The present application belongs to the technical field of preparation of multi-curved surface
silicon carbide, and discloses a preparation method of reaction
sintering multi-curved surface
silicon carbide whole plate, comprising: mixing 100 parts of alpha-SiC
powder, 15-20 parts of composite
carbon source, 1-2 parts of
silicon carbide fiber, 2.3-3.8 parts of dispersing agent, 8-12 parts of water-soluble phenolic resin, 2-4 parts of additive and 42-46 parts of water according to weight parts, pre-dispersing, ball-milling, spray granulating, pressing into multi-curved surface
green body; the
green body is stacked with
graphite support parts and filled with graded silicon particles, and is subjected to step-by-step
degreasing and step-by-step reaction
sintering under vacuum
argon, and then is cooled after
temperature control to obtain the product. Through the synergistic effect of formula control of composite
carbon source, specific ternary additive and fine
sintering process, the technical problem of sintering
cracking and
cracking of multi-curved surface whole plate is eliminated, and the product density, bending strength and
fracture toughness are effectively improved.