Patents
Literature
Patsnap Eureka AI that helps you search prior art, draft patents, and assess FTO risks, powered by patent and scientific literature data.

33 results about "Dodecylbenzene" patented technology

Dodecylbenzene is an organic compound with the formula C₁₂H₂₅C₆H₅.Dodecylbenzene is a colorless liquid with a weak oily odor. Floats on water. This colourless waxy solid consists of a dodecyl group (C₁₂H₂₅) attached to a phenyl group (C₆H₅). Dodecylbenzene is a precursor to sodium dodecylbenzenesulfonate, a surfactant that is a key ingredient of household laundry detergents, such as detergent powder.

Preparation method of polyvinyl alcohol / polyaniline / carbon nanotube composite hydrogel based on dodecylbenzene sulfonic acid molecular bridge

The invention discloses a preparation method of polyvinyl alcohol / polyaniline / carbon nanotube composite hydrogel based on a dodecylbenzene sulfonic acid molecular bridge, and relates to the technical field of polymer composite materials and energy storage devices. The invention innovatively provides a'molecular bridge 'strategy, and a highly stable interface structure between PANI and CNTs is constructed in a PVA hydrogel matrix by adopting DBSA as a bifunctional molecule linking agent. Specifically, through the pi-pi stacking effect of one end of a DBSA molecule and CNTs and ionic bonding of the other end of the DBSA molecule and PANI, an active material is stitched to a conductive skeleton on the molecular level, and a highly integrated three-dimensional conductive network is formed. The interface engineering design starting from the molecular level fundamentally solves the problem of structure degradation of PANI in the cycle process, endows the electrode material with good cycle stability, excellent rate capability and enhanced charge storage capability, and also has excellent mechanical flexibility.
Owner:GUILIN UNIVERSITY OF TECHNOLOGY

A composite biological pond cleaning agent containing tea saponin and a preparation method thereof

This invention belongs to the field of biological agents for aquaculture, and discloses a compound biological pond-cleaning agent containing tea saponin and its preparation method. The compound biological pond-cleaning agent of this invention comprises the following components by weight: 3-10 parts tea saponin, 60-70 parts roe beetle root powder, 10-20 parts Buddleja officinalis, 5-10 parts compound microbial powder, 3-8 parts adjuvants, and 10-20 parts carrier; the adjuvant is a mixture of sodium lignin sulfonate and sodium dodecylbenzene sulfonate; the compound microbial powder is a mixture of Bacillus subtilis and photosynthetic bacteria; and the carrier is diatomaceous earth. This invention combines three natural active ingredients—tea saponin, roe beetle root powder, and Buddleja officinalis—with suitable adjuvants and a carrier, which can expand the pond-cleaning range and has good killing or inhibitory effects on harmful organisms such as wild fish, shrimp, crabs, and snails, as well as various pathogens. The pond-cleaning is thorough, and the raw materials are easily degradable, leaving no residue. It is environmentally friendly and has a long-lasting effect, which is of great significance for promoting the green and sustainable development of aquaculture.
Owner:潘培松

Gel-free high-stability positive electrode slurry, and preparation method and application thereof

The application belongs to the field of sodium ion battery materials, and mainly relates to a gel-free high-stability positive electrode slurry as well as a preparation method and application thereof. The positive electrode slurry raw materials comprise: 90-96 parts of sodium iron sulfate, 1-4 parts of a conductive agent, 2-6 parts of a binder, and 0.1-0.5 parts of a combined dispersant; the combined dispersant comprises: a monoester phosphate and a diester phosphate; wherein R in the ester group is one or more of dodecyl, phenyl, octyl, oleyl, polyethylene glycol group, and aminopropyl. The mixed system of the monoester phosphate and the diester phosphate is used as the dispersant, that is, the mixed system has high affinity with iron ions, locks the active metal ions on the particle surface, blocks the side reaction with the solvent, the short chain of the monoester quickly anchors the particle surface, the long chain of the diester extends into the solvent to form steric hindrance, and the double mechanism inhibits agglomeration, thereby improving the dispersibility and stability of the slurry.
Owner:CENT SOUTH UNIV

Combined inhibitor for reverse flotation magnesium removal of sedimentary phosphorite and method thereof

The invention relates to the technical field of mineral separation technologies, in particular to a combined inhibitor and method for reverse flotation magnesium removal of sedimentary phosphorite, and the combined inhibitor is prepared by compounding the following components in parts by mass: 20-30 parts of aluminum sulfate octadecahydrate, 50-70 parts of tartaric acid and 10-20 parts of citric acid. The method is completed through a technical route of coupling regulation and inhibition of apatite by a combined inhibitor and reinforced separation of calcium and magnesium carbonate minerals by a mixed collecting agent. The method comprises the following steps: removing magnesium through a'one-roughing, one-refining and one-sweeping 'process under the condition that the pH value is 6-7 by combining with a sodium oleate / dodecylbenzene sulfonic acid / 2-ethylhexyl phosphate 2-ethylhexyl ester mixed collecting agent, so as to obtain phosphate concentrate with MgO less than 0.8%, P2O5 more than 29% and recovery rate more than 90%.
Owner:YUNNAN PHOSPHATE CHEM GROUP CORP +1

