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40 results about "Mixed fatty acid" patented technology

Method for recovering cis-15-tetracosenoic acid from acer truncatum seed oil byproduct

The invention relates to the technical field of separation and purification, in particular to a method for recovering cis-15-tetracosenoic acid from an acer truncatum seed oil byproduct, which comprises the following steps: selecting the acer truncatum seed oil byproduct, crushing, sieving, washing, adding modified attapulgite and beta-cyclodextrin, stirring and adsorbing at constant temperature, and filtering; preparing the modified attapulgite; adding a KOH-EtOH solution containing lipase and polyethylene glycol into a pretreated product for refluxing, and adding a saturated saline solution for refluxing; standing and layering the reaction liquid, and extracting, acidifying, washing, drying and distilling an organic phase to obtain mixed fatty acid; and carrying out composite purification to obtain a pure cis-15-tetracosenoic acid product. According to the method, the purity and the extraction rate of the cis-15-tetracosenoic acid are remarkably improved, the oxidation, heat and storage stability of the product is enhanced, the color is improved, and the comprehensive application performance is better.
Owner:YILIJIA (BEIJING) HEALTH TECHNOLOGY CO LTD

Method for separating stearic acid lactone from mixed fatty acid

The invention discloses a method for separating stearic acid lactone from mixed fatty acid, which comprises the following steps: dispersing an oleic acid isomerization hydrogenation product in an organic solvent which is one of normal hexane, methanol, ethanol, ethyl acetate and acetonitrile, then carrying out freezing crystallization, then carrying out solid-liquid separation, taking the liquid, and carrying out reduced pressure distillation to obtain the stearic acid lactone. The stearic acid lactone is obtained. The method for separating the stearic acid lactone from the mixed fatty acid has the advantages of simplicity in operation, high separation efficiency, low energy consumption, mild conditions, high purity of the separated stearic acid lactone and the like, and is suitable for large-scale industrial application.
Owner:SOUTH CHINA UNIV OF TECH

Anti-inflammatory analgesic indomethacin long-acting suppository and preparation method thereof

The invention relates to the technical field of pharmaceutical preparations, and particularly discloses an anti-inflammatory analgesic indometacin long-acting suppository and a preparation method thereof.The suppository is composed of indometacin sustained-release microspheres and a modified fatty matrix; eudragit RS100 / RL100 is used as a compound framework of the sustained-release microspheres, the sustained-release microspheres are prepared through a spherocrystal granulation process, the modified fatty matrix is prepared from a mixed fatty glyceride compound matrix sustained-release aid, a three-dimensional suspending dispersant and the like through melting, pre-crystallization and high-speed homogenization processes, and the three-dimensional suspending dispersant contains modified nano silicon dioxide, glycerin monostearate and beewax. According to the invention, a microsphere-matrix dual controlled release system is constructed, so that burst release of drugs is eliminated, and long-acting stable release is realized; the microspheres are prevented from settling and agglomerating through a physical locking mechanism, and the storage stability of the preparation is improved by matching with a dual anti-oxidation system; meanwhile, rectal mucosa stimulation is reduced, the preparation process is simple, the quality is controllable, and the composition is suitable for anti-inflammation and analgesia of various diseases and has a wide clinical application prospect.
Owner:JIANGSU YUANHENG PHARMA

Multiple filtering device

The utility model discloses a multi-filtering device which comprises a filtering device body, and the filtering device body comprises a filtering cylinder and a filtering plate body connected in the filtering cylinder; the filter plate body comprises multiple layers of filter plates and sealing rings connected to the peripheries of the multiple layers of filter plates, and the sealing rings are connected into the filter cartridge and fixedly connected with the inner wall of the filter cartridge in a sealing manner; the bottom of the sealing ring is connected with a partition ring, the bottom of the partition ring extends in the vertical downward direction, and a gap is formed between the bottom of the partition ring and the inner wall of the filter cartridge. By arranging the sealing ring and the partition ring, the mixed fatty glyceride cannot be in contact with the cylinder wall below the filter plate body before and after filtration, so that the mixed fatty glyceride cannot be adhered to the cylinder wall, the structure is simpler, and the overall cost is effectively reduced.
Owner:GUANGZHOU CARDLO BIOCHEM TECH

