30 results about "Tall oil" patented technology

The present invention is directed to tall oil rosin in solid, crystalline form. The tall oil rosin according to the present invention has a very low color, i.e. it is essentially color-less. The present invention is also directed to a process for producing the tall oil rosin and to the use of the tall oil rosin according to the present invention.

The present invention relates to a herbicide formulation based on pine oil. The present invention also relates to a method of reducing unwanted vegetation in a soil environment and a method for reducing seed viability using the herbicide formulation. The herbicide formulation comprises a pine oil, a tall oil, and an alkali. The formulation has improved herbicidal properties, and is less subject to coagulation at low ambient temperatures.

The present invention pertains to the agricultural field, and particularly to the use of tall oil fatty acids as a phytosanitary adjuvant, particularly for preventing spray drift. The present inventors have indeed shown that the introduction of tall oil fatty acids into phytosanitary compositions allows increasing droplet size distribution upon spraying and therefore reducing off-target spraying. The present invention therefore provides methods for generating droplets, treating plants and for preventing spray drift. The invention also relates to phytosanitary compositions comprising tall oil fatty acids.

This invention relates to the field of tall oil production supervision and management technology, and discloses a tall oil production batch quality traceability management system based on big data. The system includes: a data acquisition module for acquiring time-series flow rate, material level, and temperature data from storage tanks; a batch weight calculation module for converting incoming batches into a mixed weight matrix based on flow rate and material level data, and determining the logical address segment of the flow stagnation zone based on material temperature to implement vector masking, dividing the matrix into suspended and iterative subsets; and a traceability map generation module for calculating the proportion weights and constructing an association model to generate a quality traceability map. This invention translates the physical mixing process into the flow law of data weights through a logical address management mechanism, solving the defect of ambiguous batch boundaries in continuous mixing conditions, and realizing penetrating quality auditing and risk warning from the original raw material source to the finished product.

The present invention is directed to fractionation of crude tall oil, which originates from the Kraft process black liquor. In the method according to the present invention, at least two strongly basic anion exchange resins are used to efficiently separate fractions from the crude tall oil.

In tall oil production process, water is separated from a CO2 pre-acidified tall oil soap before the soap cooking phase. Method for improving a water separation from a CO2 pre-acidified tall oil soap comprises adding a synthetic polymer additive obtained by copolymerization of (meth)acrylamide and at least cationic monomers, to the CO2 pre-acidified tall oil soap prior to a water separation phase and / or in a water separation phase. The synthetic polymer additive is a net cationic at pH 7 and has a weight average molecular weight of 1 500 000 – 10 000 000 g / mol.

A method for improving a separation of tall oil soap from black liquor in a tall oil soap separation phase, which comprises adding of a polymer additive comprising cationic epichlorohydrin-dimethylamine based polymer into black liquor. The cationic epichlorohydrin-dimethylamine based polymer has a weight average molecular weight in the range of 1 500 – 500 000 g / mol. The cationic epichlorohydrin- dimethylamine based polymer may be further crosslinked with ethylenediamine (EDA). The polymer additive can be added to black liquor from pulping process prior to tall oil soap separation, and / or to a tall oil soap solution, which is achieved from separating tall oil soap from black liquor.

The present invention is directed to a method for recycling solvent and drying sodium salts of fatty acids and rosin acids obtained from crude tall oil. In the method according to the present invention, a mixture comprising sodium salts of fatty acids and rosin acids and an alcohol selected from methanol, ethanol and / or iso-propanol is subjected to a drying step wherein the alcohol is evaporated from the mixture and the salts are dried and recovered. The salts are useful for example for removal of extractives in pulp production or can be acidulated to produce high acid number tall oil.

The present disclosure relates to a process for producing rosinol from renewable materials comprising abietic acid, such as raw materials comprising crude tall oil. According to the method, abietic acid present in the renewable material is separated (101) and a stream comprising at least partially separated abietic acid is subjected to a thermal decarboxylation reaction (102) to produce a stream comprising formed rosin oil and rosin oil is recovered (103) from the stream. The present disclosure also relates to a system for carrying out the method, and the use of rosinol obtainable by the method as a renewable feedstock co-processed with fossil feedstock to increase the renewable content of fossil transport fuels and / or chemicals, and the use of co-processing with other renewable feedstocks to produce renewable fuels and / or chemicals or components thereof. The present disclosure also relates to a rosin oil product obtainable by the process.

