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301 results about "Ethyleneglycol monobutyl ether" patented technology

High-temperature-resistant and wear-resistant lubricating oil for drilling fluid and preparation method of lubricating oil

The invention relates to high-temperature-resistant and wear-resistant lubricating oil for a drilling fluid. The lubricating oil is prepared from the following raw materials in parts by mass: 30-48 parts of palm oil, 11-14 parts of sulfurized isobutylene, 5-8 parts of fatty alcohol-polyoxyethylene ether, 6-9 parts of nano graphite powder, 4-9 parts of zinc dialkyl dithiophosphate, 8-12 parts of molybdenum oxygen dialkyldithiophosphate, 1-3 parts of 3, 4, 5-trimethoxyl cinnamic acid, 10-14 parts of lauric acid monoethanolamide phosphate, 16-19 parts of glycerine, 10-13 parts of ethylene glycol monobutyl ether and 20-30 parts of pentaerythritol. By reasonably compounding the palm oil and other additives, the lubricating performance, high-temperature resistance and wear resistance of the lubricating oil are effectively improved. Meanwhile, 3, 4, 5-trimethoxyl cinnamic acid and lauric acid monoethanolamide phosphate are added, so that the high-temperature resistance, the wear resistance and the antirust time of the lubricating oil are effectively improved under the joint effect of 3, 4, 5-trimethoxyl cinnamic acid, lauric acid monoethanolamide phosphate and other components, and the friction coefficient is greatly lowered.
Owner:青岛蓬勃石油技术服务有限公司

Oil based drilling cutting microemulsion cleaning solution and cleaning method thereof

Belonging to the technical field of environment-friendly application of drilling engineering oilfield chemistry in the petroleum and natural gas field, the invention relates to an oil based drilling cutting microemulsion cleaning solution and a cleaning method thereof. For the oil based drilling cutting microemulsion cleaning solution, a surfactant, a cosurfactant, an oil phase and water are mixed in a volume percentage of (17-56):(11-18):(10-33):(21-33) to form three phases, and the middle phase is the microemulsion cleaning solution. The surfactant is ether alcohol, preferably ethylene glycol monobutyl ether or phenoxy propanol, and the cosurfactant is short chain alcohol, preferably n-butyl alcohol or isopropyl alcohol. The cleaning solution and drilling cuttings are mixed uniformly according to a mass ratio of (0.5:1)-(3:1), then solid-liquid separation is carried out, and the base oil, cleaning solution and drilling cuttings cleaned out from the oil based drilling cuttings are separated into different phases. Compared with other oil based drilling cutting treatment technologies, the process is simple, the base oil recovery rate is greater than 80%, and the residual oil content of the drilling cuttings is less than 2%, thus meeting relevant environmental protection technical standards. Also, the microemulsion cleaning solution can be used repeatedly, and the treatment cost is low.
Owner:CHINA PETROLEUM & CHEM CORP +3

High-temperature lead-free solder paste and preparation method

The invention relates to high-temperature lead-free solder paste and a preparation method. The high-temperature lead-free solder paste comprises lead-free electronic grade tin alloy powder and flux. Diethylene glycol monobutyl ether, diethylene glycol octyl ether and hydroxyl-terminated polybutadiene are added into a temperature control emulsifying machine and are heated and mixed, hydrogenated castor oil, polymerized rosin CLEARON105# and hydrogenated rosin are added into the temperature control emulsifying machine and are mixed to obtain primary mixed liquor, the primary mixed liquor is cooled, 2,3-dibromo 1,4-butylene glycol, sebacic acid and phenyl-butanedioic acid are added into the primary mixed liquor and then are mixed to obtain secondary mixed liquor, the secondary mixed liquor is cooled, polyamide wax is added into the secondary mixed liquor and then is mixed to obtain tertiary mixed liquor, the tertiary mixed liquor is cooled, fluorocarbon surfactant and triethanolamine areadded into the tertiary mixed liquor and then are mixed and vacuumized until the temperature returns to room temperature, the lead-free electronic grade tin alloy powder Sn95Sb5 is added into the prepared flux after standing at the temperature of 22-25 DEG C, and the lead-free electronic grade tin alloy powder and the flux are mixed for 15-20 minutes to obtain the high-temperature lead-free solder paste. The high-temperature lead-free solder paste has the advantages of fine solderability and wettability, high solder joint strength, high reliability and solderability in air and nitrogen protection.
Owner:惠州市斯泰尔科技有限公司