Method for preparing coal slime collector by using kitchen waste oil

PendingCN122352452ABiotechnologyAlkane
The present application relates to a kind of coal slime collector preparation method using kitchen waste oil, comprising the kitchen waste oil after being pretreated with water, emulsifier is mixed, as carbon source configuration first culture medium, Bacillus and Rhodococcus species are inoculated in it and carry out aerobic fermentation, obtain refined oil, and as carbon source configuration second culture medium, Candida species are inoculated in it and carry out aerobic fermentation, obtain mixed fatty acid, and as carbon source configuration third culture medium, Yarrowia species are inoculated in it and carry out micro-aerobic fermentation, obtain alkane mixture;Emulsified oil and / or refined oil are as carbon source configuration fourth culture medium, Pseudomonas species are inoculated in it and carry out aerobic fermentation, obtain rhamnolipid;Alkane mixture is mixed with rhamnolipid, obtain coal slime collector.The present application develops a new type of green, good coal slime collector by constructing multistage series biological transformation process.
Owner:SUZHOU FENGBEI BIOTECH CO LTD

Method for detecting the composition ratio of glycerides and fatty acids in mixed fatty acid glycerides by thin layer chromatography-gas chromatography

The invention discloses a method for detecting glyceride and fatty acid composition ratio in mixed fatty acid glyceride by thin-layer chromatography-gas chromatography coupling, and the method mainly comprises the following steps: 1) internal standard solution is prepared; 2) mixed fatty acid glyceride need testing solution is prepared; 3) thin-layer chromatography is used to separate mixed fatty acid glyceride; 4) fatty acid methyl ester is prepared; 5) gas chromatography is used to detect, and the fatty acid composition of monoglyceride, diglyceride and triglyceride and the ratio of each fatty acid are determined respectively; and 6) the sum of the fatty acids of each monoglyceride, diglyceride and triglyceride obtained after data analysis in step 5) is divided by the fatty acid sum of monoglyceride, diglyceride and triglyceride, and the composition ratio of each monoglyceride, diglyceride and triglyceride in mixed fatty acid glyceride is obtained. The method of the present invention is simple and efficient to operate, and is quantitatively accurate, and methyl esterification reaction conditions are mild, equipment is simple, and no special equipment is required.
Owner:GUANGZHOU GONGHE MEDICINE TECH

Modified wood and modification method thereof

The invention relates to the field of wood modification, in particular to modified wood and a modification method thereof. The method comprises the following steps: (1) drying wood to be modified to constant weight to obtain dried wood; (2) the dried wood is placed in steeping liquor to be treated, and steeped wood is obtained; the steeping liquor comprises any one of steeping liquor I and steeping liquor II; the impregnation liquid I comprises silicate and organic acid I; the impregnation liquid II comprises organic acid II, mixed fatty acid methyl ester and wax. On the premise of ensuring simple operation steps, the porosity of the wood can be reduced, and the dimensional stability, high humidity resistance and salt resistance of the wood can be improved.
Owner:BEIBU GULF UNIV +2

Wide-temperature-range modified natural ester insulating oil and molecular structure design method thereof

