1756 results about "Dimethyl benzene" patented technology

The invention discloses a catalyst for preparing aromatic hydrocarbon through methanol conversion. The catalyst comprises a component A and components B, wherein the mass ratio of component A to components B is 0.25-4; the component A is a modified zeolite molecular sieve and comprises 80-99wt% of molecular sieves and 1-20wt% of molecular sieve modifiers; the components B are oxide loaded metallic elements and halogen and comprise 85-95wt% of oxide, 0.5-10wt% of total metallic elements and 0.1-5wt% of halogen; and the component A and the components B are formed through squashing or extruding after being mixed uniformly. The catalyst has the following characteristics that: (1) the total recovery of benzene, toluene and xylene is higher and selectivity is high; (2) the raw material treatment capacity is large; (3) the non-aromatic hydrocarbon liquid product can serve as the solvent oil or gasoline component; (4) C4 hydrocarbon and non-aromatic hydrocarbon liquid phase products in the gas phase product can circularly enter into the catalyst bed layer, thus not only balancing the reaction heat but also improving the total recovery of the aromatic hydrocarbon; and (5) the catalyst has high activity and long life.

The invention relates to a preparation method of an organic exhaust gas micro-emulsion absorption liquid, and a method for applying the micro-emulsion absorption liquid for cleaning industrial organic exhaust gas comprising benzene, toluene, xylene, and the like. The invention belongs to the technical field of atmosphere pollution control. The absorption liquid is prepared from the components of, by mass, 80-90% of water, 0.5-3% of a surfactant, 7-19.5% of a coupling agent, and 0.02-0.06% of an auxiliary agent. The surfactant is sufficiently mixed with water, such that a surfactant solution is obtained; the auxiliary agent is dissolved in water, such that an auxiliary agent solution is obtained; the two solutions are combined and uniformly mixed; and the coupling agent is added, and the obtained solution is stirred, such that the organic exhaust gas micro-emulsion absorption liquid is obtained. The organic exhaust gas micro-emulsion absorption liquid is suitable to be used for controlling exhaust gas containing benzene-series volatiles, and has the advantages of convenient raw material source, low cost, mild and stable property, low toxicity, environment-friendliness, no absorption tower corrosion or blocking phenomena, no severe influence to human health, high removal rate to organic exhaust gas, no need of pretreatment upon exhaust gas, and low investment and running cost. Saturated absorption liquid and absorbed organics can be recycled, such that waste can be turned useful.

The invention discloses a manufacturing method of paraffin sections of zostera marina embryo, comprising the following steps: (1) material drawing and fixation: zostera marina seeds are taken and the fruit skin is stripped, and after endosperm is removed, an integral zostera marina embryo is soaked in FAA (free amino acids) fixing solution and is fixed for more than 48 hours; (2) dehydration: the zostera marina embryo is taken out from the fixing solution and is soaked in alcohol for dehydration; (3) waxing and embedding: paraffin is added gradually in a vessel containing the zostera marina embryo and dimethylbenzene, and conventional paraffin embedding is carried out to obtain the wax blocks containing the zostera marina embryo; (4) slicing, spreading and drying: the wax blocks coated with the zostera marina embryo is fixed on a wheel rotation type slicing machine for carrying out continuous slicing of the paraffin, so as to obtain wax bands and enable the wax bands to be attached to an object slide; (5) dewaxing, rehydration and dyeing of hematoxylin dye solution; (6) slicing, dehydration and dyeing of eosin and alcohol; and (7) transparence and mounting are carried out to manufacture a permanent section. In the manufacturing method disclosed by the invention, the paraffin sections of the zostera marina embryo, which have clear dyeing and an integral texture structure, can be obtained.

The invention discloses a polyurethane chemical grouting water plugging-reinforcing material which comprises a component A and a component B. The invention is characterized in that the component A is composed of polyether glycol and auxiliary materials, and the component B is composed of isocyanate and/or prepolymer thereof and auxiliary materials; and the auxiliary materials comprise catalyst, foam stabilizer and other assistants. The polyurethane chemical grouting water plugging-reinforcing material disclosed by the invention does not contain benzene, xylene, acetone and other solvents and does not influence the water quality after curing, and the solid content is 100%, thereby being environment-friendly and pollution-free; and when in use, the reaction speed of the double components is very high, the reaction starts after 20 seconds and basically finishes after 90 seconds, the reaction time is adjustable according to the engineering demands, and thus, the polyurethane chemical grouting water plugging-reinforcing material can effectively and quickly solve the problems of water leakage and water inflow of mines.