Rust remover for ultrasonically cleaning metal mould and preparation method thereof

The invention discloses non-corroding ultrasonic cleaning equipment. A rust remover for ultrasonically cleaning a metal mould is used for rapidly and completely removing rusts on the surface of the metal mould, generating a dense and complete passivation film at the same time and avoiding a secondary oxidization. The rust remover is prepared from the following raw materials by mass percent: 8-30% of phosphoric acid, 6-25% of room-temperature steel surface conditioning agent, 1-4% of citric acid, 1-5% of tartaric acid, 1-4% of phytic acid, 1-8% of polyethylene glycol, 1-3% of penetrant JFC, 1-6% of ethylene glycol monobutyl ether and the balance of water. A preparation method of the rust remover comprises the following steps of: firstly, adding water with a calculated amount into a stainless steel reaction kettle, starting an agitator and controlling a rotary speed of the agitator to 40-60 r/min; then respectively taking the calculated amount of the phosphoric acid, the room-temperature steel surface conditioning agent, the citric acid, the tartaric acid, the phytic acid, the polyethylene glycol, the JFC and the ethylene glycol monobutyl ether and sequentially and slowly adding the materials into the reaction kettle; and adding the materials while agitating until the solution becomes a light-green transparent liquid.
Owner:DALIAN SANDAAOKE CHEM

PLA-PBSA blown film and preparation method thereof

The invention provides a polylactic acid (PLA)/ poly(butylene succinate-butylene adipate) (PBSA) blown film and a preparation method thereof. The blown film comprises a mixture of PLA, PBSA, plasticizer diethylene glycol monobutyl ether adipate, a lubricant, a plastic lubricant and an antioxidant. The PLA, the PBSA, the lubricant, the plastic lubricant and the antioxidant are first mechanically mixed into a premix, the premix is added through a feeding port of a twin-screw extruder, meanwhile the plasticizer diethylene glycol monobutyl ether adipate is metered and added in through a liquid feeding port of the twin-screw extruder, modified polylactic acid blown film special resin is prepared by melt-extruding, water-cooling, pelletizing and drying, the modified polylactic acid blown film special resin is blown by a film blowing machine to form a transparent tear-resistant biodegradable film. The PBSA, the plasticizers, the lubricant, the plastic lubricant and the antioxidant can effectively increase the tensile elongation at break and tear strength of polylactic acid films, maintains the transparency of the polylactic acid, and solves the brittleness defects of the polylactic acid films. The polylactic acid (PLA)/ poly(butylene succinate-butylene adipate) (PBSA) blown film has good mechanical properties and excellent transparency, and can replace PE, PP, PVC and the like for preparation of films and sheets.
Owner:HEILONGJIANG XINDA ENTERPRISE GRP +1