Iron ore reverse flotation low-temperature collecting agent and preparation method thereof

The invention belongs to the technical field of mineral processing flotation reagents, and particularly relates to an iron ore reverse flotation low-temperature collecting agent and a preparation method thereof, the iron ore reverse flotation low-temperature collecting agent comprises the following raw materials by weight: 60-100 parts of sodium aliphatate, 10-30 parts of MES, 10-30 parts of soybean oleic acid, 5-10 parts of an anionic surfactant, 1-5 parts of sodium dodecyl benzene sulfate, and 5-15 parts of a palm light component. The iron ore reverse flotation low-temperature collecting agent is wide in raw material source, good in stability, simple in manufacturing process and low in production cost; and meanwhile, the low-temperature collecting agent for reverse flotation of the iron ore is high in beneficiation efficiency at low temperature, the grade of obtained fine iron powder is high, and the yield of concentrate is increased. The iron ore reverse flotation low-temperature collecting agent does not cause harm to the environment and human bodies, belongs to a green and environment-friendly collecting agent, and has a wide application prospect.
Owner:HEBEI SHUNJIA MINING PROD TECH CO LTD

Film coating method for improving film coating rate of microbial fertilizer particles

The invention relates to the technical field of microbial fertilizer preparation, and provides a coating method for improving the coating rate of microbial fertilizer particles in order to solve the problem of poor affinity between a hydrophilic material and hydrophobic microbial fertilizer particles and improve the coating rate of the hydrophilic material as a film layer to the microbial fertilizer particles. The fertilizer is composed of a microbial fertilizer particle core layer and a modified film layer coating the outer layer of the fertilizer, and the mass ratio of the core layer to the film layer is 100: (0.5-10). Wherein the core layer can be made of trichoderma harzianum, penicillium baylii or aspergillus niger microbial fertilizer particles; the raw material of the film layer can be composed of the following components: polyvinyl alcohol (PVA), a hydrophilic material (such as starch, glucose, maltose or dextrin) capable of providing glycogen, a surfactant capable of changing the surface tension of water, a wetting agent, a dispersing agent (such as lauryl sodium sulfate, disodium methylene dinaphthalene sulfonate, sodium dodecyl benzene sulfonate or fatty acid salt) and the like. According to the coating method for improving the coating rate of the microbial fertilizer particles, the higher coating rate is achieved, the coated microbial fertilizer further has the longer container life and the higher pressure resistance, the looseness problem is greatly solved, the problems that traditional microbial fertilizer particles are prone to inactivation, breaking and loosening are solved, and the yield of the microbial fertilizer particles is improved. Good popularization and application values are realized.
Owner:QINGDAO UNIV OF SCI & TECH

Reinforcing agent composition for improving friction performance of No.8 hydraulic transmission oil and application of reinforcing agent composition

The invention belongs to the technical field of lubricating oil, and particularly relates to a reinforcing agent composition for improving the friction performance of No.8 hydraulic transmission oil and application. The reinforcing agent composition is prepared from the following raw materials: ethyl pyrimiphos, 2-amino-2-oxy-1-(3-phenoxy phenyl) ethyl] 2-(4-dodecylbenzene)-3-methyl butyrate, a dispersing agent and base oil A. The invention further discloses a preparation method of the reinforcing agent composition. According to the invention, a compound system of ethylpyrimidinphosphorus and 2-amino-2-oxy-1-(3-phenoxy phenyl) ethyl] 2-(4-dodecyl-phenyl)-3-methylbutyrate is adopted, so that the friction performance is excellent, the friction performance of the hydraulic transmission oil 8 # can be improved, the test requirements of an Allison C-4 paper-based friction bench are met, and the friction performance of the hydraulic transmission oil 8 # is improved. And the device can adapt to different hydraulic transmission oil formula systems.
Owner:PETROCHINA CO LTD

