The invention provides a determination method for rapid screening of plastic part color
masterbatch carcinogenic dyes, and the determination method for rapid screening of plastic part color
masterbatch carcinogenic dyes comprises the following steps: crushing a plastic sample, adding the crushed plastic sample into
dichloromethane, carrying out swelling and decoloration, and carrying out ultrasonic extraction to obtain a swelling
mixed solution; adding methylbenzene into the swelled
mixed solution to swell and decolor, and performing ultrasonic extraction and concentration to obtain a
concentrated extract; adding the
concentrated extract into a
methanol precipitator, and separating to obtain a precipitate
mixed solution; and eluting the precipitate mixed solution through an
activated alumina small column,
drying, and re-dissolving in
methanol to obtain a to-be-detected solution, and analyzing by using a liquid chromatograph-
mass spectrometer. Dye molecules are selectively released through step-by-step swelling of
dichloromethane and
toluene, so that the extraction effect of the color
masterbatch dye in the plastic is improved; through combination of step-by-step
solvent synergistic swelling extraction and multi-stage purification,
drying of
polymer dissolved impurities is avoided, and efficient and accurate extraction and determination of the plastic color masterbatch dye are realized.