The invention relates to the technical field of road paving materials, and discloses aminated PET (polyethylene terephthalate) and desulfurized rubber powder composite modified asphalt and a preparation method thereof, the aminated PET and desulfurized rubber powder composite modified asphalt is prepared from matrix asphalt, desulfurized rubber powder, tall oil fatty acid, epoxidized soybean oil, zinc isoocatanoate, aminated PET and styrene-maleic anhydride copolymer, coating the desulfurized rubber powder with tall oil fatty acid, and carrying out esterification ring-opening reaction on the tall oil fatty acid and the epoxidized soybean oil to generate an anti-migration structure; the terminal amino of the aminated PET and the epoxidized soybean oil are subjected to addition to form a bridging prepolymerization micro-area; and the styrene-maleic anhydride copolymer is subjected to dehydration ring-closure reaction, so that the pre-polymerized micro-area is grafted into the matrix asphalt in situ. According to the invention, a homogeneous three-dimensional interpenetrating network is constructed in an asphalt system through a chemical reaction, so that the interfacial compatibility of a modifier and matrix asphalt is improved, the unidirectional migration of light components and the segregation of polymers are inhibited, and the long-term storage stability and rutting deformation resistance of the composite modified asphalt are improved.

Provided is an asphalt composition for repairing asphalt pavement, the asphalt composition comprising an asphalt and a lubricative solidification material, wherein the lubricative solidification material contains a tall oil fatty acid and / or a tall oil fatty acid ester, and a C6-C30 branched saturated fatty acid.

The invention relates to the technical field of pipeline repair, and discloses a pipeline trenchless repair material and a preparation method thereof, the repair material is a bi-component solvent-free thixotropic fluid, and is composed of a component A and a component B, wherein the component A takes bisphenol A type and bisphenol F type liquid epoxy resin as a matrix, and is matched with hydrophilic fumed silica and quartz powder to construct a thixotropic network; the component B comprises a reaction product of tall oil fatty acid and triethylene tetramine, benzyl alcohol, an alicyclic amine curing agent, an aromatic amine curing agent and a tertiary amine accelerator. Through compounding of an amine curing system and thixotropic adjustment, the problems that an existing material is prone to sagging during construction on a vertical plane and the bonding strength of a wet base plane is low are effectively solved. The material has excellent thixotropy, wet surface bonding strength and chemical corrosion resistance, is compact in curing, low in shrinkage rate and free of solvent residues, and is particularly suitable for non-excavation in-situ repair construction of underground drainage pipelines.

This invention discloses a thick-film solvent-free epoxy fire-retardant coating and its application. The thick-film solvent-free epoxy fire-retardant coating comprises component A and component B. Component A includes the following components: polyester-modified epoxy resin, tall oil fatty acid, glass fiber filaments, thixotropic thickener, rheology modifier, and flame retardant. Component B includes the following components: curing agent, curing accelerator, modifier, glass fiber filaments, thixotropic thickener, rheology modifier, and melamine. The coating formed by applying the above coating to a substrate exhibits excellent adhesion, good wind resistance, water resistance, weather resistance, and durability, and there is no fire risk at the joints.

The application provides a beneficiation method of low-grade spodumene, which comprises the following steps: wet grinding of the to-be-beneficiated raw ore to obtain a first ore slurry, then adding water to the first ore slurry and stirring to obtain a to-be-beneficiated ore slurry with a preset concentration; adding a first preset reagent to the obtained to-be-beneficiated ore slurry to perform slime reverse flotation to obtain slime and desliming tailings; adding a second preset reagent to the desliming tailings to perform desliming tailings direct flotation to obtain lithium concentrate and tailings; the second preset reagent comprises an adjusting agent, a composite depressant and a composite collector; the composite depressant is obtained by compounding tannic acid, hydroxyl citric acid, lactic acid and sodium lignosulfonate; and the composite collector is obtained by compounding oleic acid, tall oil, naphthenic acid and white oil. The beneficiation method of low-grade spodumene is characterized in that the beneficiation process of desliming by reverse flotation and direct flotation of spodumene is used to separate a large amount of gangue minerals; then, under the joint action of the composite depressant and the composite collector, the low-grade spodumene is effectively recovered, and the resource utilization rate is improved.