The invention relates to wide-temperature-range modified natural ester insulating oil and a molecular structure design method thereof, and the molecular structure of the wide-temperature-range modified natural ester insulating oil with different ester chain structures is obtained by converting natural ester into mixed fatty acid methyl ester with the chain length of C8-C18, then blending the proportion and introducing groups for molecular modification. According to the design method, natural ester insulating oil molecules with different ester chain structures are constructed, and the influence rule of the fatty acid methyl ester carbon chain length proportion, the C = C double bond number and the modification group on the flash point and pour point of the natural ester insulating oil is obtained; the obtained wide-temperature-range modified natural ester insulating oil not only keeps the high flash point of the natural ester insulating oil, but also has the characteristic of low pour point, so that the working temperature range of the natural ester insulating oil is widened, and the defect that a natural ester insulating oil transformer operates under high-altitude, cold regions and extreme weather conditions is overcome; the preparation process is simple, reaction conditions are mild, the environment is not polluted, and batch production is easy.
Owner:STATE GRID CHONGQING ELECTRIC POWER CO ELECTRIC POWER RES INST +2

Process for preparing a flotation reagent, flotation reagent and method for the flotation of rare earth ores

PendingCN122625328AMixed fatty acidFenton reagent
The embodiment of the application discloses a flotation reagent preparation method, a flotation reagent and a flotation method of a rare earth ore. The flotation reagent preparation method is characterized in that the method comprises the following steps: mixing a plurality of flotation reagents to obtain a mixed fatty acid collector; adding a sodium hydroxide solution to the mixed fatty acid collector to obtain a collector solution; and electrolyzing the collector solution and oxidizing the collector solution to make the collector solution generate nanobubbles and hydroxyl radicals, thereby obtaining a flotation reagent. The flotation reagent preparation method can simultaneously realize dispersion activation and in-situ oxidation modification of the fatty acid collector, can generate hydroxyl radicals without additional addition of a Fenton reagent, and can avoid problems such as impurity pollution of ore slurry and unstable oxidation effect caused by an exogenous reagent.
Owner:BEIJING RESEARCH INSTITUTE OF CHEMICAL ENGINEERING AND METALLURGY

Method for extracting and separating nervonic acid from vegetable oil

The invention discloses a method for extracting and separating nervonic acid from vegetable oil, and belongs to the technical field of nervonic acid extraction and separation. The extraction and separation method of nervonic acid comprises the following steps: (1) mixing vegetable oil with an alkaline ethanol solution, and carrying out saponification reaction to obtain fatty acid salt; (2) adding an acid solution into the fatty acid salt, stirring to fully acidify the fatty acid salt, standing for layering, separating an oil phase, and washing to be neutral to obtain mixed fatty acid; (3) performing macroporous resin column chromatography separation and purification on the mixed fatty acid, and collecting eluent to obtain a chromatography sample; and (4) mixing the chromatography sample with a solvent, recrystallizing, and drying to obtain nervonic acid with the content of 95% or above. The method provided by the invention has the advantages of simple process steps, no need of special production equipment, good extraction stability and repeatability, high nervonic acid extraction purity and high yield.
Owner:YUNNAN HEMPMON PHARMA CO LTD

Ester for refrigerator oil, base oil for refrigerator oil, refrigerator oil, and working fluid composition

PendingCN120641542AHeat-exchange elementsBase-materialsMixed fatty acidPentaerythritol
An ester for refrigerator oil, which contains a first ester that is an ester of a polyhydric alcohol and a C6-9 fatty acid, a second ester that is an ester of pentaerythritol and a fatty acid, and a third ester that is an ester of pentaerythritol, a dicarboxylic acid and a fatty acid, the fatty acid constituting the second ester and the fatty acid constituting the third ester are both mixed fatty acids of at least one selected from the group consisting of branched butyric acid, branched pentanoic acid, and linear pentanoic acid, and any one selected from branched caprylic acid and branched nonanoic acid.
Owner:JXTJ NIPPON OIL & ENERGY CORP +1

Method for preparing special grease for infant formula milk powder by enzyme method

