270results about "Magnesium hydroxide" patented technology

The invention discloses a crosslinked polyethylene low-smoke halogen-free flame-retardant power cable which comprises the following hierarchical structures: a conductor layer; an insulating layer; a shielding layer; the shielding layer takes polyethylene as a matrix and comprises the following components in parts by weight: 70-78 parts of matrix, 20-25 parts of carbon black and 2-5 parts of nano montmorillonite modified lignin, the thickness of the shielding layer is 0.8-1.2 mm, the shielding layer and the insulating layer are molded through a co-extrusion process, and the interface gap is less than or equal to 0.1 mm. The nano montmorillonite modified lignin is adopted as a core flame retardant, the addition amount is reduced by 10%-15% compared with that of a traditional halogen-free flame retardant, by taking a 120 mm civil cable as an example, 18 parts of modified lignin replace 25 parts of a traditional flame retardant with the same flame retardant effect, the raw material cost is reduced by 8%-12%, lignin is derived from agricultural and forestry wastes, dependence on a petroleum-based material is reduced, and the environment-friendly flame-retardant cable material is suitable for industrial production. The gradient cooling process shortens the cooling time by 20%-30% compared with the traditional single-section cold water cooling process, and meanwhile, the pre-crosslinking process reduces the subsequent forming internal stress and reduces the rejection rate.

A method of photocatalytic degradation includes contacting a nanocomposite with a solution including one or more pollutants. The nanocomposite is a graphite-phase carbon nitride copper oxide and magnesium aluminum oxide (g-C3N4@CuO / MgAl2O4) material and includes a graphite-phase carbon nitride (g-C3N4) in an amount of 2 to 20 percent by weight (wt. %), copper oxide in an amount of 1 to 10 wt. %, and magnesium aluminum oxide (MgAl2O4) in an amount of 75 to 95 wt. % based on a total weight of the g-C3N4@CuO / MgAl2O4 material. The method further includes irradiating the nanocomposite with light having a wavelength of 400 to 800 nm in the absence of UV light to photocatalytically degrade the one or more pollutants in the solution.

The invention belongs to the technical field of inorganic chemical material preparation, and discloses a high-selectivity crystallization and impurity migration inhibition method of high-purity magnesium hydroxide. The method comprises the following steps: a phenylphosphonic acid surface modifier is introduced in the initial stage of crystallization, molecules of the phenylphosphonic acid surface modifier selectively occupy high-activity Mg < 2 + > sites of a magnesium hydroxide crystal face through bidentate coordination, and a molecular-level interface barrier with steric hindrance and electrostatic repulsion effects is formed, so that a Ca < 2 + > migration path is specifically blocked, and Mg < 2 + > crystallization is not influenced. The preparation method of the high-purity magnesium hydroxide is high in selectivity, high in efficiency, low in cost and environmentally friendly, the interface adsorption behavior of calcium ions is accurately intervened in the initial stage of crystallization through a molecular level surface engineering means, the technical bottleneck that impurity migration and lattice doping are difficult to control in a traditional process is fundamentally solved, and the preparation method is suitable for industrial production. And a brand new technical path is provided for green manufacturing of high-performance inorganic functional materials.

The invention relates to the technical field of inorganic material synthesis, in particular to a preparation method of a controlled-release magnesium hydroxide fertilizer. Comprising the steps of primary magnesium precipitation, hydrothermal treatment, secondary magnesium precipitation, anaerobic heat treatment and pulping. According to the method, firstly, crystal defects are eliminated through hydro-thermal treatment, crystal seeds with complete crystallinity are obtained, then the crystal seeds are added into a magnesium precipitation reaction system, the principle of Gibbs free energy minimization is followed, newly generated magnesium hydroxide tends to precipitate on the surfaces of the crystal seeds, under the interference effect of a crystal form regulator, the newly generated magnesium hydroxide crystal has many defects, and the magnesium precipitation effect is good. And then oxygen-free heat treatment is carried out, so that the defects of the magnesium hydroxide on the surface layer are further increased, and the initial dissolution and release capacity is improved. The controlled-release magnesium fertilizer which is high in early-stage release speed and long-acting in later-stage slow release is synthesized by utilizing a crystal defect engineering tool, and is different from a traditional coating scheme, and a brand new thought is provided for the design of the controlled-release fertilizer.