Preparation method of water-borne acrylic resin

The invention provides a preparation method of water-borne acrylic resin. The preparation method comprises the following steps of: (1) preparing blocked isocyanate; and (2) synthesizing acrylic resin, i.e., weighing 25-40 g of dimethylaminoethyl methacrylate, 25-40 g of butyl acrylate and 25-40 g of methyl methacrylate and uniformly stirring; adding 0.3-0.8 g of azo-bis-iso-butyrynitrile; adding 40-60 g of blocked isocyanate prepared by the first step and 20-30 g of ethylene glycol monobutyl ether into a flask provided with a stirrer, a thermometer, a condensing pipe and a dropping funnel; introducing nitrogen and stirring; heating to a temperature of 75+/-1 DEG C; slowly dropwise adding 1/4 to all mixed monomer and 1/3-3/4 initiator azo-bis-iso-butyrynitrile; preserving the heat and reacting for about 1 hour after the dropwise addition is finished; slowly dropwise adding residual monomer for about 2-3 hours; fully dissolving the residual initiator with the ethylene glycol monobutyl ether; slowly dropwise adding into a reaction bottle for several times; controlling the temperature to be kept at a temperature of about 80 DEG C; preserving the heat and reacting for 1 hour; cooling to a temperature of 50 DEG C and discharging to obtain the water-borne acrylic resin. The resin has the advantages of simple preparation process, environmental friendliness, good storage stability and excellent curing performance.
Owner:佛山科富科技有限公司

Graphene/waterborne epoxy zinc-rich coating with high corrosion resistance and strong adhesive force and preparation method of graphene/waterborne epoxy zinc-rich coating

The invention discloses a graphene/waterborne epoxy zinc-rich coating with high corrosion resistance and strong adhesion. The graphene/waterborne epoxy zinc-rich coating is composed of a component A and a component B. The component A comprises the following components in parts by mass: 0.3-1.5 parts of modified graphene, 5-25 parts of deionized water, 20-75 parts of waterborne epoxy resin and 0.3-1 part of a substrate wetting agent, and the component B comprises the following components in parts by mass: 40-70 parts of zinc powder, 15-30 parts of ethylene glycol monobutyl ether and 10-25 partsof a waterborne epoxy resin curing agent. According to the graphene/waterborne epoxy zinc-rich coating with high corrosion resistance and high adhesive force, graphene oxide is used as a precursor, polyethyleneimine is adopted for graft reduction of graphene oxide, graphene oxide is uniformly inserted and combined into waterborne epoxy resin through stirring and shearing effects, and a uniform system is achieved; and further stirring is conducted with a waterborne epoxy resin curing agent component mixed with zinc powder and ethylene glycol monobutyl ether to obtain the anticorrosive paint with high corrosion resistance and strong adhesive force.
Owner:广东豪之盛新材料有限公司

Environment-friendly fluoride-free foam extinguishing agent and preparation method thereof

The invention belongs to the technical field of fire extinguishing materials, particularly relates to an environment-friendly fluoride-free foam extinguishing agent and a preparation method thereof, and solves the problems that a traditional extinguishing agent in the prior art is toxic, not environment-friendly and limited in application range, and a fluorocarbon surfactant, a chelating agent andthe like used in an existing foam extinguishing agent are harmful to the environment. The technical scheme of the invention is as follows: the environment-friendly fluoride-free foam extinguishing agent is formed by mixing a foam concentrate liquid and water according to the volume ratio of 6:94; and the foam concentrate liquid includes the following ingredients: a modified organic silicon surfactant, lauryl sodium sulfate, alkyl glycoside, water-soluble imidazoline, dodecyl dimethyl betaine, dodecanol, polyethylene glycol, xanthan gum, sodium carboxymethylcellulose, ethylene glycol, urea, diethylene glycol monobutyl ether and water. According to the product, a traditional fluorocarbon surfactant is replaced with the modified organic silicon surfactant, so that the product is green and pollution-free, and can be widely applied to fire prevention key units such as oil fields, oil depots, ships, submarines, petrochemical plants, hangars, airports and the like.
Owner:SOUTHWEST PETROLEUM UNIV