The invention relates to the technical field of enzymatic preparation of grease, in particular to a method for enzymatic preparation of special grease for infant formula milk powder, which comprises the following steps: constructing a pH response type interface biocatalysis system, and synthesizing and enriching functional ester; the preparation method comprises the following steps: preparing an sn-2 palmitic acid diglyceride intermediate based on alcoholysis reaction, and reacting the sn-2 palmitic acid diglyceride intermediate with mixed fatty acid to synthesize the composite structure lipid; and preparing the target mixed grease from the functional ester, the composite structure grease and the fat-soluble vitamin by adopting a low-temperature high-speed shearing and homogenizing technology. According to the method for preparing the grease special for the infant formula milk powder through the enzyme method, pH response type magnetic nano immobilized lipase is prepared, the enzyme activity is controllable, and the grease is recycled and reused through the dual mechanisms of magnetic separation and pH induced aggregation; a fat-soluble vitamin-structural fat-essential fatty acid composite synergistic system is constructed, the functions of energy supply, mineral absorption and micronutrient supplementation are achieved, and a target grease product is purified by adopting a multi-stage molecular distillation step.
Owner:姚专

Pentaerythritol ester and preparation method thereof

The invention provides pentaerythritol ester and a preparation method thereof. The preparation method comprises the following steps: mixing mixed fatty acid and pentaerythritol according to the molar ratio of carboxyl to hydroxyl of (1-1.5): 1, irradiating by using ultraviolet light under 0.01-0.09 MPa, and carrying out esterification reaction under the condition of ultrasonic treatment to obtain pentaerythritol ester; wherein the mixed fatty acid comprises monobasic fatty acid and dibasic fatty acid, the monobasic fatty acid is at least two of C5-C10 monobasic fatty acid, and the dibasic fatty acid is at least one of C5-C9 dibasic fatty acid. According to the preparation method, the reaction esterification rate can be remarkably increased, the reaction time is shortened, the process is simple, and the large-scale application prospect is good.
Owner:PETROCHINA CO LTD

Rigid foam high flame retardant phase change polyurethane material and preparation method thereof

The application provides a hard-bubble high-flame-retardant phase change polyurethane material and a preparation method thereof, and belongs to the technical field of building materials. The preparation method is mixing polyether polyol, calcium carbonate, a gel phase change material, a catalyst, a foaming agent, a foam stabilizer, a plasticizer, a chain extender, ammonium polyphosphate, an antioxidant DNP and an ultraviolet absorber, then adding isocyanate, rapidly stirring, freely foaming, and aging to obtain the hard-bubble high-flame-retardant phase change polyurethane material. The gel phase change material is prepared by using mixed fatty acid formed by mixing myristic acid and octadecanoic acid as core material, using sodium silicate and tetraethyl silicate as aerogel wall material, using the hydrophobic end of an emulsifier to include the core material, and using the hydrophilic end of the emulsifier to combine with the aerogel wall material. The application effectively reduces the thermal conductivity of the prepared hard-bubble high-flame-retardant phase change polyurethane material, reduces heat loss caused by heat transfer, and improves temperature adjustment and control capacity.
Owner:SHIJIAZHUANG BANGDI POLYMER MATERIAL CO LTD +1

Method for preparing high-purity oleic acid from tea oil based on coupling of molecular distillation technology and urea embedding technology

The invention relates to a method for preparing high-purity oleic acid from tea oil based on coupling of a molecular distillation technology and a urea embedding technology in the technical field of deep processing of edible oil and fat. The method comprises the following steps: firstly, microfiltering the tea oil by using a 0.1-0.5 mu m membrane to remove impurities; then preparing mixed fatty acid; mixing the mixed fatty acid with a urea-ethanol solution according to the ratio of fatty acid to urea being 1: (1.2-1.8), stirring at 45-50 DEG C for 2-3 hours, cooling to-15 to-5 DEG C, crystallizing for 1-14 hours, separating and taking a liquid phase; and finally, treating the liquid phase by a wiped-film molecular distillation system to obtain high-purity oleic acid. According to the method, oleic acid enrichment is achieved, and meanwhile a large amount of heat-sensitive active ingredients are effectively prevented from being oxidized and decomposed.
Owner:贵州汇腾科技有限公司