The invention belongs to the technical field of oil exploitation, and particularly relates to a plugging agent for oil-based drilling fluid and a preparation method thereof.The preparation method of the plugging agent for the oil-based drilling fluid comprises the steps that chitin and organic acid are subjected to an amidation reaction in water, water is removed after the reaction is completed, and a liquid intermediate is obtained; performing esterification reaction on the liquid intermediate and fatty acid in the presence of an organic solvent and a catalyst to obtain the plugging agent for the oil-based drilling fluid, the organic acid contains two carboxyl groups, and the carbon atom number of the organic acid is an integer between 2 and 6; the fatty acid is any one of oleic acid, linoleic acid and tall oil; the D90 particle size of the plugging agent for the oil-based drilling fluid is 620-910 nm. The particle size of the plugging agent is in a micro-nano scale, the plugging agent can plug micro-nano-scale microcracks and achieve the effect of stabilizing a well wall, and the plugging agent has good compatibility with an oil-based drilling fluid and can improve the emulsion stability of the oil-based drilling fluid.

Corrosion inhibitor compositions including an alkoxylated polyamine and an imidazoline. The alkoxylated polyamine may be derived from aminoethylethanolamine (AEEA), ethylenediamine (EDA), diethylenetriamine (DETA), triethylenetetramine (TETA), or tetraethylenepentamine (TEPA). The imidazoline is typically derived from tall oil fatty acid (TOFA). The composition provides effective corrosion inhibition when present at 5 to 100 ppm in a corrosive medium. Methods of inhibiting corrosion of a metal substrate in contact with a carbon dioxide-containing corrosive medium using the composition are also disclosed, as well as systems for inhibiting corrosion in oil and gas production processes incorporating the composition.

The application provides a cutting fluid and application and a cutting fluid circulation system. The cutting fluid comprises: an extreme pressure agent, a lubricant, a coolant, a defoaming agent, a corrosion inhibitor and a surfactant; the mass ratio of the extreme pressure agent, the lubricant, the coolant, the defoaming agent, the corrosion inhibitor and the surfactant is 2-15:1-30:1-30:0.01-2:0.1-2:0.1-40; the extreme pressure agent comprises at least one of a sulfurized alkene and a sulfurized fatty acid ester, and is free of chlorine and phosphorus; the lubricant comprises at least one of castor oil triethanolamine and tall oil; the coolant comprises diethyl ethanol; the defoaming agent comprises at least one of a silicone oil emulsifier and a higher alcohol; the corrosion inhibitor comprises triethylene glycol maleate; and the surfactant comprises octylphenyl alcohol. In this way, when a neodymium iron boron magnet is cut by using a diamond wire cutting process, the dissolution of neodymium oxide in the neodymium iron boron magnet cutting waste by the cutting fluid can be avoided, and the recycling rate of the neodymium iron boron magnet cutting waste can be improved.

The invention provides a composite fluorite collecting agent and application thereof, and belongs to the technical field of ore flotation. The composite fluorite collecting agent consists of the following raw materials in percentage by mass: 30-60% of oleic acid, 5-15% of lower alcohol, 0.05-0.2% of an esterification catalyst, 2-10% of an alkali compound, 2-8% of an emulsifier, 0.5-2% of a water repellent agent, 2-5% of a synergist, 1-5% of a cosolvent, 0.01-0.2% of a defoaming agent and the balance of water. Wherein the oleic acid comprises two or more of low-iodine-value oleic acid, high-iodine-value oleic acid, ricinoleic acid and tall oil fatty acid. By improving the formula and process of the collecting agent, the concentrate purity is greatly improved, the average grade of concentrate powder is 93% or above, the average concentrate recovery rate is 80% or above, and the average concentrate and middling recovery rate reaches 90%.

The application relates to the technical field of pipeline repair, and discloses a pipeline trenchless repair material and a preparation method thereof. The repair material is a two-component solvent-free thixotropic fluid, which is composed of component A and component B. The component A takes bisphenol A type and bisphenol F type liquid epoxy resin as a matrix, and is matched with hydrophilic fumed silica and quartz powder to build a thixotropic network. The component B contains a reaction product of tall oil fatty acid and triethylenetetramine, benzyl alcohol, an alicyclic amine curing agent, an aromatic amine curing agent and a tertiary amine accelerator. The amine curing system and the thixotropic adjustment are compounded, so that the problems of easy flow hanging in vertical surface construction and low bonding strength on a wet base surface of the existing material are effectively solved. The material has excellent thixotropy, wet surface bonding strength and chemical corrosion resistance, is dense after curing, has low shrinkage, and has no solvent residue, and is particularly suitable for trenchless in-situ repair construction of underground drainage pipelines.

Described is a saponified tall oil that can be used as an insecticide. Also described is an insecticide that contains a saponified tall oil. Also described is to a method for producing a composition or an insecticide containing the saponified tall oil. The method includes: providing a heated basic solution of water and lye; and performing saponification by adding tall oil to the heated basic solution during mixing, to form a saponified solution.

