for the unsaponifiable matter. Then, a solvent is added to the oil mixture in a ratio between oil and solvent from 1:2 to 1:20, and the mixture is heated to transparency. The oil / -solvent-mixture is cooled in one or more steps to a final temperature in the range from -35 to +30° C., and the precipitated high-melting fraction(s) is (are) filtered off. The filtrate is desolventised, leaving a fraction rich in unsaponifiable matter. By this process very high concentrations of in particular the non-tocolic, higher melting unsaponifiables can be achieved, and the composition of the glyceridic part of the enriched fraction can betailored to specific applications. Also, a novel blood cholesterol-lowering effect of the unsaponifiable constituents from shea butter has been found.
Owner:AAK DENMARK

Process for preparing vegetable oil fractions rich in non-tocolic high-melting, unsaponifiable matter

A vegtable oil fraction rich in non-tocolic, high-melting, unsaponifiable matter is prepared by the following steps: A vegetable oil having a slip melting point of not more thatn 30 DEG C. and a content of unsaponifiable matter of at least 0.5% by weight is hydrongenated to fully saturate the fatty acids of the glycerides and to reach a slip melting point of at least 57 DEG C. To the hydrongenated oil is added from 1 to 75% by weight of the unhydrogenated starting oil or another oil having a slip melting poing of not more than 30 DEG C. in order to act as a carrier and vehicle for the unsaponifiable matter. Then, a solvent is added to the oil mixture in a ratio between oil and solvent from 1:2 to 1:20, and the mixture is heated to transparency. The oil / -solvent-mixture is cooled in one or more steps to a final temperature in the range from -35 to +30 DEG C., and the precipitated high-melting fraction(s) is (are) filtered off. The filtrate is desolventised, leaving a fraction rich in unsaponifiable matter. By this process very high concentrations of in particular the non-tocolic, higher melting unsaponifiables can be achieved, and the composition of the glyceridic part of the enriched fraction can betailored to specific applications. Also, a novel blood cholesterol-lowering effect of the unsaponifiable constituents from shea butter has been found.
Owner:AAK DENMARK

Method for extracting unsaponifiable matter from vegetable oil and application

The invention discloses a method for extracting unsaponifiable matter from vegetable oil, and the method specifically comprises the following steps of (1) adding a high-alkali saponification solutionto a vegetable oil sample for vortex shock for 0.5 to 0.7min and for subsequent saponification treatment under the effect of ultrasonic heating; (2) after the saponification treatment of the vegetableoil sample, firstly adding deionized water to a treatment solution for shaking to dilute, adding n-hexane to extract the unsaponifiable matter, leaving the treatment solution to stand after extracting the unsaponifiable matter once until the layering of an aqueous phase and an organic phase to complete the extraction of the unsaponifiable matter; (3) designing an SPE cartridge dedicated to waterand soap removal, and adsorbing the organic layer at the bottom after standing and layering to pass through the SPE cartridge for water and soap removal treatment, wherein the SPE cartridge is provided with a lower sieve plate, the lower layer is filled with 1/3 column volume of anhydrous sodium sulfate, and the upper layer is filled with 1/3 column volume of 3A molecular sieve; and (4) collectingthe effluent that passes through the SPE cartridge after water and soap removal in an evaporating dish, evaporating the solvent completely, and collecting infrared spectrums of the unsaponifiable matter for analysis.
Owner:仕宝(天津)技术检测有限公司

Multi-effect nursing cosmetic composition for infants

ActiveCN113599319AQuick and effective treatment for dry chapped skinQuick and effective treatment of sensitive muscle symptomsCosmetic preparationsToilet preparationsPimpleGlycerol
The invention discloses a multi-effect nursing cosmetic composition for infants. The multi-effect nursing cosmetic composition is prepared by selecting various functional components such as glycosylglycerol, vaccinium myrtillus seed oil, high-molecular-weight sodium hyaluronate, hydrolyzed algae extract, coconut oil alcohol-octoate/caprate and sunflower seed oil unsaponifiable matter, and adding Vernix-Care and three composite skin conditioning components at the same time. The texture improver is supplemented, and all the components cooperate with one another, so that the composition has multiple effects of long-acting moisturizing, relieving and anti-allergy, red skin eliminating and anti-inflammation, itching relieving and repairing and the like, and can be used for quickly and effectively treating sensitive skin symptoms such as infant skin dryness, chap and tension, red apple skin and papule accompanying pruritus and the like. Tests prove that the cosmetic composition disclosed by the invention is high in safety, mild and non-irritant, the skin feeling is soft, comfortable and non-sticky after the cosmetic composition is used, the skin burden of infants is relieved, and the cosmetic composition has a remarkable effect of improving and repairing sensitive skin of the infants.
Owner:ZHONGSHAN AIHU COMMODITY

Method for simultaneously preparing rare ginsenoside and grease unsaponifiable matter

The invention, which belongs to the field of ginseng extract preparation methods, provides a method for simultaneously preparing rare ginsenoside and a grease unsaponifiable matter. The method comprises the following steps: processing dried ginseng into powder, adding petroleum ether, sodium hydroxide, n-butyl alcohol, ethanol and water, and performing extracting by using a stirring device; afterextraction finishing, performing standing, taking an upper-layer solution, and performing concentrating under a reduced pressure or normal pressure to obtain a ginseng grease unsaponifiable matter; taking a lower-layer solution, performing concentrating, performing treatment with a macroporous resin column, performing eluting with water until an ethanol eluent is colorless, clear and transparent,performing eluting with an ethanol solution until the ethanol eluent is colorless, clear and transparent, collecting the ethanol eluent, recovering ethanol, and performing drying to obtain the dry extract-like rare ginsenoside. The method can be used for preparing rare ginsenoside and a grease unsaponifiable matter at the same time and is convenient, efficient, and easy to operate; the cost is low; and the utilization rate of ginseng is increased. The development and utilization requirements in the fields of medicines, foods and chemical engineering are met. The method for simultaneously preparing rare ginsenoside and a grease unsaponifiable matter has the great application and development values.
Owner:CHANGCHUN NORMAL UNIVERSITY