Production method of modified dibutyltin dilaurate

InactiveCN120136916ATin organic compoundsMixed fatty acidDibutyl tin dilaurate
The invention provides a production method of modified dibutyltin dilaurate, and relates to the technical field of chemical engineering. The method comprises the following steps: sequentially adding coconut oil acid, dibutyltin dichloride and ethanol raw materials into a reactor, and stirring to obtain a mixed solution; adding a catalyst into the mixed solution, and stirring and reacting at 40 DEG C to obtain a first reaction solution; adding a sodium hydroxide solution into the first reaction solution, and adjusting the pH value to obtain a second reaction solution; stirring the second reaction solution at 40 DEG C to obtain a third reaction solution; distilling the third reaction liquid, and removing the solvent to obtain a crude product; carrying out water washing treatment on the crude product; and drying the washed product to obtain the modified dibutyltin dilaurate product. The coconut oil acid is used for replacing lauric acid, the coconut oil is used as liquid feeding, the feeding method is more convenient, and dibutyl coconut oil acid is mixed fatty acid tin mainly containing dibutyltin dilaurate and is low in melting point and convenient to use in winter.
Owner:NINGXIA LINGSHI NEW MATERIAL TECH CO LTD

Modified palm oil polyol, preparation method thereof and polyurethane structural adhesive

The invention discloses a modified palm oil polyol, a preparation method thereof and a polyurethane structural adhesive, and belongs to the field of polymer chemistry, the preparation method comprises the following steps: (1) performing saponification reaction on palm oil by using alkali liquor to obtain mixed fatty acid salt; (2) carrying out acidification reaction on the fatty acid salt crude product by utilizing acid liquor to obtain mixed fatty acid; (3) mixing the mixed fatty acid with micromolecular polyol for esterification reaction to obtain palm oil-based polyol ester; and (4) performing epoxidation reaction on the palm oil-based polyol ester to obtain the modified palm oil polyol, and the modified palm oil polyol obtained by the preparation method provided by the invention can endow the polyurethane structural adhesive with the advantages of low viscosity, low hardness and high bonding strength.
Owner:HANGZHOU ZHIJIANG SILICONE CHEM +1

Pentaerythritol mixed fatty acid ester as well as preparation method and application thereof

The invention belongs to the technical field of pentaerythritol fatty acid ester synthesis, and particularly relates to pentaerythritol mixed fatty acid ester as well as a preparation method and application thereof. The preparation method comprises the following steps: mixing pentaerythritol, fatty acid, a catalyst and a water-carrying agent, and carrying out esterification reaction to obtain esterification reaction liquid; carrying out purification treatment on the esterification reaction liquid to obtain pentaerythritol mixed fatty acid ester; the fatty acid comprises n-heptanoic acid, n-octanoic acid and 3, 5, 5-trimethyl hexanoic acid, and the molar ratio of the n-heptanoic acid to the n-octanoic acid to the 3, 5, 5-trimethyl hexanoic acid is (1-8): (1-8): 2. According to the invention, acid raw materials for esterification reaction are reasonably selected to react with pentaerythritol, and meanwhile, the molar ratio of three fatty acids is regulated and controlled, so that the obtained pentaerythritol mixed fatty acid ester has the characteristics of low viscosity and high ignition point, thereby having excellent low-temperature fluidity and high-temperature stability; meanwhile, the pentaerythritol mixed fatty acid ester provided by the invention also has excellent electrical performance.
Owner:LANZHOU INSTITUTE OF CHEMICAL PHYSICS CHINESE ACADEMY OF SCIENCES

Coating method and application of hydroxy fatty acid-containing compound fertilizer