Antibacterial detergent containing tea saponin and preparation method thereof

The invention relates to the technical field of detergents, in particular to a tea saponin-containing antibacterial detergent and a preparation method thereof. The preparation method comprises the following steps: mixing deionized water, tea saponin, dodecylbenzene sulfonic acid, vanillin, guar gum, glycerol, aromatherapy essential oil, a zeolite silver-loaded antibacterial agent and sodium hydroxide, and granulating to obtain tea saponin-containing antibacterial detergent powder; taking an oxidized starch-gelatin composite gel solution as a capsule inner shell wall material, reacting ethylenediamine tetraacetic acid with chitosan to obtain a chelating agent, mixing the chelating agent with a hydroxypropyl methylcellulose solution to obtain an outer shell wall material, and spraying the outer shell wall material to the surface of the capsule inner shell wall material to obtain a composite capsule shell; and packaging the tea saponin-containing antibacterial detergent powder by using the composite capsule shell to obtain the tea saponin-containing antibacterial detergent. The detergent prepared by the invention is good in foaming ability and strong in decontamination effect, and also has excellent antibacterial performance.
Owner:XINYANG NORMAL UNIVERSITY

Carbon fiber composite material for linerless liquid hydrogen container and its preparation method

This invention relates to a linerless liquid hydrogen container carbon fiber composite material and its preparation method. The preparation method includes the following steps: reacting a hydroxyl-terminated polymer with a sulfonyl chloride group to generate a first solution; the hydroxyl-terminated polymer includes a hydroxyl-terminated hyperbranched polymer, a hydroxyl-terminated polyether polyol, or a hydroxyl-terminated liquid rubber; the sulfonyl chloride group organic compound includes dodecylbenzenesulfonyl chloride or ethylsulfonyl chloride; reacting the first solution with 1-methylimidazole, washing the product with a solvent, and vacuum drying to evaporate the solvent to obtain an ionic liquid; mixing the ionic liquid uniformly with graphene or hexagonal boron nitride nanosheets, adding a curing agent, mixing uniformly, then adding epoxy resin, mixing uniformly, and repeatedly vacuuming to obtain a modified epoxy resin mixed solution; and using the modified epoxy resin mixed solution to wind and mold carbon fiber composite material parts. This invention enhances the low-temperature toughness and gas barrier properties of carbon fiber composite materials.
Owner:SOUTHEAST UNIV

Cleaning composition and application thereof, leveling process and electronic device

The invention provides a cleaning composition and application thereof, a leveling process and an electronic device. The cleaning composition comprises an anionic surfactant and an organic acid complexing agent, the anionic surfactant comprises one or more of ammonium dodecyl sulfate and dodecylbenzene sulfonic acid; the organic acid complexing agent comprises a first complexing agent containing a carboxylic acid group and a second complexing agent containing a phosphonic acid group, and / or the organic acid complexing agent comprises a third complexing agent containing a carboxylic acid group and a phosphonic acid group; in the cleaning composition, the mass percentage content of the anionic surfactant is less than 0.5%; the pH value of the cleaning composition is greater than 7 and less than or equal to 12. According to the cleaning composition, the foam amount can be effectively reduced by performing proper component matching and pH value regulation and control on the cleaning composition, grinding materials and other impurities remaining on the surface of a workpiece can be effectively removed by applying the cleaning composition to cleaning of the leveling workpiece, and the comprehensive performance of a semiconductor device is remarkably improved.
Owner:ZHUHAI CORNERSTONE TECH CO LTD

Surfactant combination

PendingCN122373884AActive agentEthyl group
This invention relates to a surfactant composition comprising: a) an anionic component A (hereinafter referred to as surfactant component A), which is selected from C 10 -C 14 Sodium alkylbenzene sulfonate, such as linear dodecylbenzene sulfonate; and b) non-anionic component B (hereinafter referred to as surfactant component B), which is selected from compounds having formula (I) and mixtures thereof, R-O-(CH2CH2-O). n -H(I), where R is a branched C8-C 10 Alkyl, particularly 2-ethylhexyl or 2-propylheptyl, and n is an integer in the range of 0 to 10, particularly in the range of 0 to 6.
Owner:BASF SE

Flexible ammonia concentration and distance double-parameter sensing element and preparation method thereof

The invention relates to a flexible ammonia concentration and distance double-parameter sensing element and a preparation method thereof, and belongs to the technical field of flexible sensors. According to the sensing element, a polyimide (PI) flexible substrate with a central electrode lead is used as a substrate, and a spiral carboxylated multi-walled carbon nanotube and dodecylbenzene sulfonic acid doped polyaniline composite material (MWCNT-COOH-DBSA-PANI) is used as a sensitive material; according to the sensing element, the distance is detected through an eddy current effect generated by a spiral sensitive material, and the ammonia gas concentration is detected by virtue of the synergistic gas-sensitive characteristics of MWCNT-COOH and DBSA-PANI; wherein the DBSA-PANI is used as a p-type semiconductor material and endows the sensor with the capability of detecting ammonia gas (NH3) at normal temperature, the MWCNT-COOH is used for constructing a three-dimensional conductive network and is connected with the DBSA-PANI, a rough surface structure formed by the MWCNT-COOH provides more active sites for NH3, and the NH3 adsorption capability of the sensing element is enhanced. The sensing element prepared by the invention has the advantages of flexibility, simple structure and convenience in attachment, and is suitable for synchronously sensing the ammonia concentration and distance between narrow curved surface layers of complex industrial equipment.
Owner:CENT SOUTH UNIV