Solid/liquid extraction

InactiveCN102724887ACosmetic preparationsFatty acid esterification2-Methyl propane2-ethoxy-2-methylpropane
The invention relates to a method for the solid / liquid extraction of an oil or butter, particularly having a high unsaponifiable content, contained in at least one solid vegetable matter or a micro-organism. The method includes at least the following steps: solid / liquid extraction of at least one solid vegetable matter or a micro-organism using a first solvent system comprising a concentration of solvent selected from among fluorinated aromatic solvents, particularly trifluorotoluene (BTF) and hexafluorobenzene (BHF), tert-butyl ethers, particularly 2-ethoxy-2-methylpropane, also known as ethyl-tert-butyl-ether (ETBE), and 2-methoxy-2-methylpropane or methyl-tert-butylether (MTBE), solvents comprising at least one silicon atom, particularly hexamethyldisiloxane (HMDS) and tetramethylsilane (TMS), methyl-tetrahydrofuran (MeTHF), and mixtures thereof, representing at least 50 vol.-% in relation to the total volume of the solvent system; and, optionally, recovery of a fraction comprising the oil or butter, particularly unsaponifiable enriched. The invention also relates to an unsaponifiable fraction, oil or butter obtained using this method and to compositions containing said oil or fraction.
Owner:LAB EXPANSCIENCE

Protective cream and preparation process thereof

The invention discloses protective cream and a preparation process thereof. The protective cream comprises a component A, a component B and a component C, wherein the component A comprises the following raw materials in parts by weight: 8-12 parts of butanediol, 4-6 parts of meadowfoam seed oil, 2.5-3.5 parts of jojoba esters, 3-5 parts of sunflower seed oil unsaponifiable matters, 1.1-2.9 parts of moringa pterygosperma seed oil, 1.6-2.4 parts of oat kernel oil and 2-4 parts of a first skin conditioner; the component B comprises the following raw materials in parts by weight: 60.3-64.3 parts of water, 1.3-2.7 parts of a second skin conditioner and 0.4-0.9 part of carbomer; and the component C comprises the following raw materials in parts by weight: 0.7-1.3 parts of an extract of roots ofradix sophorae flavescentis, 0.3-1.3 parts of a fructus cnidii extract, 0.1-0.3 part of arginine, 0.1-0.2 part of chlorhexidine diacetate and 0.4-1.6 parts of a moisturizer. The protective cream has the effects of improving skin barrier repair, promoting regeneration of epidermal lipid and adjusting the composition thereof, strengthening intercellular adhesion, and preserving moisture for a long time, and has a relieving effect, and thus, the skin condition is improved; and in addition, the invention further provides the preparation process of the protective cream. The protective cream has theadvantages of improving the properties and quality of a final product.
Owner:JOTM DAILY CHEM HANGZHOU CO LTD

Application of morpholine in controlling unsaponifiable matter content in schizochytrium limacinum fermentation process and increasing DHA grease content

The invention discloses application of morpholine in controlling unsaponifiable matter content and increasing DHA grease content in a schizochytrium limacinum fermentation process, and aims to reduce sterol content and increase grease content in the schizochytrium limacinum fermentation process by exogenously adding morpholine in the schizochytrium limacinum fermentation process. In addition, optimum addition concentration of morpholine is determined according to the biomass of cell growth of schizochytrium limacinum, the oil yield and the unsaponifiable matter content index; compared with the situation that 1.8 g / L of morpholine is added, the sterol content is reduced by 64.86%, the oil yield is increased by 67.51%, the DHA content is increased by 25.5%, and the astaxanthin content is increased by 85%. By means of the technical scheme, the content of DHA grease and astaxanthin produced by the schizochytrium limacinum is obviously improved. In the invention, the morpholine is applied to regulation and control of the unsaponifiable matter content of schizochytrium limacinum for the first time, wherein a new thought is provided for increasing the content of grease in schizochytrium limacinum, and the method has huge potential in the aspect of industrial production.
Owner:NANJING NORMAL UNIVERSITY

Supercritical fluid extraction method of sword iris seed oil and application thereof

The invention relates to the technical field of sword iris seed oil extraction, in particular to a supercritical fluid extraction method of sword iris seed oil and application thereof. The method specifically comprises three steps: raw material treatment, supercritical fluid extraction condition optimization and supercritical fluid extraction. The supercritical fluid extraction method is simple, convenient, rapid and accurate, the average yield of sword iris seed oil is 11.15%, and the relative error between the average yield and a theoretical value is 0.53% and is higher than the existing yield of sword iris seed oil. The content of unsaponifiable matters in the obtained sword iris seed oil is 1.31%, 40 components are identified in total, the total content of eight sterol compounds is upto 87.44%, betulinaldehyde is identified in iris plants for the first time; there are 18 kinds of fatty acids, the unsaturated fatty acids account for about 85%, the polyunsaturated acids account for54.87%; more than 30 volatile components exist; the average content of total polyphenol is 49.83 mg/kg, and the obtained sword iris seed oil has strong antioxidant activity, can be applied to cosmetics, foods and medicines, and can also be applied to industry.
Owner:CHINA ACAD OF SCI NORTHWEST HIGHLAND BIOLOGY INST
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