The present invention discloses a method for preparing a
methylation reaction catalyst and
tetramethylammonium methyl carbonate. The present invention uses
boron nitride ceramic as a carrier, and under the action of polyether, anchors
metal sites, and realizes functionalization reaction of C-H bonds by adjusting the steric hindrance of transition metals and long-chain hydrocarbons; surface
grafting is performed with organic amines, so that the surface of the
boron nitride ceramic is grafted to form a catalytic surface of -N-Fe- functional groups, and the orbital hybridization between Fe-N-C provides a unique
catalytic effect, and anchoring Fe by N is conducive to improving the single-atom dispersibility of Fe, further improving the
catalytic effect. The addition of co-catalyst Al, as a Lewis acid, can adjust the selectivity and
reaction rate of the reaction. The present catalytic
system has
high selectivity, greatly improving the spatiotemporal benefit of TMAC, and the catalyst structure is stable, acid and alkali resistant, and as a heterogeneous catalyst, it is easy to separate, does not introduce impurities into the
system, and can maintain the stability of catalytic performance for a long time.