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500 results about "Diethylene glycol monobutyl ether" patented technology

Water-based ink

The present invention relates to [1] a water-based ink including pigment-containing water-insoluble polymer particles A, water-insoluble vinyl-based polymer particles B and an organic solvent C, in which the water-insoluble polymer particles A are obtained by crosslinking polymer particles; the water-insoluble polymer particles B include at least one material selected from the group consisting of water-insoluble vinyl-based polymer particles and the like; the organic solvent C includes at least one compound selected from the group consisting of diethylene glycol monobutyl ether and diethylene glycol monoisobutyl ether, and propylene glycol, in which a total content of diethylene glycol monobutyl ether and diethylene glycol monoisobutyl ether in the water-based ink is not less than 0.8% by mass, and a content of an organic solvent having a boiling point of higher than 250° C. in the water-based ink is not more than 5% by mass; and a content of water in the water-based ink is not less than 45% by mass, and [2] an ink-jet printing method including the step of printing characters or images on a recording medium using the aforementioned water-based ink. The water-based ink of the present invention is excellent in long-term storage stability as well as ejection stability upon ink-jet printing, and can be improved in image quality of printed characters or images, rub fastness, water resistance, solvent resistance and adhesion to a substrate with a high level and a good balance when printed on a non-water absorbing recording medium.
Owner:KAO CORP

Lead-free silver and aluminum slurry for solar photocell and preparation method of slurry

The invention discloses lead-free silver and aluminum slurry for a solar photocell. The slurry is prepared from raw materials in percent by mass as follows: 75-80% of silver powder, aluminum powder and copper powder, 15-20% of organic bond, 1-5% of inorganic glass powder, and 1-5% of additive; the purities of the silver powder, the aluminum powder and the copper powder are more than or equal to 99.9%; the organic bond is prepared from the following materials in percent by mass of: 0.5-2% of butyl carbitol, 1-2.5% of resin, 1-4% of rosin, 11-13% of ethylene glycol monomethyl ether, 5-9% of diethylene glycol monobutyl ether, 65-75% of cyclohexanone and 10-20% of n-butyl alcohol; the inorganic glass powder is prepared from the following materials in percent by mass of: 1-3% of titanium dioxide, 55-75% of boric acid, 3-5% of aluminium sesquioxide, 15-25% of antimony oxide and 2-5% of zirconium oxide; and the additive is prepared from the following materials in percent by mass of: 35-45% of span and 55-65% of pump oil. The lead-free silver and aluminum slurry prepared by the raw material has the advantages of good weldability and strong adhesion and meets the lead-free environmental friendless requirement.
Owner:JIANGSU RUIDE NEW ENERGY TECH

Device and processing method for synthesis of ethylene glycol monobutyl ether through reactive distillation

The invention provides a device and technological process for synthesis of ethylene glycol monobutyl ether through reactive distillation. The device comprises a reactor, a reactive distillation tower, a treating tower, a condenser, a reboiler, a heat exchanger, a return tank, a kettle outlet tank, a pump and a pipeline. In the technological process, the reactive distillation tower is combined with the reactor and the treating tower. Acidic cation exchange resin or alkali anion exchanger is selected for being used as a catalyst. Preheated ethylene oxide and butanol enter into a reactor for reaction, and unreacted materials pumped into the reactive distillation tower react or are rectified on a tower plate or a filling material on the section; materials flowing down after passing through the reaction section are rectified through a stripping section; total reflux is conducted at the tower top of the reactive distillation tower; materials discharged from the tower kettle of the reactive distillation tower are pressurized to enter into the treating tower for rectification; the ethylene glycol monobutyl ether with the purity higher than 99.9 percent is obtained from the tower top of the treating tower, the yield is greater than 97 percent, and the diethylene glycol monobutyl ether is obtained from the tower kettle of the rectification tower. The device solves the problems that ethylene glycol monobutyl ether produced intermittently is not stable in product quality, the yield is relatively low, the loss of the catalyst is high, and sewage treatment is difficult.
Owner:TIANJIN PULAI CHEM TECH

