The invention relates to the technical field of functional
polymer material preparation, in particular to a method for in-situ rapid synthesis of
carbon quantum dots based on a
spinning chemical process, and discloses a method for macroscopic preparation of
carbon quantum dots by using a
spinning chemical means. The method is characterized in that a novel process for preparing a carbon
quantum dot material by micro-fluidic gas injection is developed based on a
spinning chemistry principle, compounds with good
biocompatibility and
high activity, such as
citric acid and
urea, are used as functional precursors, and a strong heat release type
monomer, such as hydroxyethyl
acrylate and
hydroxypropyl methacrylate, is used as a medium through a point heat micro-fluidic gas injection means, so that the carbon
quantum dot material is prepared. According to the present invention, the carbon
quantum dot material is obtained in situ by using the thermal self-
catalysis effect and the large specific surface contact surface of the
exothermic reaction and using the
chip micro-channel and the micro-nano-
fiber as the reactor, the carbon
quantum dot is synthesized through the micro-nano-
fiber in-situ reaction, the operation is simple, the process condition is easy to control, and the strong promotion and application value is provided.