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174 results about "Evaporating dish" patented technology

An evaporating dish or watch glass is a piece of laboratory glassware used for the evaporation of solutions and supernatant liquids, and sometimes to their melting point. Evaporating dishes are used to evaporate excess solvents – most commonly water – to produce a concentrated solution or a solid precipitate of the dissolved substance.

Lycium ruthenicum Murr effective extract and its extraction method and use

The invention discloses Lycium ruthenicum Murr effective extract and its extraction method and use. The extraction method comprises the following steps of carrying out vacuum drying of Lycium ruthenicum Murr, crushing it, adding 95% of ethanol into the crushed Lycium ruthenicum Murr, carrying out backflow 2 times, wherein each backflow process lasts for 1h, carrying out filtration, carrying out distillation of the filtrate at a temperature of 75 DEG C for concentration, transferring the concentrate into an evaporating dish, carrying out water-bath evaporation, carrying out vacuum drying at a temperature of 70 DEG C for 2h to obtain dry extract, adding methanol into the dry extract until a constant volume is realized, filtering by an organic microporous filter membrane having the aperture size of 0.45 microns and carrying out procyanidine extraction. The Lycium ruthenicum Murr effective extract obtained by the scientific and reasonable extraction method has novel purposes of reducing blood pressure, blood fat and blood sugar. The extraction method provides a novel measure for effective and full utilization of the Lycium ruthenicum Murr effective extract in products for treating or preventing diabetes, hyperlipidemia and hypertension. The extraction method shortens extraction separation time, reduces energy consumption in processes, and effectively reduces a production cost. The Lycium ruthenicum Murr effective extract has high purity, stable performances, fewer extract impurities and good quality. The extraction method adopts pharmaceutical health-care products having antioxidation effects.
Owner:SHANGHAI GENE CELL BIO MEDICAL TECH

Method for synthesizing manganese lithium phosphate/carbon serving as positive material of lithium ion battery

The invention discloses a method for synthesizing manganese lithium phosphate/carbon serving as a positive material of a lithium ion battery. The method comprises the following steps of: 1) mixing materials, namely adding a lithium source compound, a phosphorous source compound and a manganese source compound serving as raw materials into a ball mill jar, adding a carbon source compound, adding liquid medium until the raw materials and the carbon source compound are immersed and ball-milling until all the materials are uniform; 2) drying the ball-milled mixture, namely taking the mixture obtained in the step 1) out, putting into an evaporating dish, drying and grinding into powder; and 3) calcining at a high temperature, namely calcining the mixture powder obtained in the step 2) in an inert atmosphere at the temperature of between 500 and 800 DEG C for 1 to 12 hours to obtain the carbon-coated manganese lithium phosphate. The method has a simple synthesis process and easily controlled experimental conditions, the production cost of the manganese lithium phosphate is reduced, and the implementation of industrial production is facilitated; and the prepared positive material of the lithium ion battery has high electrochemical performance.
Owner:GUANGZHOU HKUST FOK YING TUNG RES INST

Method for preparing nanometer nitro celluloses

The invention relates to a method for preparing nanometer nitro celluloses, and belongs to the technical field of special chemical engineering. The preparation method comprises the following steps of: 1, performing ultrasonic pre-treatment on cotton cellulose powder in ice bath, and performing pumping filtration and drying on the cotton cellulose powder for later use; and soaking the cellulose powder in sulfuric acid solution at a certain concentration, controlling a solid-liquid ratio within 17.5 to 50g/mL, stirring the mixed solution to perform reaction in water bath at the temperature of between 45 and 75 DEG C for certain time, adding water to dilute the mixed solution, performing the centrifugal separation on the reaction solution until a pH value of the mixed solution is 6 to 7, and ultrasonically dispersing the mixed solution to obtain the stable nanometer cellulose crystal whisker suspension; 2, adding a proper amount of nitric acid into the nanometer cellulose crystal whisker suspension so as to make the nanometer cellulose crystal whisker suspension reach the needed concentration, adding water to dilute the mixed solution, and performing centrifugation and washing until the pH value of the mixed solution is 6 to 7; and 3, moving precipitates to an evaporating dish, and performing vacuum drying on the precipitates at the temperature of 50 DEG C to obtain the nanometer nitro cellulose powder. In the method, because the composition of the acid is single, the post-treatment and the reutilization of the acid are convenient; and the nitrifying time is shortened, and the stability is improved; and the nanometer nitro celluloses can be used as the energetic reinforcing materials.
Owner:BEIJING INSTITUTE OF TECHNOLOGYGY

Irrigation prediction system based on automatic water supplementing evaporating dish

