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2453results about How to "Good emulsifying effect" patented technology

Preparation method of high-solid-content aqueous polyurethane for leather

The invention relates to the field of synthetic leather material polyurethane, in particular to a preparation method of high-solid-content aqueous polyurethane for leather. The method comprises the process steps of: prepolymerization reaction: reacting polyol, a hydrophilic chain extender and isocyanate monomer; monomer modification: adding polyhydroxy monomer to be modified together with polyurethane prepolymer; salt formation by neutralization: adding a neutralizing agent so that an emulsion forms salt ion groups; and chain extension subsequent to emulsification: dissolving an external emulsifying agent and a sulfonic acid chain extender in water to obtain a solution and adding the solution to the system for performing emulsification. In the invention, the emulsification property of theemulsion is improved by using carboxylic acid type and sulfonic acid type chain extenders, so that polyurethane and water are fully emulsified; simultaneously, due to the employment of the method in which self emulsification and external emulsification are combined, not only the stable emulsion can be synthesized, but also the solid content can be increased; in addition, the use of water as the solvent in emulsification is consistent with the requirement of clean production process; and the finally-synthesized emulsion has good film forming performance, high drying speed, no yellowing, excellent mechanical properties and short process flow, is suitable for the synthesis of leather substrates or surface materials, and can take the place of solvent-type products.
Owner:溧阳常大技术转移中心有限公司

Preparation method of high dispersed white carbon black

The invention discloses a preparation method of high dispersed white carbon black. According to a new method and technology, a synthesis reaction of liquid soluble glass and concentrated sulfuric acid is carried out in two steps by first preparing fine seeds, and then carrying out a synthesis reaction, wherein the synthesis reaction is a precipitation reaction carried out under effects of an organic surfactant SDS and a composite silane coupling agent. The high dispersed precipitated white carbon black specially used in high-performance tyres is obtained through particle surface cladding, modification treatment, press filtration, washing, pulping and pressure drying. The method improves a traditional white carbon black production technology of a precipitation method by optimizing technological parameters and using an optimized auxiliary agent to meet a requirement of enhanced product dispersiveness; besides the method overcomes defects of an ordinary precipitation method, such as crude particles, wide distribution, strong hydrophilism and weak mixing dispersion. A prepared product has characteristics of fine primary particles, low surface hydroxyl content, increased lipophilicity,high bonding force with rubber high molecules and high wettability, and is an ideal reinforcing filling material specially used in high-performance tyres.
Owner:FUJIAN ZHENGSHENG INORGANIC MATERIAL

Method of preparing silicon dioxide delustrant by large pore volume gel

The invention relates to a preparation method of a silicon dioxide flatting agent used for coating flatting with a large pore volume gelatin method, which comprises the following steps of: adding a sodium silicate water solution in a reaction kettle; at the temperature of 26 DEG C and under stirring, adding 30% sulphuric acid until forming gelatin in the kettle; then stirring for 15min, raising the temperature to 50 DEG C and continually adding the sulphuric acid until pH value being up to 3; when no gelatin block by stirring, slowly adding 30% sodium hydroxide into the reaction kettle, regulating the pH value to be 5-6, and then regulating the pH value to be 9-10 by using ammonia water; and raising the temperature to 98 DEG C, ageing for 1 hour, adding water for cooling to the temperature of 75 DEG C, filtration washing, slurrying, sponging drying and crashing classifying to obtain the finished product. The product has the characteristics of large pore volume, large specific surface area, high purity, moderate DBP absorption value, good dispersion performance, high transparency and the like as well as the advantages of reasonable technology and high production efficiency. The product can be added with wax for carrying out surface treatment, thus leading the surface paint film of the coating to be smooth, and improving scratch resistance and precipitate resistance.
Owner:通化双龙化工股份有限公司