The invention provides a coating method and application of a hydroxy fatty acid-containing compound fertilizer. Comprising the following steps: preparing a solution from a mixture of medium-chain potassium 3-hydroxyaliphatate, long-chain potassium aliphatate and sodium alginate, and spraying the solution on the surfaces of compound fertilizer particles to form a pre-coating layer; then spraying a metal salt solution containing CaCl2 or MgCl2, reacting and drying under the condition of 40-60 DEG C, so that the mixed potassium aliphatate is converted into Ca / Mg metal soap in situ on the surfaces of the particles, thereby forming a hydrophobic metal soap film layer. The obtained film layer is insoluble in the initial stage, is resistant to water corrosion and can effectively delay dissolution of nutritional ingredients in the compound fertilizer; after application, the metal soap film is exposed in a microorganism or CO2 environment, and the metal soap film is gradually degraded, so that the controlled release of the fertilizer and the coating film layer is realized. The method is convenient to use and suitable for large-scale production of the compound fertilizer. Medium-chain 3-hydroxy fatty acid has a unique effect of promoting growth of underground rhizomes, and the fatty acid metal soap coated compound fertilizer can be used for promoting growth of underground rhizome crops so as to achieve the purpose of increasing production and income.
Owner:HUZHOU ZIJIN BIOLOGICAL TECH CO LTD

Trimethylolpropane mixed fatty acid ester, and preparation method and application thereof

This invention discloses a trimethylolpropane mixed fatty acid ester, its preparation method, and its applications. The mixed fatty acid ester is obtained by esterification of two or more fatty acids with trimethylolpropane. The fatty acids are selected from combinations of octanoic acid, decanoic acid, and oleic acid, or combinations of oleic acid with octanoic acid or decanoic acid. The mixed fatty acid ester of this invention possesses both a high flash point and a low pour point, while maintaining low viscosity at low temperatures. It also exhibits excellent dielectric properties, meeting the various requirements of electrical equipment for insulating media. Furthermore, this mixed fatty acid ester uses renewable fatty acids as raw materials, has good biodegradability, aligns with the trend of green and environmentally friendly development, and avoids the environmental pollution problems caused by traditional mineral insulating oils and some synthetic insulating oils. It has broad application prospects in power equipment such as transformers and capacitors.
Owner:LANZHOU INSTITUTE OF CHEMICAL PHYSICS CHINESE ACADEMY OF SCIENCES

Bastnaesite collecting agent and preparation method and application thereof

PendingCN120169569AFlotationMixed fatty acidActive agent
The invention belongs to the technical field of mineral flotation, and particularly relates to preparation of a bastnaesite collecting agent, which comprises the following steps: mixing and uniformly stirring mixed fatty acid ester, an oximation reagent, a solvent and a surfactant, adding an acid-binding agent in batches, controlling the reaction temperature to be lower than 40 DEG C, heating after the addition of the acid-binding agent is finished, reacting for 2-8 hours at the temperature below 70 DEG C, and filtering to obtain the bastnaesite collecting agent. And after the solvent is removed, the bastnaesite collecting agent is obtained. The bastnaesite collecting agent is applied to flotation of bastnaesite, and the grade and the recovery rate of the bastnaesite can be remarkably improved through the flotation process of one-time roughing, one-time scavenging and three-time concentration.
Owner:CHONGQING KOOPPER CHEM IND

A textile auxiliary composition and a process for its preparation

ActiveCN117822313BActive agentGlycerol
The application discloses a textile auxiliary composition, comprising: 60-90% of mixed fatty acid glyceride and the balance of mixed non-ionic surfactant, wherein the mixed fatty acid glyceride comprises a mixture of triglyceride, polyglycerol triglyceride, mixed fatty acid and polyglycerol; and the mixed non-ionic surfactant comprises fatty alcohol alkoxylate, fatty acid alkoxylate, glycerol monostearate and the like. The mixed fatty acid glyceride is first put into a reaction kettle, the reaction kettle is heated to 70 DEG C, and the mixed fatty acid glyceride is melted; the fatty acid alkoxylate, the glycerol monostearate and the fatty alcohol alkoxylate are weighed in the reaction kettle in sequence, constant temperature stirring and emulsification are carried out, and the product is obtained; then the product is transferred to a granulation packaging line, weighed, packaged and stored, and the textile auxiliary composition is obtained. The application can effectively solve the problem of oil and fat chemical waste, convert low-value by-products into high-value products, realize waste recycling and sustainable production of oil and fat chemicals.
Owner:APICAL OLEOCHEMICAL(TAIXING) CO LTD