PendingCN106613786ASolve the problem of low accuracy in measuring actual evaporationRealize intelligent measurementWatering devicesCultivating equipmentsEvaporating dishEngineering
The invention discloses an irrigation prediction system based on an automatic water supplementing evaporating dish. The irrigation prediction system comprises a water supplementing device (3), the evaporating dish (5), a metering dish (8), a rain cover (16) and a central processing unit (9); a communicating pipe (12) is connected between the water supplementing device (3) and the evaporating dish (5), a valve a (13) is installed on the communicating pipe (12), an overflow pipe (6) is connected between the evaporating dish (5) and the metering dish (8), and the rain cover (16) is installed at one side of the evaporating dish (5); the central processing unit (9) comprises a clock module, a processing module, a storing module, a weather forecast module, a program setting module, a communication module, a control module and a display screen. The irrigation prediction system has the advantages that intelligent control over evaporation capacity observation is achieved, and the observation precision is improved; the water demand of crops is predicted according to the observed evaporation capacity of the evaporating dish, and the crop irrigation schedule is made by combining a weather forecast system.
Owner:SICHUAN UNIV

Farm irrigation indicating device and use method thereof

The invention discloses a farm irrigation indicating device, which comprises an evaporating dish and a water-replenishing sealing box, wherein the evaporating dish is covered with a mesh cover corresponding to the growth period of crop; the water-replenishing sealing box is connected with the evaporating dish via a connecting pipe; the water level in the water-replenishing sealing box can be displayed by self; the water-replenishing sealing box is provided with a water filling hole with a sealing plug; the top cover of the water-replenishing sealing box is provided with a ventilating pipe in integral structure with the top cover; the ventilating pipe is inserted into the water-replenishing sealing box; the end part of the ventilating pipe is near the bottom of the water-replenishing sealing box; and the connecting pipe is provided with a tong. According to the farm irrigation indicating device disclosed by the invention, the farm water consumption amount can be accurately reflected, and the production cost is low. The invention also discloses a use method used for the farm irrigation indicating device. The method is favorable for the device to accurately reflect the farm water consumption amount and is convenient for the device to indicate the reasonable irrigation time.
Owner:FARMLAND IRRIGATION RES INST CHINESE ACAD OF AGRI SCI

Method used for simultaneous extraction of radix isatidis polypeptides and polysaccharides

The invention discloses a method used for simultaneous extraction of radix isatidis polypeptides and polysaccharides. The method comprises following steps: radix isatidis is smashed, and is immersed in ethyl acetate, an obtained solution is filtered, and an obtained filter cake is washed with distilled water for 3 to 5 times, and is dried; the filter cake is immersed in distilled water for 1 to 2h, and is subjected to ultrasonic treatment for 10 to 80s; an obtained mixed solution is heated to 60 to 90 DEG C, is stirred for 1 to 3h at a stirring speed of 120 to 300rpm, and is filtered, and a filtrate is collected; an obtained filter cake is immersed in distilled water for 1 to 2h, is heated, and is subjected to acid alkali adjustment respectively, an obtained mixture is stirred for 1 to 3h at a stirring speed of 120 to 300rpm, and is filtered, and a filtrate is collected; the filtrates obtained via the above steps are mixed, and an obtained mixed material is delivered into an evaporating dish for evaporation and concentration, ethyl alcohol is added, an obtained product is allowed to stand for 12 to 24h, and is subjected to centrifugation, a supernatant is discarded, an obtained precipitate is collected, and is subjected to vacuum drying so as to obtain a polypeptide and polysaccharide mixture. The method can be used for simultaneous extraction of radix isatidis polypeptides and polysaccharides; operation is simple; polypeptides extraction rate is as high as 95.45%; polysaccharides extraction rate is as high as 92.48%; and impurity content is less than 5%.
Owner:SUZHOU COSMETIC MATERIALS

Method for preparing barium-cobalt-iron-niobium composite oxide with a low-temperature self-propagating combustion method

The present invention belongs to a method for preparing barium-cobalt-iron-niobium oxide powder and is applied to the field of oxygen permeable membrane. The invention is characterized by comprising the following steps: firstly combining the treated Nb2O5, Ba(NO3)2, Co(NO3)2*6H2O and Fe(NO3)3*6H2O according to a stoichiometric proportion for preparing into an uniform transparent water solution, adding appropriate amount of complexing agent of lemon acid and glycin for obtaining a clear precursor solution; after evaporating most of water in the precursor solution, transferring the solution into an evaporating dish and heating when the temperature is controlled to 200-300 DEC C until the heating is finished for obtaining the fleecy primary powder; calcining the primary powder for 5 hour in the temperature of 950 DEG C for obtaining the final product Ba1.0Co0.7Fe0.2Nb0.1O3-delta in the cubic perovskite phase. The device required by the method is few and the consumed time is little. The molecule-level homogeneous mixing and accurate and controllable chemometry can be obtained. The obtained product has the advantages of fine particle and high purity. The phase-forming temperature of cubic phase is reduced. The interval between the pure cubic phase material synthesis and the fusion temperature of material is enlarged. The baking of tube oxygen permeable device is facilitated.
Owner:UNIV OF SCI & TECH BEIJING