The invention relates to micron-sized hexagonal flaky magnesium hydroxide with controllable particle size by using sodium hydroxide and bittern as raw materials and a preparation method thereof, belonging to the technical field of inorganic material preparation. The preparation method of the granularity-controllable micron-sized hexagonal flaky magnesium hydroxide with sodium hydroxide and bittern as raw materials comprises the following three steps: preparation of a magnesium hydroxide precursor, hydrothermal synthesis and post-treatment. According to the micron-sized hexagonal flaky magnesium hydroxide which takes sodium hydroxide and bittern as raw materials and is controllable in particle size, the particle size distribution tested by a laser particle analyzer is as follows: D10 is 0.96-1.18 mu m, D50 is 1.83-2.13 mu m, and D90 is 3.85-4.44 mu m.

The invention relates to the field of preparation of battery materials and precursors of the battery materials, and discloses a method for efficiently preparing battery-grade manganous-manganic oxide by using electrolytic manganese residue leachate and a harmless treatment method for tail liquid of the battery-grade manganous-manganic oxide. Treating the manganese residue leachate concentrated water obtained in the previous step with ammonia water and oxygen to prepare battery-grade manganous-manganic oxide; adjusting the pH value of the filtrate obtained in the previous step to prepare magnesium hydroxide; the filtrate obtained in the previous step is subjected to evaporative crystallization, ammonium sulfate is prepared, finally, harmless treatment of preparation of battery-grade manganous-manganic oxide from the manganese residue leachate and the tail liquid of the battery-grade manganous-manganic oxide is achieved, and the recovery efficiency of valuable components is greatly improved.

The application discloses a preparation method of low-chlorine magnesium oxide. The method comprises the following steps: adding high-chlorine magnesium hydroxide slurry into an electrolytic cell, adding an anode liquid into an anode chamber, adding a cathode liquid into a cathode chamber, and adding a reinforcing agent into the high-chlorine magnesium hydroxide slurry. A direct current electric field is applied between the anode and the cathode by using a pulse power source to remove chlorine. Under the action of the electric field, the negative-charged chlorine ions move to the anode chamber by electromigration, and the chlorine moves to the cathode chamber by electrodialysis in the form of chlorides or other soluble ions, so as to reduce the concentration of the chlorine ions in the high-chlorine magnesium hydroxide slurry. After the chlorine is removed, the magnesium hydroxide is filtered and calcined to obtain the low-chlorine magnesium oxide. The method has the advantages that the high-energy-consumption processes such as ball milling and calcining in the traditional chlorine removal process of magnesium hydroxide are avoided, the harm of the chlorine ions to the equipment is reduced, the chlorine ions in the magnesium hydroxide are removed only by electromigration and electrodialysis, and the green and efficient preparation of the low-chlorine magnesium oxide is realized.

The invention belongs to the technical field of water treatment brine reuse, and provides an electrochemistry-based brine calcium and magnesium graded extraction process, which comprises the following steps: brine enters a primary electrolysis device for electrochemical reaction, carbon dioxide is introduced, and calcium ions in the brine are precipitated; further entering a primary precipitation separation device, and intercepting and collecting precipitated calcium; then the brine enters a secondary electrolysis device, the density of current applied to an electrode is increased, and magnesium ions in the brine are precipitated; the solution enters a secondary precipitation separation device, and precipitated magnesium is intercepted and recycled; drying the separated calcium and magnesium precipitates to obtain a product; and finally, introducing the reacted effluent into an ion exchange resin chromatographic column to remove untreated calcium and magnesium ions, and applying the obtained hardness-free alkaline water to the hydrogen production industry. By regulating the current density and introducing CO2, calcium and magnesium in various kinds of saline water are respectively precipitated and extracted, and the device is suitable for salt-containing organic wastewater, seawater, seawater desalination concentrated solution, bitter brine and industrial circulating cooling water.

