Looking for breakthrough ideas for innovation challenges? Try Patsnap Eureka!

Method for extracting unsaponifiable matters from shea butter oil

A technology of shea butter and liquid oil, applied in chemical instruments and methods, digestive systems, biofuels, etc., can solve the problem of low content or purity of biologically active substances, improve nutritional application value, enhance functionality, reduce The effect of cosmetic effects

Active Publication Date: 2013-12-18
WILMAR SHANGHAI BIOTECH RES & DEV CENT
View PDF8 Cites 18 Cited by
  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0020] Therefore, there is an urgent need for a method for extracting high-purity unsaponifiables from shea butter liquid oil to solve the problem of low content or purity of biologically active substances in products prepared in the current technology

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
View more

Image

Smart Image Click on the blue labels to locate them in the text.
Viewing Examples
Smart Image
  • Method for extracting unsaponifiable matters from shea butter oil
  • Method for extracting unsaponifiable matters from shea butter oil
  • Method for extracting unsaponifiable matters from shea butter oil

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0128] 1. Take 4Kg of refined shea olein with AV=0.5, triterpenoid alcohols and sterol content of 7.20%, add methanol and milk with a mass ratio (refined shea oil:methanol) of 3:1 Sodium methoxide with 0.7% mass of fruit liquid oil, reacted at 70°C for 2.5 h, separated the liquid, took the upper liquid, washed with water, stood still to separate the liquid, took the upper liquid, and distilled under reduced pressure to remove the residual solvent to obtain the transesterification product, The yield was 92.0%, and the content of triterpene alcohols and sterols was 7.13%.

[0129] 2. Take 1kg of the shea olein transesterification product obtained in the previous step, and carry out molecular distillation at a distillation temperature of 110°C, a rotation speed of 250rpm, and a pressure of 10 -3 mbar. A 130 g heavy phase sample was obtained by distillation, and the content of triterpene alcohols and sterols was 50.86%. (The specific content of unsaponifiable matter in molecular...

Embodiment 2

[0139] 1. Take 4Kg of refined shea olein with AV=0.5, triterpenoid alcohols and sterol content of 7.20%, add methanol and milk with a mass ratio (refined shea oil:methanol) of 3:1 Sodium methoxide with 0.7% mass of fruit liquid oil, reacted at 70°C for 2.5 h, separated the liquid, took the upper liquid, washed with water, stood still to separate the liquid, took the upper liquid, and distilled under reduced pressure to remove the residual solvent to obtain the transesterification product, The yield was 92.0%, and the content of triterpene alcohols and sterols was 7.13%.

[0140] 2. Take 1kg of the shea olein transesterification product obtained in the above steps, and carry out molecular distillation at a distillation temperature of 110°C, a rotation speed of 250rpm, and a pressure of 10 -3 mbar. A 130 g heavy phase sample was obtained by distillation, and the content of triterpene alcohols and sterols was 50.86%. (The specific content of unsaponifiable matter in molecular d...

Embodiment 3

[0147] 1. Take 4Kg of refined shea olein with AV=0.5, triterpenoid alcohols and sterol content of 7.20%, add methanol and milk with a mass ratio of 3:1 (refined shea oil:methanol) Sodium methoxide with 0.7% mass of fruit liquid oil, reacted at 70°C for 2.5 h, separated the liquid, took the upper liquid, washed with water, stood still to separate the liquid, took the upper liquid, and distilled under reduced pressure to remove the residual solvent to obtain the transesterification product, The yield was 92.0%, and the content of triterpene alcohols and sterols was 7.13%.

[0148] 2. Take 1kg of the shea olein transesterification product obtained in the previous steps, and carry out molecular distillation at a distillation temperature of 110°C, a rotational speed of 250rpm, and a pressure of 10 -3 mbar. A 130 g heavy phase sample was obtained by distillation, and the content of triterpene alcohols and sterols was 50.86%. (The specific content of unsaponifiable matter in the mo...

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

PUM

No PUM Login to View More

Abstract

The invention provides a method for extracting unsaponifiable matters from shea butter oil. The method comprises the steps of ester exchange, molecular distillation, crystallization and the like. An unsaponifiable matter composition with high purity can be obtained by adopting the method. The content of the unsaponifiable matters in the composition can reach 60%, 70% or even higher; the composition contains high contents of triterpene alcohols and sterol which can exist in the form of solids; the shelf life of the unsaponifiable matters is prolonged; the unsaponifiable matters can be applied to various purposes.

Description

technical field [0001] The invention relates to a method for extracting unsaponifiable matter from Shea olein. Background technique [0002] Shea olein is a liquid or semi-solid fat product obtained from shea butter through fractionation and other processes. Shea butter is a natural light yellow semi-solid oil extracted from African shea nuts. [0003] Shea butter can effectively prevent solar dermatitis, and has anti-aging and high moisturizing effects. Shea butter is the closest to the indicators of human sebum secretion and oil. It contains rich non-saponifiable ingredients and is easy to absorb by the human body. It can not only prevent dryness and cracking, but also further restore and maintain the natural elasticity of the skin. Moisturizing effect. [0004] According to historical records, the indigenous people of Africa often used shea butter in ointments to treat rheumatic pains and boils. Aboriginal people massage newborn babies with shea butter to protect thei...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

Application Information

Patent Timeline
no application Login to View More
IPC IPC(8): A61K8/97A61K36/185C11C3/04C11C1/10C11D3/382C11D9/04C10L1/02A61P1/02A61P9/10A61P17/00A61P29/00A61P19/00
CPCY02E50/10
Inventor 黄贤校邹彦平杨天奎高圆圆
Owner WILMAR SHANGHAI BIOTECH RES & DEV CENT
Who we serve
  • R&D Engineer
  • R&D Manager
  • IP Professional
Why Patsnap Eureka
  • Industry Leading Data Capabilities
  • Powerful AI technology
  • Patent DNA Extraction
Social media
Patsnap Eureka Blog
Learn More
PatSnap group products