Method for preparing high-purity bismuth oxide

The invention belongs to a method for preparing high-purity bismuth oxide, which comprises the steps: (1) metal bismuth is added to a stainless steel reaction vessel after being washed by high-purity water, the high-purity water and high-purity nitric acid are added to carry out a heating reaction; the reactant is filtered after being cooled; the filtrate is condensed and cooled to obtain crystals; (2) the crystals in the step (1) are dissolved into a saturated solution by high-purity water; the saturated solution is added to the stainless steel reaction vessel and hydrolyzed under the stirring for standing; the bismuth subnitrate is completely precipitated; the supernatant liquor is eliminated; the precipitation is pumped; the pumped precipitation is washed by high-purity water, pumped and dried; the dried bismuth subnitrate is pulverized and added to a ceramic evaporating dish; then the pulverized bismuth subnitrate is transferred to a muffle furnace to be baked; the baked bismuth subnitrate is pulverized after being cooled; and the pulverized bismuth subnitrate is added to the muffle furnace to be baked and cooled so as to obtain the high-purity bismuth oxide finished product. The method for preparing the high-purity bismuth oxide has the advantages of simple process step and high production efficiency, and the high-purity bismuth oxide has the advantages of low impurity content and high purity.
Owner:TIANJIN CHEM REAGENT RES INST

Bonsai automatic irrigating and water-supplying device and applying method thereof

The invention relates to a bonsai automatic irrigating and water-supplying device and an applying method thereof, and belongs to the technical field of horticulture irrigation. The method comprises the steps of firstly injecting water into an evaporating dish water supplying device and an evaporating dish separately till the water level reaches an initial water level line and an evaporating dish initial water level line, setting a bonsai water allowable transpiration amount and a water level warning line, and using the evaporating dish to simulate bonsai water dissipation. Under the effect of the atmospheric evaporation power, the water level of the evaporating dish is lowered, the water in bonsai soil is also dissipated and reduced under evaporation and transpiration effects, when the evaporation amount of the evaporating dish reaches the bonsai water allowable transpiration amount, a water pressure sensor detects a signal and transmits the signal to an irrigating valve, the irrigating valve is switched on, so that the water in a bonsai water supplying device flows into a water-injecting sand layer at the bottom of a bonsai flowerpot, and thus automatic irrigating and water-supplying of bonsai plants are achieved. According to the bonsai automatic irrigating and water-supplying device and the applying method thereof, it is unnecessary to specially assign people to maintain the bonsai automatic irrigating and water-supplying device, the air humidity and temperature can be adapted to, the watering time is determined through an evaporation amount, so that the water control amount is more accurate, a large amount of labor is saved, and thus the bonsai automatic irrigating and water-supplying device has a wide application prospect.
Owner:刘凡领

Method for detecting content of total nonvolatile matters in high-purity and ultra-pure ammonia

The invention discloses a method for detecting content of total nonvolatile matters in high-purity and ultra-pure ammonia. The method comprises the following steps of: directly introducing ammonia into a volumetric flask and dissolving the ammonia in water, weighing a mass difference of the volumetric flask before and after the ammonia is dissolved, calculating the ammonia mass, slowly heating a ammonia water solution, releasing the ammonia through low-temperature evaporation, and then setting the heating temperature to be 100+/1 DEG C; pouring the ammonia water solution into an evaporating dish after the ammonia water solution is volatilized to a scale line of 100mL; heating the solution on an oven with the temperature of 100+/5 DEG C for 30 minutes after the ammonia water in the evaporating dish is totally evaporated; cooling in a dryer for 15 minutes; analyzing the scale weight and recording the reading; and finally, proportioning the mass difference of the ammonia water solution before and after the ammonia water solution is evaporated in the evaporating dish to the mass of the ammonia dissolved in the water, thus obtaining the content of total nonvolatile matters in the ammonia. The method has the advantages of being simple to sample, easy and convenient to operate, low in cost, high in analysis speed, high in detection precision, low in detection limit and short in analysis period.
Owner:SUZHOU JINHONG GAS CO LTD

Anesthesia respirator evaporation device

The invention relates to an anesthesia respirator evaporation device. The problems are effectively solved that drawdown of liquid levels of current anesthesia evaporators influences evaporation speed,the evaporation speed and the amount of carried gas cannot be matched and adjusted, and the evaporation speed is low. According to the technical scheme, the anesthesia respirator evaporation device includes an evaporation chamber, multiple layers of evaporating dishes are arranged inside the evaporation chamber, a drug storage cavity is formed above the evaporation chamber, a vertical pipe whichpenetrates through the evaporating dishes in sequence is installed inside the evaporation chamber, the upper end of the vertical pipe is communicated with the bottom of the drug storage cavity, a plurality of plungers which are in one-to-one correspondence to the evaporating dishes and capable of moving up and down are installed inside the vertical pipe, and the plungers move up and down and thencan control whether or not medical liquid is stored inside the corresponding evaporating dishes. The liquid level of the anesthesia respirator evaporation device is constant; according to the amount of the carried gas, the working conditions of the evaporating dishes on each layer can be selectively started and closed, so that the evaporation efficiency of the medical liquid inside the evaporationchamber is matched with the amount of the carried gas; the space utilization rate of the evaporation chamber is high, and the anesthesia respirator evaporation device is compact in structure, small in size and high in evaporation speed.
Owner:刘书勇
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