Industrial production method of hydrolyzed wheat protein for feeding

The invention discloses an industrial production method of hydrolyzed wheat protein for feeding, belonging to the technical field of feed additive production. In the method, through the method of synergy of multiple enzymes and combined treatment of multiple steps, the hydrolyzed wheat protein for feeding is prepared by taking wheat gluten meal and water with weight ratio of 1:10-1:2 and adding compound enzyme, ensuring the mass percent concentration of the compound enzyme in the solution is 0.2-1.4%, hydrolyzing the mixture for 1-13h under the conditions that the temperature is 30-70 DEG C and pH value is 5.0-10.0, then carrying out such processes as filtering, decoloring and drying, etc. Compared with the traditional methods, the method of the invention features mild hydrolysis conditions, sanitation and safety and maintains the original nutritive composition of amino acid free of loss; the hydrolysate is low in salt content, mellow in mouth feel and high in yield which is up to 98%. The tests that the hydrolyzed wheat protein is added in the feed for suckling pigs, chicks, calves, aquaculture and the like to be used show that the hydrolyzed wheat protein has the advantages and evident effects of improving daily feed intake, reducing diarrhea rate, enhancing immunity, slowing weanling stress, improving growth performance and the like.
Owner:郑州新威营养技术有限公司

Preparation method and application of polyphenol-protein/polypeptide-carbohydrate covalent complexes

The invention discloses a preparation method and application of polyphenol-protein / polypeptide-carbohydrate covalent complexes, and belongs to the technical field of food ingredients and food processing. The method comprises the steps that polyphenol, protein / polypeptide are used as raw materials, an alkaline method is used for inducing a reaction, and polyphenol-protein / polypeptide covalent complexes are prepared; then, a carbohydrate and the prepared polyphenol-protein / polypeptide covalent complexes are used as raw materials, and a maillard reaction is utilized for preparing the polyphenol-protein / polypeptide-carbohydrate covalent complexes. According to the preparation method, the natural raw materials are adopted, no any organic reagent is adopted, the polyphenol-protein / polypeptide-carbohydrate covalent complexes with the good performance can be obtained through two steps, the preparation method is simple, efficient and safe, and production is easy. The polyphenol-protein / polypeptide-carbohydrate covalent complexes have the high oxidation resistance and emulsibility, and the beta-carotene emulsion stabilized by means of the polyphenol-protein / polypeptide-carbohydrate covalent complexes has the good physical and chemical stability.
Owner:CHINA AGRI UNIV

Method capable of improving instant dissolving performance of soybean milk powder

The invention relates to a method capable of improving the instant dissolving performance of soybean milk powder and belongs to the technical field of soybean product processing. The method comprises the following steps: (1) adding weak alkali water into soaked soybeans according to a certain proportion for pulping and after pulping, carrying out pulp and residue separation to obtain raw soybean milk; (2) after pulsed electric field processing is performed on the raw soybean milk, adding a proper amount of emulsifier, then carrying out high-pressure steam pulp boiling to obtain cooked soybean milk, adding a proper amount of citric acid into the cooked soybean milk, then adding protease for enzymolysis, carrying out enzyme deactivation and filtering after enzymolysis, adding a certain amount of a reducing agent into the filtered soybean milk to carry out blending and uniform mixing, carrying out vacuum concentration after the blended soybean milk is homogenized, and after concentration, carrying out spray-drying and spraying of soybean phospholipid oil to obtain the instant soybean milk powder. The method has the advantages that the requires process equipment is simple, and is safe to operate; according to the method, the pulsed electric field technology and the enzymolysis technology are utilized; by the synergistic effect of the added reducing agent and emulsifier, the instant dissolving performance of the prepared soybean milk powder is improved; meanwhile, the prepared soybean milk powder has no beany flavor and bitter taste.
Owner:永和食品(中国)股份有限公司

Emulsion gel embedding fat-soluble vitamins and production method based on pulsed electric field

The invention discloses an emulsion gel in which fat-soluble vitamins are embedded and a production method based on a pulse electric field. The production method includes the following steps: dissolving octenyl succinic acid modified starch in water, heating in a water bath, stirring until the material is completely gelatinized and dissolved, and cooling to room temperature; adding edible oil in which fat-soluble vitamins are dissolved to obtain a mixed solution; using a high-speed shearing machine and a high-pressure homogenizer to shear and homogenize the obtained mixed solution so as to a coarse emulsion; adding starch into the coarse emulsion, and uniformly stirring to obtain an emulsion; adding a methylcellulose solution to the emulsion, uniformly mixing and performing pulse electricfield treatment, heating in a water bath, degassing, and cooling to obtain an emulsion gel. The pulsed electric field of the invention promotes the interaction between methylcellulose and starch molecules, has a higher elastic modulus, and is easier to form a network structure that is more favorable for embedding fat-soluble vitamins. Thereby, fat-soluble vitamins are effectively embedded, and thepurpose of slowly releasing fat-soluble vitamins is achieved.
Owner:SOUTH CHINA UNIV OF TECH
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