A method for reinforcing copper matrix composites based on MAX phase

A method for reinforcing copper-based composite materials based on the MAX phase includes the following steps: (1) powder pretreatment; (2) high-temperature reduction; and (3) spark plasma sintering. This invention incorporates the MAX phase Ti4AlN3, which enhances the mechanical properties of copper-based alloys due to its high elastic modulus, good high-temperature plasticity, and thermal shock resistance. Traditional ball milling easily generates a large amount of heat, and the relatively soft copper material causes copper powder to agglomerate, resulting in a large particle size. This invention replaces the powder with a suspension, transferring the heat generated during ball milling by adding ethanol and isolating it from air. Sodium dodecylbenzoate is used as a dispersant, reducing the powder's agglomeration ability and accelerating the ball milling process. The combined effect of plasma activation and sintering densification refines the grain size of the alloy, ultimately producing a dense Cu-Ti4AlN3 composite material with superior mechanical properties and wider applications.
Owner:HEFEI UNIV OF TECH

Oil for hot heat treatment of steel

ActivePL249997B1Fatty alcoholMineral oil
The subject of the application is an oil for hot heat treatment of steel, which contains 80.5% - 92.0% (m / m) of base oil containing I) 20.0% - 60.0% (m / m) of wax - modified lanolin having a kinematic viscosity at 40°C of 485.0 - 598.0 mm2 / s and a pour point of 2°C - 16°C and characterized by a distillation range such that less than 5% V / V distils to 458°C and at least 95% V / V distils to 645°C, II) 20.0% - 45.0% (m / m) of mineral oil having a kinematic viscosity at 40°C of 28.0 - 39.0 mm2 / s and a pour point of -8°C to -18°C and which is characterized by a distillation range such that less than 5% V / V distills to 315°C and at least 95% V / V distills to 470°C, III) 5.0 - 40.0 (m / m) of Brightstock base oil, having a kinematic viscosity at 40°C of 470.0 - 560.0 mm2 / s and a pour point of -5°C to -12°C, and which is characterized by a distillation range such that,that less than 5% V / V distils up to 440°C and at least 95% V / V distils up to 675°C and contains two packages of improvers in the amount of: a) 1.5% - 6.0% (m / m) of a package of improvers containing, calculated on the total weight of this package, 5% - 9.9% (m / m) bis(nonylphenyl)amine and 5% - 9.9% (m / m) sulphurised calcium salts and alkyl derivatives of phenols, mainly dodecylphenol and 0.5% - 0.99% (m / m) tetrapropenylphenol isomers dissolved in mineral base oil, the content of which in the package is from 30% to 60% (m / m), b) 1.5% - 8% (m / m) of a package of improvers containing, in calculated on the total weight of this package, a mixture of 70% (m / m) hydrocarbon resins with 30% (m / m) non-aromatic hydrocarbons obtained from the vacuum residue after distillation of crude oil or by separating the raffinate - oil in the process of deasphalting the vacuum residue, and additionally contains 2 refining additives with different functions, in amounts of c) 0.2% - 4,0% (m / m) of ashless dispersant, type mono- and / or bis-polybutenesuccinimides, with a base number of not more than 18 mg KOH / g and a viscosity at 100°C of not more than 330 mm2 / s, d) 0.2% - 3.0% (m / m) of viscosity modifier - polymer of esters of acrylic acid and methacrylic acid with aliphatic alcohols (C1-C18), dissolved in mineral base oil and with a viscosity of the entire mixture at 100°C in the range from 660 mm2 / s to 980 mm2 / s,
Owner:INST NAFTY I GAZU - PANSTWOWY INST BADAWCZY

Water-saving type foam washing treatment agent for cotton fabric

PendingCN122279990Areduce dosageTo achieve the purpose of water savingPotassium persulfateDyeing wastewater
This invention discloses a water-saving foam washing agent for cotton fabrics. The foam washing agent comprises, by mass percentage, one or more of a polyoxyethylene ether compound, sodium dodecyl sulfate, or sodium dodecylbenzene sulfonate, accounting for 0.1-3%; potassium persulfate, accounting for 0.1-2%; and the balance being water. A treatment process using this water-saving foam washing agent for cotton fabrics includes dyeing the cotton fabric with reactive dyes, spraying the fabric with the foam washing agent, and steaming. The advantages of this invention lie in its ability to effectively reduce water consumption during the washing process, achieving water conservation, and addressing the generation of colored wastewater at its source, thus greatly assisting in the treatment of subsequent dyeing wastewater.
Owner:TIANJIN POLYTECHNIC UNIV +1

