The invention discloses a method for extracting
sodium lignin sulfonate from a
papermaking black liquor employing sulphur treatment. The method is characterized by comprising the following steps: 1, injecting a
black liquor into a reaction circulating tank, pumping the
black liquor to the top of a reaction absorption
tower by using a pump, and spraying down from a solution distribution
sieve at the top; 2, feeding an SO2
acid gas generated by a burner into the bottom of a reaction
tower by using an exhaust fan through a pipeline, and generating reverse gas-liquid reaction by a gas inside the
tower and the black liquor sprayed down from the top; 3, absorbing SO2 in a cycle to carry out sulfuration reaction, so as to control the pH value to 3.5-4.0; 4, sulfonating
lignin and finishing
winterization to sink into the bottom of the tank after foam of reaction liquid disappears in a
precipitation tank, and discharging upper brown liquid to obtain
lignin pulp; 5, pumping the pulp into a
filter press to filter the liquid by a pump, baking and packaging after crushing a
filter cake, so as to obtain the product. The method is low in cost, safety production is achieved, the liquid after reaction is a
sodium sulfite solution, and a pulping material, and the solution after lignin is filtered and pressed can be prepared into an alkaline pulp. Thus, cyclic utilization of resources is achieved.