The invention relates to micron-sized hexagonal flaky magnesium hydroxide with bittern as a raw material and a preparation method of the micron-sized hexagonal flaky magnesium hydroxide, and belongs to the technical field of inorganic material preparation, and the preparation method of the micron-sized hexagonal flaky magnesium hydroxide with bittern as the raw material comprises three steps of preparation of a magnesium hydroxide precursor, hydro-thermal synthesis and post-treatment. According to the micron-sized hexagonal flaky magnesium hydroxide prepared by taking the bittern as the raw material, the particle size distribution tested by a laser particle size analyzer is as follows: D10 is 0.71-0.85 mu m, D50 is 1.28-1.47 mu m, and D90 is 3.26-3.65 mu m.

The utility model discloses an ammonia-ammonium chloride catalysis system for decarburization of steel slag solid waste and flue gas, and belongs to the technical field of ferrous metallurgy. The ammonia-ammonium chloride catalysis system for steel slag solid waste and flue gas decarburization comprises a steel slag dissolving tank, an ammonia gas condensation cooler and a decarburization tower which are sequentially connected, the top of the decarburization tower is sequentially connected with an ammonia recovery system, an impurity filtering system and a calcium carbonate extraction system, and the bottom of the decarburization tower is connected with the calcium carbonate extraction system. The calcium carbonate extraction system is connected with the steel slag dissolving tank, and the steel slag dissolving tank is communicated with the ammonia recovery system. According to the technical scheme, the purpose of carbon capture and high-added-value resource reutilization of the steel slag are achieved.

The present disclosure relates to a brine purification device, its purification method and uses thereof. It is disclosed a brine purification device comprising a housing with an inlet configured to receive untreated brine and an outlet configured to discharge purified brine from a purification chamber; wherein the purification chamber within said housing is configured to have two separated hemispheres; wherein the at least one plate comprises a first engraved serpentine flow channel in a first side configured for the flowing of brine and a second engraved serpentine flow channel in the opposite side of the same plate configured for the flowing of a flowing fluid; wherein the two sides of the at least one plate are separated by an anion-exchange membrane in such a way that the untreated brine combine with counter-ions from the flowing fluid through said anion-exchange membrane; wherein the at least one plate is configured for a fluid velocity of 0.007 to 0.015 m / s considering a thickness of 3 to 6 mm.

Embodiments of the present disclosure are directed to systems and methods of removing carbon dioxide from a gaseous stream using magnesium hydroxide and then regenerating the magnesium hydroxide. In some embodiments, the systems and methods can further comprise using the waste heat from one or more gas streams to provide some or all of the heat needed to drive the reactions. In some embodiments, magnesium chloride is primarily in the form of magnesium chloride dihydrate and is fed to a decomposition reactor to generate magnesium hydroxychloride, which is in turn fed to a second decomposition reactor to generate magnesium hydroxide.

The objective of the present invention is to provide a method for producing a core-shell particle without requiring the synthesis of a core particle and the adjustment of the electric charge of the surface of the core particle, and to provide a method for producing a hollow particle without requiring thermal energy in a hollowing step of the core-shell particles. The method for producing the core-shell particle according to the present invention includes a step for forming a shell by directly fluorinating the surface layer of a core particle consisting of a magnesium inorganic salt. Next, the method for producing a hollow particle of a fluoride includes a step for removing only the core particle with an acid from the core-shell particle obtained by the above-mentioned producing method.