A palladium nanocatalyst, a preparation method thereof and application thereof in solar-driven spontaneous synthesis of solid aromatic amines from solid reactants

The application relates to the technical field of organic synthesis, and particularly discloses a palladium nanocatalyst, a preparation method thereof and application of the palladium nanocatalyst in spontaneous synthesis of solid aromatic amines from solid-state reactants driven by solar energy. The preparation method of the palladium nanocatalyst is as follows: 4-dodecylaniline diazonium salt is prepared by using 4-dodecylaniline, tetrafluoroboric acid and sodium nitrite; and the palladium nanocatalyst is prepared by using palladium acetate, 4-dodecylaniline diazonium salt and sodium borohydride. Under the condition of room temperature and H2 atmosphere, the above palladium nanomaterial is used as a catalyst, solid-state nitro compounds are subjected to static irradiation of sunlight, and solid aromatic amine compounds are synthesized. The spontaneous solid-state reaction driven by solar energy is used to produce aromatic amines, the reaction can be smoothly and spontaneously carried out, and it is only needed to perform static irradiation by sunlight at room temperature for a short time without introducing mechanical chemistry. The method has wide substrate applicability, and can prepare products with potential significance from the perspective of medicines.
Owner:HENAN HYDROGEN SILICON NEW MATERIAL TECHNOLOGY CO LTD

Method for preparing carbon quantum dot nano-fertilizer by using humic acid and application thereof

The application discloses a method for preparing carbon quantum dot nanofertilizer by using humic acid and application thereof, and comprises the following steps: uniformly mixing humic acid and dodecylbenzene, and then performing ball milling to obtain humic acid after ball milling; taking the humic acid after ball milling and a nitrogen dopant as raw materials to perform hydrothermal reaction, collecting supernatant after reaction, filtering the supernatant, freeze-drying the filtrate, and obtaining carbon quantum dot nanofertilizer, wherein the nitrogen dopant is one or more of diaminocyclohexane and diethylenetriamine. The application takes humic acid as a precursor, takes diaminocyclohexane or diethylenetriamine as a nitrogen source to perform nitrogen doping modification, adjusts the fluorescence wavelength of the carbon quantum dots prepared from humic acid, and improves the fluorescence quantum yield and biocompatibility of the carbon quantum dots; the prepared carbon quantum dot nanofertilizer can promote the growth and development of small rape, the release of root exudates, and the activation of nitrogen and phosphorus in the rhizosphere soil of rape.
Owner:SHANDONG AGRICULTURAL UNIVERSITY

Mixture for effectively cleaning stains and preparation method thereof

The invention relates to the technical field of cleaning agents, in particular to a mixture capable of effectively cleaning stains. Comprising the following components in percentage by weight: 10% of an anionic surfactant, 8% of a nonionic surfactant, 2% of a biological enzyme compound, 1.5% of a bacteriostatic agent, 3% of an adsorbent, 0.5% of a pH regulator, 0.2% of a preservative, 0.3% of essence microcapsules and the balance of deionized water as a solvent and a carrier, wherein the anionic surfactant adopts sodium dodecyl benzene sulfonate and is composed of hydrophilic sulfonic groups and hydrophobic dodecylbenzene groups, in an aqueous solution, the sulfonic groups can partially ionize sodium ions, molecules are made to carry negative charges, and therefore the characteristics of the anionic surfactant are shown; compared with the cleaning efficiency, the removal rate of rubber oxidation stains is increased by 40%, and the deep descaling time of the net surface is shortened to be within 3 minutes.
Owner:河南华药药业有限公司

Pediococcus pentosaceus, composition containing same and application

The present application relates to the technical field of microorganism, and particularly relates to a Pediococcus pentosaceus QHEK025, a composition containing the same and purposes. The Pediococcus pentosaceus is Pediococcus pentosaceus QHEK025, the preservation number is CCTCC NO: M 20252985, and the preservation is carried out in China Center for Type Culture Collection. The composition contains at least one of lactic acid dodecylbenzene and a culture of the strain. The composition is used for preparing a composition for feed fermentation. Advantages of the present application are as follows: (1) can efficiently degrade mycotoxins; (2) has probiotic properties, strong growth performance, strong acid tolerance, strong bile salt tolerance and strong osmotic pressure tolerance; (3) has good hydrophobicity and self-aggregation performance; (4) high safety.
Owner:QINGHAI UNIVERSITY