The invention discloses an epoxy ester modified aqueous alkyd resin and a preparation method thereof. The method comprises the following steps of: preparing alkyd resin, synthesizing epoxy ester, and synthesizing the epoxy ester modified aqueous alkyd resin: stirring and mixing epoxy ester and basic alkyd resin in mass ratio of 0.2:1-0.5:1, 1-3 parts of organic tin catalyst and 5-15 parts of dimethyl benzene, and performing reflux reaction at the temperature of 180 DEG C for 1-2 hours until the acid value is measured to be less than 7mgKOH/g; and water-dissolving the modified alkyd resin. A product provided by the invention keeps superior performances of paint dryness, glossiness, durability, flexibility, hardness, higher solubility and the like of the alkyd resin, has superior cohesive property, salt fog resistance and good self-drying property of the epoxy resin, and can keep that a coating has superior solvent resistance and chemical resistance.

The invention discloses a production method for a paraffin section of a paeonia lactiflora mature embryo. The production method comprises the following steps: drawing materials and fixing: stripping a seed coat, cutting a seed, immersing the seed top part containing the embryo or part endosperm into a FAA stationary liquid, and fixing for more than 24 hours; dehydrating: washing in ethyl alcohol with the concentration of 70% for 3 to 5 times, and performing gradient dehydration from the ethyl alcohol with the concentration of 70%; performing hyalinization: carrying out five level hyalinization by using dimethyl benzene as a transparent reagent; waxing and embedding: pouring out one half volume of dimethyl benzene, adding wax crumbs in a bottle until saturation, staying overnight at the temperature of 40 DEG C; then changing a wax liquid every two hours for three times per day, repeating for three days, and carrying out conventional paraffin embedding; slicing; flattening and bonding: flattening a linoleum tape on an iron plate of a water bath kettle at the constant temperature of 50 DEG C, dewaxing, rehydrating, dyeing through safranine and fast green and performing hyalinization; mounting. According to the invention, the paeonia lactiflora mature embryo paraffin section of which the tissue structure is integrated and clear can be obtained, so that accurate technical support can be provided for researching paeonia lactiflora seed dormancy and germination.

The invention concerns a simulated moving bed adsorption separation device comprising a limited number of valves. According to the invention, the device comprises a column with a plurality of sectors Sk with 2 superimposed plates Pi with a single distribution network, each sector Sk comprising an external principal bypass line Lk connected to each plate Pi of Sk via a plate valve V_i. Each line Lk comprises a flow limitation means and is connected to each of the fluid networks via a single valve.

Further, the connectors of lines Lk onto the column are offset by at most 20° inside Sk to limit the volume of lines Lk, and are offset by a mean angle in the range 70° to 110° between two neighbouring sectors Sk and Sk+1 so as not to weaken the column mechanically. The plates preferably comprise panels DMEi,j with parallel segments the direction of which varies from plate to plate or per group of 2 plates.

The invention also concerns a separation process using said device, in particular to separate para-xylene or meta-xylene from an aromatic C8 cut.

The present invention provides a method for enhancing electrical characteristics of organic electronic devices, especially for an organic thin-film transistors, comprising the steps of: providing a substrate with a gate and an insulator layer formed thereon; preparing an organic solution by mixing materials of an organic semiconductor polymer, an organic insulator polymer, a conducting particle and a solvent; forming an organic semiconductor layer on top of the insulator layer between the source and the drain using the organic solvent. Wherein, the organic semiconductor polymer can be a polymer selected from the group consisting of poly(3-alkylthiophene) (P3AT) with different alkyl side groups of 2, 4, 6, 8, 10, 12, and 18, as the P3HT is a P3AT with alkyl side group of 6, and the organic insulator polymer can be a polymer selected from the group consisting of poly(methylmethacrylate) (PMMA), and polybutylene terephthalate (PBT), etc. and the conducting particle can be a kind of particle selected from the group consisting of carbon nanotubes (CNTs), C₆₀, and nano silver particle, and so on, and the solvent can be a solvent selected from the group consisting of xylene, toluene, and THF, and so forth.

A synthesis method of polycarbosilane capable of being used for thermosetting crosslinking comprises the following steps: taking polycarbosilane used for preparing a composite material as a raw material; placing the polycarbosilane used for preparing the composite material and an organosilan compound containing 2 to 3 -C=C- groups into a reaction vessel; adding dimethyl benzene; mixing uniformly for dissolving; adding a Si-H additive reaction catalyst; vacuumizing; carrying out replacing with high-purity nitrogen; carrying out an Si-H additive reaction under a normal-pressure or high-pressure heating condition and the protection of the high-purity nitrogen. The synthesis method is simple and convenient, and easy to implement; the product PVCS can be used for self-setting crosslinking under an inert atmosphere after being treated at 400 DEG C; the smelting outflow of PCS during heat treatment can be avoided; the ceramic yield can be improved remarkably; the polycarbosilane synthesized according to the synthesize method can be used as a precursor polymer of ceramic-based composite materials such as Cf/SiC, and SiCf/SiC.