A method for preparing medium-chain triglycerides, related products and applications

The application provides a preparation method of medium-chain triglyceride, related products and application, and relates to the technical field of oil manufacturing. The preparation method comprises the following steps: mixing anhydrous calcium hydrogen phosphate, hydroxyapatite, carboxymethyl chitosan, Candida rugosa lipase and water, stirring, ultrasonic treatment, centrifugation, and obtaining immobilized lipase; then, the immobilized lipase is used for enzymolysis reaction with coconut oil and / or palm kernel oil to obtain mixed fatty acids; and then, catalyzing esterification reaction between the mixed fatty acids and glycerol to obtain medium-chain triglyceride. Through adjusting the types and proportions of the components in the immobilized lipase, the hydrolysis selectivity of the lipase to medium-chain fatty acids is improved, and then the yield of the medium-chain triglyceride is improved.
Owner:GUANGDONG KEVIN BIOTECHNOLOGY CO LTD +2

Basil volatile oil vaginal suppository and its preparation method and application

The present invention discloses a basil volatile oil vaginal suppository, a preparation method, and an application thereof. The suppository is composed of a mixture of a water-soluble matrix, an oily matrix, basil volatile oil, and an emulsifier. The water-soluble matrix comprises distilled water, polyethylene glycol 4000, and polyethylene glycol 6000, and the oily matrix comprises mixed fatty acid glycerides (stearin). The ratio of the water-soluble matrix to the oily matrix is ​​8:8-10. The basil volatile oil vaginal suppository of the present invention has moderate hardness, is not easily deformed, has good plasticity and stability, and has a moderate dissolution time and good solubility. This prevents the drug from dissolving too quickly or too slowly in the human body, ensuring that the drug is absorbed in the body to achieve the desired effect. It can stably release the drug in the vagina while reducing irritation to the vaginal mucosa. It has a precise therapeutic effect and low side effects in the treatment of vaginitis caused by Candida albicans.
Owner:广州新华学院

Method for efficiently preparing arachidic acid and behenic acid by adsorbing and removing impurities from raw materials through bio-based calcium oxide

The invention discloses a method for efficiently preparing arachidic acid and behenic acid by adsorbing and decontaminating raw materials through bio-based calcium oxide, and relates to the field of grease chemical engineering, the method comprises the following steps: S1, high-erucic acid rapeseed oil raw materials are subjected to decontaminating treatment through an adsorption column filled with bio-based calcium oxide, and the bio-based calcium oxide is prepared by calcining aquatic organism shells; s2, carrying out acidic hydrolysis on the impurity-removed raw material to obtain mixed fatty acid; according to the method for efficiently preparing the arachidic acid and the behenic acid by adsorbing and removing impurities from the raw materials through the bio-based calcium oxide, the bio-based calcium oxide is prepared from waste shells, high-value utilization of waste is achieved, and the cost is low. The material has a high specific surface area and abundant mesopores, and shows a selective adsorption capacity far higher than that of common calcium oxide on polar impurities such as thioglycoside and colloid, the removal rate can reach 88% or above, and the purity of the raw materials is guaranteed from the source.
Owner:HAIHE ENVIRONMENTAL PROTECTION TECHNOLOGY (DEZHOU) CO LTD +1

A continuous separation and purification device and method for oil methyl esterification reaction liquid based on super-hydrophobic PVDF membrane