A self-compacting concrete and a method for producing the same

PendingCN122277168APolymer scienceCrushed stone
This invention relates to a self-compacting concrete and its preparation method, belonging to the field of concrete technology. The raw materials for the self-compacting concrete provided by this invention include cement, fly ash, slag powder, sand, crushed stone, a high-performance water-reducing agent, an air-entraining agent, and water. The high-performance water-reducing agent is obtained by blending a polycarboxylate water-reducing agent, an organosilicon-modified hyperbranched star polymer, and a polyether-modified organosilicon polymer. The air-entraining agent is obtained by compounding sodium dodecylbenzene sulfonate and sodium fatty alcohol polyoxyethylene sulfonate. The self-compacting concrete prepared by this invention has a high water reduction rate, low slump loss, and high stability, resulting in a significant improvement in overall performance.
Owner:GUANGDONG XINRUILONG ECOLOGICAL BUILDING MATERIALS CO LTD

Method for detecting content of diethyl phosphite in FRC-6 flame retardant

PendingCN121385132AComponent separationDiethyl phosphatePhosphoric Acid Esters
The invention discloses a method for detecting the content of diethyl phosphite in an FRC-6 flame retardant. The detection method comprises the following steps: adding carbon tetrachloride, 4-dodecylaniline and triethylamine into an FRC-6 flame retardant sample, uniformly shaking, heating in a constant-temperature water bath kettle at 70 DEG C for 15 minutes, derivatizing diethyl phosphite to obtain a diethyl phosphite derivatization reaction product, and detecting by adopting a liquid chromatography external standard method and a quantitative method. According to the method, diethyl phosphite in the FRC-6 flame retardant sample is derivatized through carbon tetrachloride and 4-dodecylaniline, then the content of the FRC-6 flame retardant sample is measured through a liquid chromatography external standard method, the relative standard deviation RSD of the measurement result is smaller than 3.3%, the precision is high, the analysis and test method is simple, consumed time is short, multiple groups of parallel test results of the method are close, and the method is suitable for industrial production. The method has the advantages of simple operation, good repeatability and high accuracy, the adding standard recovery rate is 95-105%, the recovery rate is stable, the method is suitable for popularization and application, and tests show that the detection method is also suitable for determining the content of diethyl phosphite in other phosphate esters.
Owner:ZHEJIANG WANSHENG CO LTD

A modified dodecylbenzenesulfonate compound, its preparation method, its application, and a dust suppressant.

This application relates to a modified dodecylbenzenesulfonate compound. The preparation method of the modified dodecylbenzenesulfonate compound includes: an amino substitution reaction between 3-aminobenzene-1,2-diol and ammonium polyphosphate to obtain hydroxybenzene-containing ammonium polyphosphate; and a hydroxyl dehydration reaction between the hydroxybenzene-containing ammonium polyphosphate and dodecylbenzenesulfonic acid to obtain the modified dodecylbenzenesulfonate compound, which can simultaneously play the roles of dust inhibition and dust suppression, further improving the wetting and capturing effect of water droplets on dust and the effect of inhibiting dust pollution.
Owner:SHANDONG LUQIAO GROUP CO LTD +1

Process for the catalytic esterification of a plasticizer

This application relates to the field of chemical synthesis technology, specifically disclosing a method for preparing a plasticizer by catalytic esterification. The catalyst used in this method is a temperature-sensitive ternary bifunctional catalytic complex, and the raw materials include p-hydroxybenzenesulfonic acid, N,N-dimethyldodecyl tertiary amine, and p-dodecylbenzoic acid. The preparation method is as follows: first, the above-mentioned catalytic complex is prepared; then, a carboxylic acid or anhydride substrate, a fatty alcohol substrate, and the catalytic complex are added to a reaction vessel. After replacement with an inert atmosphere, the reaction process is dynamically controlled based on the water effluent rate. The esterification reaction is completed by segmented temperature control. The product is then obtained by cooling to precipitate the catalyst, pressure filtration separation, vacuum distillation, and decolorization filtration. The plasticizer prepared by this application can be used for the modification and processing of polymer materials such as polyvinyl chloride. The product has high purity and few impurities; the preparation method has high catalytic activity, easy catalyst recovery, and low raw material alcohol consumption. The catalyst can be recycled, which has the advantages of being green, environmentally friendly, and simple.
Owner:河南顺泓环保材料有限公司

Polyolefin master batch, high-conductivity modified carbon black as well as preparation method and application of high-conductivity modified carbon black

PendingCN121873435AMasterbatchPolymer science
The invention relates to the technical field of polyolefin pipes, in particular to a polyolefin master batch, high-conductivity modified carbon black and a preparation method and application of the high-conductivity modified carbon black. The high-conductivity modified carbon black is prepared by coating the surfaces of carbon black particles with a polymer of an organic conductive monomer and dodecylbenzene sulfonic acid. After the high-conductivity modified carbon black is applied to the polyolefin master batch, the mechanical property of the polyolefin material can be improved while the conductivity of the polyolefin material is improved; the technical problem that a polyolefin material is difficult to have certain conductivity and relatively good flexibility at the same time is solved.
Owner:BEIJING BEIHUA GAOKE NEW TECH +1