The invention relates to an extraction agent and an extraction method, and relates to the technical field of wet extraction of industrial solid waste, and the extraction agent comprises the following components in parts by mass: an extraction main agent, an anti-impurity stabilizer and an extraction aid; the extraction main agent comprises di (2-ethylhexyl) phosphate and mono (2-ethylhexyl) phosphate, the impurity-resistant stabilizer comprises an imidazoline derivative, a triazine derivative and dimethyl methylphosphonate, and the extraction assistant comprises isooctyl alcohol; the extraction method comprises the steps of ash ball preparation, impurity removal, extraction and the like. According to the extraction agent and the extraction method, interference impurities such as trace heavy metal ions, sulfides and cyanides generated due to component fluctuation in the purified ash of the calcium carbide furnace are selectively chelated, the impurities are prevented from being combined with the extraction main agent, and then the anti-interference stability of the extraction agent under the condition that the impurity content of the purified ash of the calcium carbide furnace fluctuates is improved; and the control difficulty in the production process is reduced.

To provide a method for producing particles of magnesium hydroxide by which the particles of the magnesium hydroxide can simply be grown by using a magnesium hydroxide material containing a prescribed amount of silicon.SOLUTION: The present disclosure relates to a process for producing particles of magnesium hydroxide. The manufacturing method according to the first disclosure includes a mixture forming step. In the mixture formation step, a mixture is formed by mixing a magnesium hydroxide material containing 100ppm or more and a slurry containing a seed crystal of magnesium hydroxide. The production method according to the first disclosure includes an aging method. In the aging method, the mixture is aged to grow the seed crystals and form particles of the magnesium hydroxide having a larger particle size than the seed crystals.SELECTED DRAWING: None

Disclosed herein are acid-base leaching methods and systems. Specifically, the systems and methods can include reacting a feed material comprising at least two metals selected from the group consisting of iron, magnesium, and calcium with a weak acid to produce a first leachate comprising ions of the at least two metals and an insoluble product; reacting the first leachate with a base to produce a first solid product comprising a first metal and a second leachate comprising ions of a second metal different from the first metal; and reacting the second leachate with the base to produce a second solid product comprising the second metal and a third leachate.

A method of making a material for capturing carbon dioxide from the earth's atmosphere, comprises producing an acid and a base with an electrochemical acid-base generator; dissolving a mineral in the acid to produce a mineral rich solution, separating silica from the mineral rich solution to form a silica depleted solution; adding a first portion of the base to the silica depleted solution to remove impurities by precipitation, adding a second portion of the base until ferrous hydroxide (Fe(OH)2) precipitates, then pausing base addition and removing the ferrous hydroxide precipitate from the solution. Then adding a third portion of the base to the iron-depleted solution to precipitate magnesium hydroxide (Mg(OH)2) and / or calcium hydroxide (Ca(OH)2). Then recovering a salt solution and directing the recovered salt solution to the electrochemical acid-base generator to produce a new acid and a new base. The magnesium hydroxide and / or calcium hydroxide may be used to capture and sequester carbon dioxide from a CO2-containing gas (e.g., air) by forming a carbonate or from the ocean by forming bicarbonate.

The present invention relates to a method for recovering valuable materials from waste. The method for recovering valuable materials from waste comprises the steps of: (a) pulverizing waste, which is generated from an evaporator or a crystallizer among equipment of a zero liquid discharge process for desulfurization wastewater, and then injecting same into a dissolution tank so as to dissolve same in a solvent and separating same into a gypsum (CaSO4) precipitate and a supernatant from which the gypsum has been removed; (b) dissolving, in a desulfurization tank, barium chloride (BaCl2) in the supernatant from which the gypsum has been removed, and separating same into a barium sulfate (BaSO4) precipitate and a supernatant from which the barium sulfate has been removed; (c) dissolving, in a hydroxide tank, sodium hydroxide (NaOH) in the supernatant from which the barium sulfate has been removed, and separating same into a magnesium hydroxide (Mg(OH)2 precipitate and a supernatant from which the magnesium hydroxide has been removed; and (d) injecting, into a salt pond, the supernatant from which the magnesium hydroxide has been removed, so as to recover sodium chloride (NaOH).

