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2039results about How to "Good emulsification" patented technology

Preparation method of high-viscosity organic silicon defoamer

InactiveCN104069654AIncrease the molecular chain lengthGood defoaming performanceFoam dispersion/preventionRoom temperatureOil phase
The invention discloses a preparation method of a high-viscosity organic silicon defoamer. The preparation method comprises the following steps of preparing a silicon grease by using organopolysiloxane, dewatering particles, catalysts and silicon resin under 180-240 DEG C, and stirring and uniformly mixing the silicon grease, polyether modified silicone oil and an emulsifying agent under 72-78 DEG C so as to obtain an oil phase mixture, dissolving a dispersing thickening agent in water; then adding a sodium hydroxide solution to uniformly stir to obtain emulsifying thickening water, adding the emulsifying thickening water into an oil-phase mixture, and carrying out emulsifying stir on the oil-phase mixture under 72-78 DEG C to obtain a coarse emulsifying object; and homogenizing the coarse emulsifying object under 50-55 DEG C to obtain a fine emulsifying object, adding residue water into the fine emulsifying object, stirring and uniformly mixing the fine emulsifying object under room temperature so as to obtain the high-viscosity organic silicon defoamer. The preparation method provided by the invention has the advantages that high-viscosity simethicone is utilized as an emulsifying main raw material, and thus, the obtained high-viscosity organic silicon defoamer has an ultra-strong defoaming speed and an anti-foam effect.
Owner:道尔达(西安)新材料有限公司

Polyacrylamide microsphere deep profile control agent and preparation method and application thereof

ActiveCN108315003AHigh solid contentHigh effective solid contentDrilling compositionMicrosphereEngineering
The invention relates to a polyacrylamide microsphere deep profile control agent and a preparation method thereof, and mainly solves the problems that in the prior art polymer microspheres used for profile control, plugging oil displacement of medium-high-permeability oil reservoirs are poor in effects, deep profile control cannot be realized, and cost is increased by increasing of the concentration of the polymer microspheres. The polyacrylamide microsphere deep profile control agent includes the following components by weight: 0.05-0. 5 parts of a polymer microsphere emulsion, 0.1 to 1 partof an oil-displacing surfactant, and 0 to 99.85 parts of water; wherein the polymer microsphere core-shell structure comprises a core and a shell, the core is a crosslinked polymer gel microsphere containing an ionic monomer structural unit, the shell is a crosslinked polymer gel containing an ionic monomer structural unit different or same in electrical property with the ionic monomer structuralunit in the core. The polyacrylamide microsphere deep profile control agent solves the problems well and can be used for field enhanced oil recovery application such as deep profile control, water shutoff and oil displacement in the medium-high-permeability oil reservoirs.
Owner:CHINA PETROLEUM & CHEM CORP +1

Method for preparing rosin-based surfactant

The invention discloses a method for preparing a rosin-based surfactant, which comprises the following steps: 1, adding a catalyst in an amount of 0.1 to 1.0 percent based on the mass of the rosin or a rosin derivative and polyethylene glycol or alkylene oxide in an amount of 2 to 3,000 percent based on the mass of the rosin or a rosin derivative into the molten rosin or a rosin derivative to allow the polyethylene glycol or alkylene oxide to react with the rosin or a rosin derivative at the temperature of 230 to 290 DEG C for 2 to 5 hours; 2, perform reduced pressure vacuumization and keeping a vacuum degree of less than or equal to 2kPa for 5 to 60 minutes to remove low-boiling-point substances; and 3, decreasing the temperature to 60 to 120 DEG C, adding antioxygen in an amount of 0.1 to 1 percent based on the mass of the rosin or a rosin derivative and an esterifying agent in an amount of 5 to 12 percent based on the mass of the rosin or a rosin derivative in batch into the product obtained by the step, performing a reaction at the temperature of 65 to 110 DEG C for 2 to 6 hours, and discharging the resulting material to obtain the rosin-based surfactant. The product has low surface tension, low critical micelle concentration, high emulsifying performance and low Krafft point and can be used as an emulsifier, a dispersant and an oil field assistant.
Owner:INST OF CHEM IND OF FOREST PROD CHINESE ACAD OF FORESTRY

Method for preparing gydroxysulfobetaine amphoteric surface active agent including polyether chain segment

The invention relates to a method for preparing a gydroxysulfobetaine amphoteric surface active agent including a polyether chain segment, belonging to the technical field of preparation of surface active agents. The gydroxysulfobetaine amphoteric surface active agent including the polyether chain segment is prepared by taking fatty amine polyoxyethylene ether and 3-chlorine-2-hydroxyl propane sodium sulfonate as raw materials. The gydroxysulfobetaine amphoteric surface active agent including the polyether chain segment is shown as a chemical structural formula in the specification. According to the gydroxysulfobetaine amphoteric surface active agent including the polyether chain segment synthesized by using the method disclosed by the invention, three hydrophilic groups consisting of polyoxyethenyl, quaternary ammonium salt and sulfonyl and hydrophobic alkyl are included; the gydroxysulfobetaine amphoteric surface active agent including the polyether chain segment has the two good surface activities of the non-ionic and amphoteric surface active agent; in addition, besides the good performance of the traditional gydroxysulfobetaine amphoteric surface active agent, the performances, such as water solubility, detergency, emulsifiability, dispersibility, solubilising power and the like, are improved obviously.
Owner:HENAN TITANING CHEM TECH
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