Liquid for hot hardening of steel

The subject of the application is a liquid for hot hardening of steel, which is characterized in that it contains - 79.5% - 91.0% (m / m) of base oil containing: I) 22.0% - 63.0% (m / m) of wax - modified lanolin with a kinematic viscosity at 40°C of 485.0 - 598.0 mm2 / s and a pour point of 2°C - 16°C and which is characterized by a distillation range such that less than 5% V / V distils up to 458°C and at least 95% V / V distils up to 645°C, II) 21.0% - 42.0% (m / m) of wax - jojoba oil, with a kinematic viscosity at 40°C of 20.4 - 27.5 mm2 / s and a pour point of 5°C to 10°C and which is characterized by a distillation range such that less than 5% V / V distils to 398°C and at least 95% V / V distils to 595°C, III) 3.5 - 34.0 (m / m) of Brightstock type base oil having a kinematic viscosity at 40°C of 470.0 - 560.0 mm2 / s and a pour point of -5°C to -12°C and which is characterized by a distillation range such that,that less than 5% V / V distils to 440°C and at least 95% V / V distils to 675°C, and contains two packages of improvers in the amount of: a) 2.5% - 6.5% (m / m) of the improver package containing, calculated on the total mass of this package, 5% - 9.9% (m / m) of bis(nonylphenyl)amine and 5% - 9.9% (m / m) of sulphurised calcium salts and alkyl derivatives of phenols, mainly dodecylphenol and 0.5% - 99% (m / m) of tetrapropenylphenol isomers dissolved in mineral base oil, the content of which in the package is from 30% to 60% (m / m), b) 2.5% - 9.0% (m / m) of the improver package containing, based on the total mass of this package, a mixture of 70% (m / m) of hydrocarbon resins with 30% (m / m) of non-aromatic hydrocarbons obtained from the vacuum residue after distillation of crude oil or by separating the raffinate - oil in the process of deasphalting the vacuum residue, and additionally contains 2 refining additives with different functions, in the quantities of: c) 1,4% - 6.0% (m / m) of an antioxidant additive containing 50% - 100% (m / m) of branched bis(nonylphenyl)amine and 0.25% - 1% (m / m) of diphenylamine, d) 0.1% - 3.2% (m / m) of an ash-free dispersant, of the mono- and / or bis-polybutenesuccinimide type, with a base number of not more than 18 mg KOH / g and a viscosity at 100°C of not more than 330 mm2 / s.,
Owner:INST NAFTY I GAZU - PANSTWOWY INST BADAWCZY

Vortex flexible fiber membrane with interstitial ammonia gas measurement function and development method of vortex flexible fiber membrane

The invention discloses a vortex flexible fiber membrane with an interstitial ammonia gas measurement function and a development method of the vortex flexible fiber membrane. The vortex flexible fiber membrane is composed of a flexible thermoplastic polyurethane (TPU) fiber membrane, a copper electrode lead and a vortex sensitive layer; the preparation method comprises the following steps: preparing a flexible TPU fiber film by adopting a high-voltage electrostatic spinning process; preparing a copper electrode lead on the surface of the flexible TPU fiber film through a magnetron sputtering process, and then preparing through holes in the two ends of the copper electrode lead; preparing a carboxylated multi-walled carbon nanotube and dodecylbenzene sulfonic acid doped polyaniline composite dispersion liquid, covering the surface, away from the copper electrode lead, of the flexible TPU fiber film with a spiral mask, and depositing the composite dispersion liquid on the surface of the flexible TPU fiber film through a pneumatic spraying technology to form a vortex sensitive layer; a multi-process fusion technology is adopted, and the prepared vortex flexible fiber membrane with the gap ammonia gas measurement function can be directly attached to a curved surface and has the capability of detecting the gap and the ammonia gas concentration.
Owner:CENT SOUTH UNIV