Concrete shrinkage reducing agent and preparation method and application thereof

The invention relates to a concrete shrinkage reducing agent and a preparation method and application thereof. The preparation method comprises the following steps that acrylic polyether, an initiator and water are mixed to be uniform, a first reactant is obtained, and temperature rise is carried out; crylic acid and water are mixed to be uniform, and a second reactant is obtained; methacrylic acid diethylene glycol monobutyl ether ester and phellandrene are mixed to be uniform, and a third reactant is obtained; a reducing agent, a chain transfer agent and water are mixed to be uniform, and a fourth reactant is obtained; the second reactant, the third reactant and the fourth reactant are dropwise added into the first reactant obtained after temperature rise at the same time; after all the reactants are dropwise added, heat preservation is carried out, and then cooling is carried out; an alkaline solution and water are added into the obtained product, and the concrete shrinkage reducing agent is obtained. According to the prepared concrete shrinkage reducing agent, the water reducing and shrinkage function of the concrete shrinkage reducing agent can be enhanced, the antifreezing capacity, compressive strength and anti-cracking ability of concrete can be improved, and the service life of the concrete can be prolonged; the production cost of the concrete can be reduced, and the application range is wide.
Owner:江苏超力建材科技有限公司

Anti-breaking paint for glass and preparation method thereof

The invention discloses an anti-breaking paint for glass. The invention is characterized in that the anti-breaking paint for glass is prepared from the following raw materials in parts by weight: 43-48 parts of methyl organic silicon resin emulsion, 4-6 parts of nitrocellulose, 8-12 parts of modified styrene acrylic emulsion, 15-18 parts of 50% rubber latex, 1-2 parts of alcohol ester 12, 2-3 parts of 1,2-propanediol, 0.3-0.6 part of glycerol, 0.2-0.4 part of sorbitol alcohol, 1-2 parts of diethylene glycol monobutyl ether, 0.3-0.6 part of alkylol amino alkoxy titanate, 0.3-0.5 part of leveling agent BYK-307, 1-2 parts of N-methylpyrrolidone, 0.2-0.4 part of polyethylene wax emulsion, 1-2 parts of wollastonite powder, 1-2 parts of yttrium oxide crystal seed, 0.3-0.5 part of iron powder, 1-3 parts of pigment and 10-15 parts of deionized water. The modified styrene-acrylic emulsion added to the water-based paint has the bactericidal, dust-proof and antistatic actions; the added nitrocellulose and 50% rubber latex can protect the glass and reduce the possibility of breaking of the glass due to heating and pressure, thereby ensuring the personal safety. The paint is simple to produce and convenient to operate, and has the advantages of high drying rate, smooth paint film and excellent properties.
Owner:凤阳徽亨商贸有限公司

Novel environment-friendly thermal insulation anti-corrosive coating

The invention discloses novel environment-friendly thermal insulation anti-corrosive coating. The novel environment-friendly thermal insulation anti-corrosive coating comprises a component A, a component B and a component C, wherein the weight ratio of the component A to the component B to the component C is (500-1000): (50-80): 2, the component A comprises the following materials in parts by weight: 40-50 parts of acrylic emulsion, 140-180 parts of titanium dioxide, 35-45 parts of lithopone, 5-8 parts of expanded perlite, 3-5 parts of hollow glass beads, 3-5 parts of vermiculite, 3-5 parts of sericite powder, 8-12 parts of epoxy resin, 12-18 parts of acetone, 3-8 parts of ethylene glycol monobutyl ether, 1-3 parts of commercially available OP-10 type emulsifier, 0.1-0.3 part of sodium hydroxide, 30-50 parts of ethanol and 70-100 parts of deionized water; the component B comprises the following materials in parts by weight: 3-5 parts of coating curing agent, 2-4 parts of tetrachloroisophthalonitrile, 1-2 parts of antifreeze agent, 0.3-0.8 part of defoaming agent, 0.1-0.15 parts of sterilizing agent, 0.1-0.4 part of dispersant, 1-1.5 parts of alkali swelling thickening agent, 0.1-0.2 part of cellulose thickener, 0.1-0.15 part of wetting agent and 0.5-1 part of film-forming agent; and the component C is ultramarine or phthalocyanine blue or phthalocyanine green or phthalocyanine red or bright red.
Owner:苏州瑞邦塑胶有限公司
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