A green making technology of animal tissue paraffin section disclosed in the invention aims at providing a technique of making a paraffin section of animal tissue applied to the agricultural university medicine and other majors, characterized by that the type of chemical reagents that are used is limited, the chemical reagents have no toxicity, and dehydrate the tissue thoroughly, accelerate making sections but not lead to excessive contraction and increasement of hardness of the tissue, and substitute dimethyl benzene used in the traditional making technology of the paraffin section which isharmful to human body, so as to eliminate the occupational diseases and environmental pollution caused by dimethyl benzene. The making technology comprises the following steps: carrying out fixation with a fixative solution (100ml of the fixative solution comprises 91 ml 85% alcohol, 4 ml methanol and 5 ml glacial acetic acid ), dehydrating the tissue with graded ethanol, then putting the fixative and dehydrated tissue in a mixed transparent reagent (comprising 14wt% of analytically pour n-butanol, 29wt% of acetone and 57wt% of absolute alcohol ) for standing for 3 hours, then carrying out normal waxing and embedding, using analytically pour turpentine (60 DEG C) for section staining, carrying out dewaxing twice, carrying out hydration under normal temperature, using haematoxylin for staining nuclei, decoloration and bluing, and using eosin for staining, dehydrating until get absolute alcohol, then carrying out air drying, and directly using the gum diluted by turpentine to sealing the section.

The invention relates to a method for preparing an aromatic hydrocarbon mixture rich in benzene, toluene and xylene (BTX) by conversion of methanol in a fixed bed reactor. The method comprises the following steps of feeding a catalyst for preparation of low-carbon olefin by conversion of methanol and a catalyst for aromatization of low-carbon olefin in the same fixed bed reactor to form a catalyst combined unit in which the lower layer is the catalyst for aromatization of low-carbon olefin and the upper layer is catalyst for preparation of low-carbon olefin by conversion of methanol; dividing methanol steam into a plurality of blasts, mixing one blast of the methanol steam, circulating LPG and water steam to obtain a mixture, feeding the mixture into the fixed bed reactor from a material inlet formed in the top of the fixed bed reactor, feeding the residual methanol steam into the fixed bed reactor from a material inlet formed in the side wall of the reactor to obtain the aromatic hydrocarbon mixture rich in BTX. The method has the advantages that the process is simple, the cost is low and the large-scale production can be achieved.

The invention discloses a method for preparing a high-barrier graphene oxide-polyethylene nano composite film. The method comprises the following steps: ultrasonically dispersing modified graphene oxide into xylene and heating; then adding high-density polyethylene and stirring so as to obtain an ODA-GO/HDP mixed solution; cleaning an ultra-high molecular weight polyethylene film by xylene; after xylene is evaporated, soaking a UHMWPE film into a hot ODA-GO/HDPE mixed solution in a dipping manner; drying; and repeating the above steps until the required layer quantity is reached. The high-barrier graphene oxide-polyethylene nano composite film prepared by the method is high in safety and good in environmental protection property; the oxygen permeating coefficient is reduced by about 49%; the nano composite film has ultra-high oxygen barrier property, can meet the packaging requirements of a plurality of foods and drugs and use of other products, is simple in process and low in cost, and has broad practicability and promotional value.

Disclosed is a porous film formed of a polyolefin resin comprising an ethylene-α-olefin copolymer (A) which comprises structural units originating from ethylene and structural units originating from one or more sorts of monomers selected from α-olefins having 4-8 carbon atoms and which satisfies the requirements (I) the intrinsic viscosity [η] is 9.0 to 15.0 dl/g; (II) the melting point Tm is not lower than 115° C. but lower than 130° C.; (III) the content of cold-xylene-soluble components included in the ethylene-α-olefin copolymer (A) is 3% by weight or less; and (IV) Tm≦0.54×[η]+114. A battery separator including the porous film and a method for the preparation of the porous film are also disclosed.

The invention belongs to the technical field of the preparation of high-temperature anti-oxidation coatings, in particular to an anti-oxidation coating used in a long-time heat treatment process of iron, and the like at high temperature. The coating comprises solid powder and liquid, and is characterized in that the solid powder comprises following components by weight part: 30 to 50 parts of glass powder, 10 to 50 parts of boron nitride, 2 to 5 parts of chromic oxide and 3 to 10 parts of metal aluminum powder; and the liquid comprises following components by weight part: 0.1 to 5 parts of modified magnesium aluminosilicate, 20 to 35 parts of organic silicone resin and 100 parts of xylene. Through the adoption of the coating, oxydic weight gain of carbon steel or alloy steel can be guaranteed to be reduced by more than 80 percent in the heat treatment process for a long time (larger than 30 hours) at temperature of 1200 DEG C and above.

