Method for extracting unsaponifiable matters from shea butter oil

A technology of shea butter and liquid oil, applied in chemical instruments and methods, digestive systems, biofuels, etc., can solve the problem of low content or purity of biologically active substances, improve nutritional application value, enhance functionality, reduce The effect of cosmetic effects

Active Publication Date: 2013-12-18
WILMAR SHANGHAI BIOTECH RES & DEV CENT
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0020] Therefore, there is an urgent need for a method for extracting high-purity unsaponifiables from shea butter liquid oil

Method used

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  • Method for extracting unsaponifiable matters from shea butter oil
  • Method for extracting unsaponifiable matters from shea butter oil
  • Method for extracting unsaponifiable matters from shea butter oil

Examples

Experimental program
Comparison scheme
Effect test

Example Embodiment

[0127] Example 1:

[0128] 1. Take 4Kg of refined shea olein with AV=0.5, 7.20% triterpene alcohol and sterol content, and add methanol and milk with a mass ratio (refined shea olein) of 3:1 Sodium methoxide containing 0.7% of the mass of the liquid oil of the tree fruit was reacted at 70°C for 2.5 h. The liquid was separated, the upper layer was taken, washed with water, and left to stand for liquid separation. The upper liquid was taken, and the residual solvent was removed by vacuum distillation to obtain the transesterified product. The yield was 92.0%, and the content of triterpene alcohols and sterols was 7.13%.

[0129] 2. Take 1kg of the transesterified product of shea olein obtained in the previous step and carry out molecular distillation. The distillation temperature is 110℃, the rotation speed is 250rpm, and the pressure is 10 -3 mbar. A 130g heavy phase sample was obtained by distillation, and the content of triterpene alcohols and sterols was 50.86%. (The specific c...

Example Embodiment

[0138] Example 2:

[0139] 1. Take 4Kg of refined shea olein with AV=0.5, 7.20% triterpene alcohol and sterol content, and add methanol and milk with a mass ratio (refined shea olein) of 3:1 Sodium methoxide containing 0.7% of the mass of the liquid oil of the tree fruit was reacted at 70°C for 2.5 h. The liquid was separated, the upper layer was taken, washed with water, and left to stand for liquid separation. The upper liquid was taken, and the residual solvent was removed by vacuum distillation to obtain the transesterified product. The yield was 92.0%, and the content of triterpene alcohols and sterols was 7.13%.

[0140] 2. Take 1kg of the transesterified product of shea olein obtained in the above steps and carry out molecular distillation. The distillation temperature is 110℃, the rotation speed is 250rpm, and the pressure is 10 -3 mbar. A 130g heavy phase sample was obtained by distillation, and the content of triterpene alcohols and sterols was 50.86%. (The specific con...

Example Embodiment

[0146] Example 3:

[0147] 1. Take 4Kg of refined shea olein with AV=0.5, 7.20% triterpene alcohols and sterol content, and add methanol and milk with a mass ratio of 3:1 (refined shea olein) Sodium methoxide containing 0.7% of the mass of the liquid oil of the tree fruit was reacted at 70°C for 2.5 h. The liquid was separated, the upper layer was taken, washed with water, and left to stand for liquid separation. The upper liquid was taken, and the residual solvent was removed by vacuum distillation to obtain the transesterified product. The yield was 92.0%, and the content of triterpene alcohols and sterols was 7.13%.

[0148] 2. Take 1kg of the transesterified product of shea olein obtained in the previous steps and carry out molecular distillation. The distillation temperature is 110℃, the rotation speed is 250rpm, and the pressure is 10 -3 mbar. A 130g heavy phase sample was obtained by distillation, and the content of triterpene alcohols and sterols was 50.86%. (The specific...

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Abstract

The invention provides a method for extracting unsaponifiable matters from shea butter oil. The method comprises the steps of ester exchange, molecular distillation, crystallization and the like. An unsaponifiable matter composition with high purity can be obtained by adopting the method. The content of the unsaponifiable matters in the composition can reach 60%, 70% or even higher; the composition contains high contents of triterpene alcohols and sterol which can exist in the form of solids; the shelf life of the unsaponifiable matters is prolonged; the unsaponifiable matters can be applied to various purposes.

Description

technical field [0001] The invention relates to a method for extracting unsaponifiable matter from Shea olein. Background technique [0002] Shea olein is a liquid or semi-solid fat product obtained from shea butter through fractionation and other processes. Shea butter is a natural light yellow semi-solid oil extracted from African shea nuts. [0003] Shea butter can effectively prevent solar dermatitis, and has anti-aging and high moisturizing effects. Shea butter is the closest to the indicators of human sebum secretion and oil. It contains rich non-saponifiable ingredients and is easy to absorb by the human body. It can not only prevent dryness and cracking, but also further restore and maintain the natural elasticity of the skin. Moisturizing effect. [0004] According to historical records, the indigenous people of Africa often used shea butter in ointments to treat rheumatic pains and boils. Aboriginal people massage newborn babies with shea butter to protect thei...

Claims

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Application Information

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IPC IPC(8): A61K8/97A61K36/185C11C3/04C11C1/10C11D3/382C11D9/04C10L1/02A61P1/02A61P9/10A61P17/00A61P29/00A61P19/00
CPCY02E50/10
Inventor 黄贤校邹彦平杨天奎高圆圆
Owner WILMAR SHANGHAI BIOTECH RES & DEV CENT
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