The application belongs to the field of separation and purification, and provides a continuous separation and purification device and method for oil methyl esterification reaction liquid based on super-hydrophobic PVDF membrane. The device comprises a super-hydrophobic separation membrane, a separation cavity, an oil outlet cavity, a magnetic attraction assembly and an oil collection tank. The super-hydrophobic separation membrane, the separation cavity and the oil outlet cavity are clamped by the magnetic attraction force of the magnetic attraction assembly; after the acidic oil methyl esterification reaction liquid is poured into the separation cavity, the mixed fatty acid methyl ester in the mixed methyl esterification reaction liquid is separated and purified by the super-hydrophobic porous PVDF membrane; in order to prevent the separation membrane from being damaged due to excessive oil pressure, the upper liquid is discharged into the oil inlet cavity through the oil discharge port, and then is circulated into the separation cavity through the external pipeline; the lower liquid continues to be separated and purified by the super-hydrophobic separation membrane, so that the continuous and rapid separation and purification of the acidic oil methyl esterification reaction liquid are realized.
Owner:DALIAN UNIV OF TECH

Bear gall hemorrhoid suppository composition and preparation method thereof

The invention relates to the technical field of medicine, in particular to a bear gall hemorrhoid suppository composition and a preparation method thereof.The preparation method comprises the steps that calcined calamine, nacre mother of pearl and borneol are smashed into fine powder and sieved; mixing and grinding the bear gall powder and the bile massecuite through a running-in method to form a pasty mixture; and heating the mixed fatty glyceride to 50-60 DEG C, adding the fine powder and the paste mixture, uniformly stirring and mixing, and performing injection molding and cooling to prepare the bear gall hemorrhoid suppository. Wherein the injection cooling process comprises the following steps: acquiring suppository surface images and suppository weight information of corresponding suppositories under each production batch; the crack defect degree and the bubble defect degree are determined according to the suppository surface image; determining weight difference characteristics according to the suppository weight information, wherein the weight difference characteristics comprise system deviation and random deviation; according to the crack defect degree, the bubble defect degree and the weight difference characteristic, the adjusting mode of the cooling mode, the cooling temperature and the injection amount is determined; the suppository forming quality is effectively improved.
Owner:SHANDONG ZHONGTAI PHARMA

Troxerutin suppository and preparation method thereof

The invention belongs to the technical field of medicines, and particularly relates to a troxerutin suppository and a preparation method thereof. The invention provides a troxerutin suppository. The troxerutin suppository is prepared from the following raw materials in percentage by mass: 20-40% of troxerutin, 25-35% of cocoa butter and 35-45% of mixed fatty glyceride. According to the troxerutin suppository, the cocoa butter and the mixed fatty glyceride are adopted as auxiliary materials of the suppository, meanwhile, the cocoa butter and the mixed fatty glyceride are optimized to be matched with the troxerutin in a proper mass ratio, the obtained troxerutin suppository has good stability, and the release degree meets the standard. Meanwhile, the troxerutin suppository provided by the invention can realize rectal administration, reduces gastrointestinal irritation, is long in acting time, improves bioavailability, is suitable for patients who cannot take orally or are difficult to take orally, and improves drug compliance.
Owner:HANGZHOU HUANGSEN BIOLOGICAL TECH CO LTD

Preparation method of foaming material, foaming material and refrigeration equipment

The invention provides a preparation method of a foaming material, the foaming material and refrigeration equipment, and the preparation method of the foaming material comprises the following steps: mixing epoxy fatty glyceride and hydroxyl functionalized ionic liquid to obtain mixed fatty glyceride; mixing the mixed fatty glyceride with a polyol cross-linking agent to obtain composite polyol; and mixing the composite polyol, the polyether polyol, the composite foaming agent, isocyanate and the auxiliary agent, and foaming to obtain the foaming material. The hydroxyl functionalized ionic liquid can promote the compatibility degree between different phases, improve the layering phenomenon after compounding of different materials, and improve the cell density of the foaming material.
Owner:TCL HOME APPLIANCES (HEFEI) CO LTD