Method for extracting unsaponifiable matters from shea butter oil
A technology of shea butter and liquid oil, applied in chemical instruments and methods, digestive systems, biofuels, etc., can solve the problem of low content or purity of biologically active substances, improve nutritional application value, enhance functionality, reduce The effect of cosmetic effects
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Embodiment 1
[0128] 1. Take 4Kg of refined shea olein with AV=0.5, triterpenoid alcohols and sterol content of 7.20%, add methanol and milk with a mass ratio (refined shea oil:methanol) of 3:1 Sodium methoxide with 0.7% mass of fruit liquid oil, reacted at 70°C for 2.5 h, separated the liquid, took the upper liquid, washed with water, stood still to separate the liquid, took the upper liquid, and distilled under reduced pressure to remove the residual solvent to obtain the transesterification product, The yield was 92.0%, and the content of triterpene alcohols and sterols was 7.13%.
[0129] 2. Take 1kg of the shea olein transesterification product obtained in the previous step, and carry out molecular distillation at a distillation temperature of 110°C, a rotation speed of 250rpm, and a pressure of 10 -3 mbar. A 130 g heavy phase sample was obtained by distillation, and the content of triterpene alcohols and sterols was 50.86%. (The specific content of unsaponifiable matter in molecular...
Embodiment 2
[0139] 1. Take 4Kg of refined shea olein with AV=0.5, triterpenoid alcohols and sterol content of 7.20%, add methanol and milk with a mass ratio (refined shea oil:methanol) of 3:1 Sodium methoxide with 0.7% mass of fruit liquid oil, reacted at 70°C for 2.5 h, separated the liquid, took the upper liquid, washed with water, stood still to separate the liquid, took the upper liquid, and distilled under reduced pressure to remove the residual solvent to obtain the transesterification product, The yield was 92.0%, and the content of triterpene alcohols and sterols was 7.13%.
[0140] 2. Take 1kg of the shea olein transesterification product obtained in the above steps, and carry out molecular distillation at a distillation temperature of 110°C, a rotation speed of 250rpm, and a pressure of 10 -3 mbar. A 130 g heavy phase sample was obtained by distillation, and the content of triterpene alcohols and sterols was 50.86%. (The specific content of unsaponifiable matter in molecular d...
Embodiment 3
[0147] 1. Take 4Kg of refined shea olein with AV=0.5, triterpenoid alcohols and sterol content of 7.20%, add methanol and milk with a mass ratio of 3:1 (refined shea oil:methanol) Sodium methoxide with 0.7% mass of fruit liquid oil, reacted at 70°C for 2.5 h, separated the liquid, took the upper liquid, washed with water, stood still to separate the liquid, took the upper liquid, and distilled under reduced pressure to remove the residual solvent to obtain the transesterification product, The yield was 92.0%, and the content of triterpene alcohols and sterols was 7.13%.
[0148] 2. Take 1kg of the shea olein transesterification product obtained in the previous steps, and carry out molecular distillation at a distillation temperature of 110°C, a rotational speed of 250rpm, and a pressure of 10 -3 mbar. A 130 g heavy phase sample was obtained by distillation, and the content of triterpene alcohols and sterols was 50.86%. (The specific content of unsaponifiable matter in the mo...
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