Methods and apparatus for introducing a gas into the reaction zone of a reactor. Such methods and apparatus can more evenly distribute the gas throughout the reaction zone. Spargers for introducing a gas into the reaction zone of a reactor can be employed in systems and methods for carrying out the liquid-phase oxidation of an oxidizable compound, such as para-xylene.

The invention discloses acoustic wool with high impact resistance. The acoustic wool is prepared from, by weight, 1-2 parts of barium stearate, 0.5-1 part of sodium xylene sulfonate, 5-10 parts of zircon powder, 3-5 parts of silicon carbide, 1-2 parts of ethylene bis stearamide, 80-100 parts of polypropylene, 2-4 parts of styrene, 1-2 parts of epoxy rice bran oleic acid butyl ester, 3-5 parts of butyl methacrylate, 1-2 parts of polyethylene glycol, 0.05-0.1 part of azodiisobutyronitrile, 0.5-1 part of castor oil and 3-5 parts of functional powder. The acoustic wool is good in sound absorption effect and mechanical performance, high in durability, high in impact resistance, less prone to deformation, good in processing performance, capable of absorbing harmful substances in air, effectively purifying the air and protecting human health, high in comprehensive value and high in practicality.

The present invention is related to a nano-structured composite material and process of making for air detoxing and deodoring in enclosed spaces to prevent harmful chemicals in the air from damaging human health. The nano-structured composite material consists of nano-porous carbon, zeolites with sub nano-size pores and at least 1 other component chosen from nano-porous rare earth oxides and nano-sized catalysts, and is made into highly efficient configurations with high geometric surface and low resistance air flow channels. The synergetic action of those nano-structured components can effectively remove toxic chemicals including, but not limited to formaldehyde, benzene, toluene, xylene, propene, butadiene, acetone, carbon monoxide, nitric oxide, nitrogen dioxide, sulfur dioxide, hydrogen sulfide, ammonia, alcohols, chlorine, mercaptans, as well as bad odors, such cigarette smoke and bathroom/toilet smells.

A micro electromechanical (MEMS) antenna (36) is positioned on one side of a substrate and is connected to a MEMS switch comprising a capacitor bridge (46) and to a transmission line (42) by means of a thru hole or via (48) which forms an electrically conducting path through the substrate. This arrangement provides a common ground plane for the antenna and switch and shields the switch from the electromagnetic radiation received or transmitted from the antenna. The switch may comprise a topmost metal layer which extends across a bridge structure formed by a polymer layer (19). The polymer layer comprises poly-monochloro-para-xylene (parylene-C). Homogeneous or heterogeneous antenna array structures are implemented. The antenna arrays may include one or more different type of antennas with for example different shapes, rotations and reflections.

The invention belongs to the technical field of chemical industry catalysis, and particularly relates to a catalyst for converting an alcohol ether into a high p-xylene content aromatic hydrocarbon, a preparation method and a reaction process thereof. According to the present invention, a molecular sieve loading a metal, phosphorus and rare earth and other reinforcing components are adopted to form high mechanical strength particles, and the surface acid sites are 0.01-1% (molar fraction) of the total acid sites of the catalyst; the preparation method relates to a method for forming composite particles through multiple forming and controlling acid of the surface of the composite particles; and the catalyst can be applicable for fixed beds, moving beds and fluidized beds, and can be provided for converting methanol or dimethyl ether raw materials containing water and a small amount of high carbon alcohol and ester, wherein one-time conversion efficiency of the methanol or the dimethyl ether at a temperature of 450-520 DEG C and a space velocity of 0.2-30 h <-1> is more than 99.9%, the total (carbon-base) yield of the aromatic hydrocarbon is more than 60%, and the mass fraction of the p-xylene in the xylene is more than 90%.

Belonging to the field of epoxy resin coatings, the invention discloses an epoxy modified alkyd resin and its high hardness fast reaction coating. The epoxy modified alkyd resin is prepared by the method of: (1) mixing polyhydric alcohol with polyprotic acid, adding xylene, then performing heating reaction for 1-2h, raising the temperature to completely react, thus obtaining alkyd resin; (2) mixing epoxy resin, alkyd resin and a catalyst, performing heating reaction for 2-4h, carrying out filtering and discharging, thus obtaining epoxy modified alkyd resin, which has the advantages of good adhesion (0 level), good fullness, strong toughness (2mm), high epoxy resin mechanical strength (6H), and excellent corrosion resistance. The high hardness fast reaction coating made of the epoxy modified alkyd resin has the characteristics of high hardness, good toughness and fast drying speed (4h). According to the invention, the raw materials are easily available, and the process is simple. The prepared product has a high solid content and good leveling property, and is easy to achieve film coating.