A process for recovering titanium dioxide from a titanium-bearing material, the process including the steps of: leaching the titanium-bearing material in a first leaching step at atmospheric pressure and at a temperature of 70 to 97° C. with a first lixiviant to produce a first leach solution comprising undissolved first leach solids that include a titanium content and a first leach liquor, the first lixiviant comprising hydrochloric acid at a concentration of less than 23% w / w; separating the first leach liquor and the undissolved first leach solids; leaching the first leach solids in a second leaching step at atmospheric pressure and at a temperature of 60 to 80° C. with a second lixiviant in the presence of a Fe powder reductant to produce a second leach solution comprising undissolved second each solids and a second leach liquor that includes a leached titanium content and iron content, the second lixiviant comprising a mixed chloride solution comprising less than 23% w / w hydrochloric acid and an additional chloride selected from alkali metal chlorides, magnesium chloride and calcium chloride, or mixtures thereof; separating the second leach liquor and the undissolved second leach solids; and thereafter separating the titanium dioxide and the iron content from the second leach liquor by precipitation, and regenerating the second lixiviant for recycle to the second leaching step.

The present disclosure relates to methods for producing hydrogen and calcium- or magnesium-bearing carbonates by capturing, converting, and storing carbon dioxide. The methods may include providing one or more calcium- or magnesium-bearing compounds; providing one or more water-soluble oxygenates; providing a plurality of catalysts; and reacting one or more calcium- or magnesium-bearing compounds and one or more water-soluble oxygenates with plurality of catalysts under conditions to produce hydrogen and calcium- or magnesium-bearing carbonates. The methods may include providing one or more calcium- or magnesium-bearing silicates; providing carbon monoxide; providing water vapor; and reacting one or more calcium- or magnesium-bearing silicates, carbon monoxide, and water vapor. The methods may include providing one or more calcium- or magnesium-bearing compounds; providing one or more water-soluble oxygenates; providing a catalyst; and reacting one or more calcium- or magnesium-bearing compounds and one or more water-soluble oxygenates with said catalyst.

The invention relates to the technical field of chemistry, in particular to a method for preparing magnesium hydroxide from a magnesium salt solution through a gaseous ammonia precipitation method, and the method is particularly suitable for extracting magnesium hydroxide from multi-component water mineral raw materials with high calcium content. The method comprises the following steps: in a nitrogen or inert gas atmosphere, introducing gaseous ammonia into a magnesium salt solution (comprising a multi-component water mineral raw material containing high-concentration calcium), and controlling the molar ratio of NH to Mg to be 2.5: 1-4: 1, so that magnesium hydroxide is precipitated and separated out; and after the precipitation process is completed, filtering and washing under the same atmosphere, and drying and crushing the obtained product. The method can realize one-step high-efficiency separation of magnesium hydroxide, and is also suitable for taking a multi-component natural mineral raw material with high calcium content as an initial solution.

The invention relates to a method for recovering a potassium resource from high-boron underground brine. The method comprises the following steps: (1) pretreatment; (2) separating sodium and potassium; (3) separating potassium and boron; and (4) preparing potassium chloride. The potassium chloride product is prepared by controlling the potassium separation concentration and recrystallizing, so that the potassium resource in the high-boron underground brine can be effectively recovered, and the agricultural potassium chloride product is prepared. According to the method, the potassium resource in the high-boron underground brine can be recycled, and a potassium chloride product is prepared; the method is simple and convenient in process, high in operability and easy to realize industrial production.

A structured powder for capturing CO2 from a gas stream includes an agglomerated powder, wherein magnesium hydroxide is 5 wt% to 90 wt% of the powder, and particles of the powder have a mean diameter of 1 micron to 40 microns. The structured powder has a mean largest dimension of 1 mm to 250 mm and an internal porosity of 10 vol% to 50 vol%.

The invention provides a method of producing an annealing separator, an annealing separator and a grain-oriented magnetic steel. An annealing separator obtained by the method has high purity and excellent dispersibility and bonding strength, thus allowing formation of a uniform, dense forsterite layer on the surface of a grain-oriented magnetic steel. The method of producing an annealing separator comprises the following steps: step (1) in which magnesium oxide and an ammonium salt solution are mixed and reacted to prepare a magnesium salt solution and ammonia, and then the purified magnesium salt solution and the ammonia are reacted to obtain magnesium hydroxide, step (2) in which one portion of the obtained magnesium hydroxide is subjected to high temperature ageing at 155 to 230° C. while another portion of the obtained magnesium hydroxide is subjected to low temperature ageing at 10 to 100° C., and step (3) in which the magnesium hydroxides aged under the different conditions are mixed and burned to obtain magnesium oxide for use as an annealing separator.