Cold hardening liquid for steel

ActivePL249996B1PolybutyleneDistillation
The subject of the application is a fluid for cold hardening of steel, containing 81.5% - 92.4% (m / m) of wax - modified jojoba oil, with a kinematic viscosity at 40°C of 20.5 - 26.5 mm2 / s and a pour point from -5°C to 3°C, which is characterized by a distillation range such that less than 5% V / V distils up to 395°C and at least 95% V / V distils up to 590°C, furthermore, the fluid for cold hardening of steel contains two packages of refining additives in the amount of: a) 2.2% - 7.3% (m / m) of a package of refining additives containing, calculated on the total weight of this package, 10% - 25% (m / m) of bis(nonylphenyl)amine and 1% - 5% (m / m) of calcium salts (C10-C47)-alkyl-aryl derivatives of petroleum-derived benzenesulfonic acids and 0.1% - 0.25% (mim) diphenylamine and 0.01% - 0.25% (m / m) branched dodecylphenol, dissolved in mineral base oil, the content of which in the package is from 20% to 50% (m / m), b) 0.2% - 7,6% (m / m) of a package of improvers containing, based on the total weight of this package, a mixture of 70% (m / m) of hydrocarbon resins with 30% (m / m) of non-aromatic hydrocarbons obtained from vacuum residue after distillation of crude oil or by separating raffinate - oil in the process of deasphalting of vacuum residue, and in addition to the above-mentioned components contains 3 improvers with different functions in the amounts of c) 1.9% - 6.3% (m / m) of an antioxidant additive containing, 50% - 100% (m / m) of branched bis(nonylphenyl)amine and 0.25% - 1% (m / m) of diphenylamine, d) 1.4% - 5.2% (m / m) of an ash-free dispersant, of the mono- and / or bis-polybutenesuccinimides, with a base number of not more than 18 mg KOH / g and a viscosity at 100°C of not more than 330 mm2 / s, e) 0.2% - 4.5% (m / m) of modified lanolin with a kinematic viscosity at 100°C of 28.5 - 35.7 mm2 / s and a pour point of 2°C - 16°C, which is characterised by a distillation range such that,that less than 5% V / V distils to 458°C and at least 95% V / V distils to 645°C.,
Owner:INST NAFTY I GAZU - PANSTWOWY INST BADAWCZY

A complexing extractant composition and method for lithium extraction from lithium-laden mother liquors

PendingCN122326974ADiketoneIsooctyl alcohol
This invention discloses a composite extractant composition and method for extracting lithium from lithium precipitation mother liquor. The composition includes a β-diketone extractant, an N1923 co-extractant, a modifier, and a diluent. The β-diketone extractant is one or more of dodecylphenyl-methyl-β-diketone and 1-phenyl-3-isoheptyl-1,3-propanedione. The modifier is one or more of isodecanol and isooctanol. The diluent is one or more of sulfonated kerosene, No. 260 solvent oil, white oil, n-heptane, and cyclohexane. The composition provided in this application uses N1923 as a co-extractant, which maintains good solubility and chemical stability under strongly alkaline conditions. This invention also provides a method for lithium extraction, which uses this composition to extract alkaline lithium precipitation mother liquor and uses CO2 gas for mild back-extraction to achieve efficient conversion of lithium bicarbonate and recovery of lithium. The back-extraction solution is close to neutral.
Owner:CHANGCHUN INSTITUTE OF APPLIED CHEMISTRY CHINESE ACADEMY OF SCIENCES

OSB boards modified with bioactive ingredients and manufacturing process

This invention provides an OSB board modified with bioactive ingredients and its production process. The production process includes preparing titanium dioxide molecular nests, preparing a solution containing bioactive ingredients, loading, impregnation, and molding. The loading process involves mixing the solution containing bioactive ingredients with porous titanium dioxide molecular nests and ball milling them at a ball-to-material ratio of 2-6:1, a ball milling speed of 50-54 rpm, a ball milling time of 17-23 min, and a ball milling temperature of 35-39°C. Then, palmitic acid, fatty alcohol polyoxyethylene ether, white oil, and sodium dodecylbenzene sulfonate are added, and the mixture is ball milled again at a ball milling speed of 142-151 rpm, a ball milling time of 21-27 min, and a ball milling temperature of 10-14°C. After the process, the mixture is dried to obtain the functional agent. The OSB board prepared by this invention exhibits good antibacterial and antifungal properties, maintaining excellent antibacterial and antifungal performance even in high-temperature, humid environments and environments with a moisture content of up to 30%.
Owner:寿光市鲁丽木业股份有限公司 +1

Composite phenol disinfectant and preparation method thereof

The invention discloses a compound phenol disinfectant and a preparation method thereof. The compound phenol disinfectant comprises the following components: crude phenol, dodecylbenzene sulfonic acid, acetic acid, phosphoric acid and water, wherein the mass percent of the crude phenol is 40-50%, the mass percent of the dodecylbenzene sulfonic acid is 15-22%, the mass percent of the acetic acid is 22-26%, the mass percent of the phosphoric acid is 2-8%, and the balance is water. The dodecylbenzene sulfonic acid and the phosphoric acid are added into the compound phenol disinfectant, so that the stability, the dispersity and the water solubility of the compound phenol disinfectant can be effectively improved, the compound phenol disinfectant is not easy to oxidize and deteriorate, the storage time is prolonged, and the sterilization and disinfection strength and the broad-spectrum property of the disinfectant can be further improved.
Owner:GUANGDONG YANGBLE BIOPHARMLS