High-temperature lead-free solder paste and preparation method

The invention relates to high-temperature lead-free solder paste and a preparation method. The high-temperature lead-free solder paste comprises lead-free electronic grade tin alloy powder and flux. Diethylene glycol monobutyl ether, diethylene glycol octyl ether and hydroxyl-terminated polybutadiene are added into a temperature control emulsifying machine and are heated and mixed, hydrogenated castor oil, polymerized rosin CLEARON105# and hydrogenated rosin are added into the temperature control emulsifying machine and are mixed to obtain primary mixed liquor, the primary mixed liquor is cooled, 2,3-dibromo 1,4-butylene glycol, sebacic acid and phenyl-butanedioic acid are added into the primary mixed liquor and then are mixed to obtain secondary mixed liquor, the secondary mixed liquor is cooled, polyamide wax is added into the secondary mixed liquor and then is mixed to obtain tertiary mixed liquor, the tertiary mixed liquor is cooled, fluorocarbon surfactant and triethanolamine areadded into the tertiary mixed liquor and then are mixed and vacuumized until the temperature returns to room temperature, the lead-free electronic grade tin alloy powder Sn95Sb5 is added into the prepared flux after standing at the temperature of 22-25 DEG C, and the lead-free electronic grade tin alloy powder and the flux are mixed for 15-20 minutes to obtain the high-temperature lead-free solder paste. The high-temperature lead-free solder paste has the advantages of fine solderability and wettability, high solder joint strength, high reliability and solderability in air and nitrogen protection.
Owner:惠州市斯泰尔科技有限公司

Halogen-free and lead-free solder paste and preparation method

The invention relates to a halogen-free and lead-free solder paste and a preparation method. The preparation method is characterized in that the method comprises the steps of adding diethylene glycol monobutyl ether, castor oil and polyisobutene in a temperature control emulsifying machine and mixing, then adding albolene, polymerized rosin and hydrogenated rosin and mixing again to obtain first mixing solution, reducing the temperature of the first mixing solution, adding succinic acid, sebacic acid and glutaric acid, and mixing again to obtain second mixing solution, reducing the temperature of the second mixing solution, adding polyamide wax and mixing again to obtain third mixing solution, reducing the temperature of the third mixing solution, adding a fluorocarbon surfactant and diethanol amine, then stirring and vacuuming until the temperature is restored to the room temperature, standing for 24h with low temperature, then adding lead-free electronic-grade tin alloyed powder Sn96.5Ag3.0Cu0.5, and stirring to obtain the halogen-free and lead-free solder paste. After being welded, the halogen-free and lead-free solder paste has the advantages and effects of fewer residues, extremely high surface insulation resistance, low corrosion, no needing of cleaning, good thixotropic property and electric conductivity, bright welding points after welding and incapability of collapsing easily.
Owner:惠州市斯泰尔科技有限公司

PLA-PBSA blown film and preparation method thereof

The invention provides a polylactic acid (PLA)/ poly(butylene succinate-butylene adipate) (PBSA) blown film and a preparation method thereof. The blown film comprises a mixture of PLA, PBSA, plasticizer diethylene glycol monobutyl ether adipate, a lubricant, a plastic lubricant and an antioxidant. The PLA, the PBSA, the lubricant, the plastic lubricant and the antioxidant are first mechanically mixed into a premix, the premix is added through a feeding port of a twin-screw extruder, meanwhile the plasticizer diethylene glycol monobutyl ether adipate is metered and added in through a liquid feeding port of the twin-screw extruder, modified polylactic acid blown film special resin is prepared by melt-extruding, water-cooling, pelletizing and drying, the modified polylactic acid blown film special resin is blown by a film blowing machine to form a transparent tear-resistant biodegradable film. The PBSA, the plasticizers, the lubricant, the plastic lubricant and the antioxidant can effectively increase the tensile elongation at break and tear strength of polylactic acid films, maintains the transparency of the polylactic acid, and solves the brittleness defects of the polylactic acid films. The polylactic acid (PLA)/ poly(butylene succinate-butylene adipate) (PBSA) blown film has good mechanical properties and excellent transparency, and can replace PE, PP, PVC and the like for preparation of films and sheets.
Owner:HEILONGJIANG XINDA ENTERPRISE GRP +1
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