The present invention relates to a method for the CO2-neutral commercial recovery of metallic magnesium from seawater, wherein the recovered magnesium is further processed for use as a metallurgical raw material and can also be used as a starting material for the CO2-neutral recovery of hydrogen, and the CO2 recovered or released throughout the method is dissolved and bound to seawater.

A process and system are disclosed for producing lithium oxide from lithium nitrate. In the process and system, the lithium nitrate is thermally decomposed in a manner such that a fraction of the lithium nitrate forms lithium oxide, and such that a remaining fraction of the lithium nitrate does not decompose to lithium oxide. The thermal decomposition may be terminated after a determined time period to ensure that there is a remaining fraction of lithium nitrate and to thereby produce a lithium oxide in lithium nitrate product. The lithium oxide in lithium nitrate product may have one or more transition-metal oxides, hydroxides, carbonates or nitrates added thereto to form a battery electrode. The lithium oxide in lithium nitrate product may alternatively be subjected to carbothermal reduction to produce lithium metal.

A method may comprise producing liquid sodium and chlorine gas by electrolysis. The liquid sodium may be redox reacted with iron and / or manganese oxide in an ore to produce iron and / or manganese and s

The invention relates to a preparation method of a flaky magnesium hydroxide flame retardant, belonging to the technical field of inorganic material preparation, and the preparation method of the flaky magnesium hydroxide flame retardant comprises two steps of precipitation method synthesis and epoxy coating. According to the obtained flaky magnesium hydroxide flame retardant, the particle size distribution tested by a laser particle size analyzer is that D10 is 0.022-0.034 [mu] m, D50 is 0.591-0.608 [mu] m, and D90 is 1.398-1.749 [mu] m, 40 wt% of the flaky magnesium hydroxide flame retardant is added into EVA, the limit oxygen index of the EVA is increased to 31.1-32.0%, and the UL94 vertical combustion grade can reach V-1.

The invention discloses a wet desulphurization absorption tower, which comprises a desulphurization absorption tower body, the top end of the desulphurization absorption tower body is connected with a discharge pipe, the discharge pipe is made of metal with excellent thermal conductivity, the top end of the desulphurization absorption tower body is provided with an auxiliary heating mechanism, the auxiliary heating mechanism is provided with a feeding mechanism, and the feeding mechanism is provided with a discharging mechanism. A discharge mechanism is mounted on the auxiliary heating mechanism, and a drainage mechanism is further arranged in the auxiliary heating mechanism; the hot air flow moves upwards, enters the inlet pipe, penetrates through the first branch pipe and flows into the inner groove, the heating plate is connected with the discharge pipe in an attached mode, the hot air flow heats the heating plate, then the discharge pipe is heated, and therefore energy consumption of a heating device in the discharge pipe is reduced.

This invention discloses a low-viscosity, high-solids-content magnesium hydroxide suspension and its preparation method, comprising the following components by mass: 40-60 parts water, 40-60 parts magnesium hydroxide, 0.1-4 parts dispersant, and 0.01-2 parts stabilizer; wherein the viscosity of the magnesium hydroxide suspension is <100 cp; and the particle size D of the magnesium hydroxide is... 50 The particle size is 1~3μm. This invention successfully prepared a low-viscosity, high-solids-content magnesium hydroxide suspension that is stable for a long time and does not exhibit gelation by adding appropriate amounts of dispersants and stabilizers and adjusting the particle size of magnesium hydroxide particles, combined with high-speed stirring and ball milling processes. This not only improves processing efficiency and product performance, but also demonstrates significant economic benefits in transportation and storage.