The invention discloses a cooling liquid for energy storage equipment. The cooling liquid comprises the following components in percentage by weight: 25%-55% of propylene glycol, 0.4%-4% of organic alkali, 0.1%-1% of a corrosion inhibitor, 0.002%-0.004% of a defoaming agent, 0.0001%-0.001% of pigment and the balance of pure water. Through the synergistic effect of the tall oil-based amine ethyl imidazoline corrosion inhibitor and the bis Mannich base corrosion inhibitor, the corrosion inhibition performance of the energy storage cooling liquid on metal materials, especially aluminum alloy, is effectively improved, meanwhile, the energy storage cooling liquid has good compatibility on non-metal materials, and the service life of energy storage equipment can be prolonged.

The purpose of this invention is to provide a foam inhibitor with tall oil soap separation function. It improves the defoaming performance by combining wax substances with mineral oil and fumed silica. The synergistic effect of silicone polyether and fatty alcohol polyether and chiral monoterpene alcohol in the synergist improves the recovery rate of tall oil soap, and finally prepares a product with good effect in removing tall oil soap and defoaming performance.

This disclosure relates to sticker adjuvants for agricultural concentrate compositions and agricultural spray compositions. The sticker adjuvant comprises a sticker component including a mixture of a polyterpene oligomer and distilled tall oil (DTO), in combination with one or more surfactants and additional optional additives. The polyterpene oligomer comprises polymerized units of α-pinene and β-pinene, and the DTO comprises fatty acids and rosin acids in amounts effective to reduce viscosity and enhance film formation. When incorporated into agricultural spray mixtures, the sticker adjuvant improves adhesion and rainfastness of active ingredients on plant surfaces.

The invention discloses a hot melt adhesive for a mattress spring package and a preparation method thereof, and belongs to the field of adhesives, and the preparation method comprises the following steps: adding an ethylene-octylene random copolymer and an ethylene-octylene block copolymer into a reaction kettle, heating and stirring, replacing air in the reaction kettle with protective gas, and stirring to obtain a hot melt adhesive solution; adding a titanate coupling agent and tall oil rosin glyceride, stirring until various melts are mixed, adding an antioxidant, mixing, discharging, and cooling to obtain the hot melt adhesive for the mattress spring package. The low-temperature flexibility of the hot melt adhesive is improved through the POE and the OBC, the wet viscosity and the initial bonding strength of the hot melt adhesive are improved by adding the tall oil rosin glyceride, and the titanate coupling agent can be combined with the tall oil rosin glyceride, the non-woven fabric and the spring metal, so that the flexibility and the bonding strength of the hot melt adhesive are improved; therefore, the hot melt adhesive is not easy to become brittle after being subjected to seasonal change, and the mattress can be effectively prevented from cracking due to external force in the using process.

The present invention is directed to the fractionation of crude tall oil originating from Kraft black liquor. In the process according to the invention, at least two strong base anion exchange resins are used to efficiently separate fractions from crude tall oil.

The application relates to the technical field of diesel oil additives, and particularly discloses a high-efficiency diesel oil anti-wear lubricant and a preparation method thereof.A high-efficiency diesel oil anti-wear lubricant is prepared from the following raw materials in parts by weight: 45-65 parts of double-modified fatty acid polyol ester, 6-12 parts of modified molybdenum dialkyldithiophosphate, 7-14 parts of tall oil fatty acid, 2-7 parts of nano boron nitride, 1-3 parts of antioxidant, 2-5 parts of composite organic amine stabilizer and 20-40 parts of solvent; the double-modified fatty acid polyol ester is prepared by modifying fatty acid polyol ester through two steps of epoxidation and phosphoric acid monoester esterification; and the modified molybdenum dialkyldithiophosphate is prepared by modifying molybdenum dialkyldithiophosphate with benzotriazole and a silane coupling agent.The anti-wear lubricant has excellent basic lubrication anti-wear capacity and excellent high-pressure stability.

Described is a composition and a method for producing a composition. The composition includes a saponified solution of water and lye of sodium hydroxide or potassium hydroxide, and tall oil, wherein the composition includes particles having a size of between 5 nm and 100 nm, as determined by a dynamic laser light diffraction scattering method using Malvern Zetasizer Nano-ZS. The method includes the steps: providing a preheated basic solution of water and lye of either sodium hydroxide or potassium hydroxide; and saponification by adding tall oil to the heated basic solution during mixing, to form a saponified solution.